Method for treating fluorine ions in m-aminobenzotrifluoride

The invention belongs to the technical field of chemical engineering, and particularly relates to a method for treating fluorine ions in m-aminotrifluorotoluene, which comprises the following steps: S1, pretreating biomass, and then mixing the treated biomass with fine lime of which the main compone...

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Hauptverfasser: LYU LEPING, ZHANG LIANG, LI FUXIANG, CAO ZE, ZHENG LONGSHENG, ZHAO TIANYIN
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creator LYU LEPING
ZHANG LIANG
LI FUXIANG
CAO ZE
ZHENG LONGSHENG
ZHAO TIANYIN
description The invention belongs to the technical field of chemical engineering, and particularly relates to a method for treating fluorine ions in m-aminotrifluorotoluene, which comprises the following steps: S1, pretreating biomass, and then mixing the treated biomass with fine lime of which the main component is calcium oxide to obtain a remover; s2, adding a remover into the m-aminotrifluorotoluene crude product in proportion, fully stirring and mixing the remover and the m-aminotrifluorotoluene crude product by using a mixing device, and adsorbing generated calcium fluoride precipitate by using biomass; s3, filtering the liquid in the mixing device, and separating the biomass and the calcium fluoride precipitate from the liquid; s4, drying the filtered filtrate, namely the m-aminobenzotrifluoride in which the fluorine ions are removed, so as to obtain refined m-aminobenzotrifluoride; according to the invention, biomass is utilized to adsorb calcium fluoride precipitate, the effect of subsequent single filtration is
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subjects ACYCLIC OR CARBOCYCLIC COMPOUNDS
CHEMISTRY
METALLURGY
MIXING, e.g. DISSOLVING, EMULSIFYING, DISPERSING
ORGANIC CHEMISTRY
PERFORMING OPERATIONS
PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
TRANSPORTING
title Method for treating fluorine ions in m-aminobenzotrifluoride
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