Process for preparing spinning dope of cellulose base fibre by solvent process

A process for preparing the raw dope for cellulose fibre by solvent method includes shearing the pulp, balancing at 30-50 deg.C and vacuum state for 6-12 hr, vacuum evaporation concentrating of the aqueous solution of N-methyl morpholine oxide (NMMO), mixing said pulp with the aqueous solution of NM...

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Bibliographische Detailangaben
Hauptverfasser: HUIYU SHAO, XUECHAO HU, TANLI ZHANG
Format: Patent
Sprache:eng
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Zusammenfassung:A process for preparing the raw dope for cellulose fibre by solvent method includes shearing the pulp, balancing at 30-50 deg.C and vacuum state for 6-12 hr, vacuum evaporation concentrating of the aqueous solution of N-methyl morpholine oxide (NMMO), mixing said pulp with the aqueous solution of NMMO, still standing at 70-90 deg.C for 20-40 min, fast stirring for 20-60 min, vacuumizing while slowly heating to 90-125 deg.C, and maintaining the temp for 3-6 hr.