Method for preparing ammonium chloride by evaporating ionic rare earth separated high-salinity wastewater

The invention discloses a method for preparing ammonium chloride by evaporating ionic rare earth separation high-salinity wastewater, which comprises the following steps: adding an alkaline substance into the ionic rare earth separation high-salinity wastewater, and carrying out solid-liquid separat...

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Hauptverfasser: LIU ZHIQIANG, HAN XINFU, YAN BO, CAO YUAN, QIN GUANGZONG, LING CHENG, LIN HAO, MA BAILONG, HAN XIAOYAN, LI CHUNDE, YUAN XIUJUAN, LIU HONGPING, YANG QINGYU, LIN YONGSHEN, HAN JINCHENG
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creator LIU ZHIQIANG
HAN XINFU
YAN BO
CAO YUAN
QIN GUANGZONG
LING CHENG
LIN HAO
MA BAILONG
HAN XIAOYAN
LI CHUNDE
YUAN XIUJUAN
LIU HONGPING
YANG QINGYU
LIN YONGSHEN
HAN JINCHENG
description The invention discloses a method for preparing ammonium chloride by evaporating ionic rare earth separation high-salinity wastewater, which comprises the following steps: adding an alkaline substance into the ionic rare earth separation high-salinity wastewater, and carrying out solid-liquid separation to obtain impurity-removed pretreated wastewater; wherein the ionic rare earth separation high-salinity wastewater comprises ammonium chloride; carrying out evaporative crystallization on the pretreated wastewater until the volume is reduced to 10-30%, and carrying out solid-liquid separation to obtain an ammonium chloride product and crystallization mother liquor; and extracting the crystallization mother liquor by adopting an organic phase containing an extracting agent, carrying out phase splitting to obtain raffinate, combining the raffinate with the pretreated wastewater, and repeating the evaporative crystallization step. According to the method for preparing the ammonium chloride through evaporation of t
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subjects AMMONIA
CHEMISTRY
COMPOUNDS THEREOF
CYANOGEN
INORGANIC CHEMISTRY
METALLURGY
TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
title Method for preparing ammonium chloride by evaporating ionic rare earth separated high-salinity wastewater
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