Preparation method of anhydrous organic titanium cross-linking agent concentrated solution and cross-linking type integrated suspension fracturing fluid

The invention discloses an anhydrous organic titanium cross-linking agent concentrated solution preparation method, which comprises: 1) uniformly mixing butyl titanate, triethanolamine, lactic acid and water, and heating to carry out a synthesis reaction to obtain a triethanolamine titanium lactate...

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Hauptverfasser: ZHANG XINGQIAO, JIA ZHENFU, ZUO CHENGWEI, SU XIAODONG, ZHANG HAN, LI XIAOJIANG, GAO XIAOTONG
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creator ZHANG XINGQIAO
JIA ZHENFU
ZUO CHENGWEI
SU XIAODONG
ZHANG HAN
LI XIAOJIANG
GAO XIAOTONG
description The invention discloses an anhydrous organic titanium cross-linking agent concentrated solution preparation method, which comprises: 1) uniformly mixing butyl titanate, triethanolamine, lactic acid and water, and heating to carry out a synthesis reaction to obtain a triethanolamine titanium lactate organic cross-linking agent; and 2) adding the triethanolamine titanium lactate organic cross-linking agent into a dialysis bag for dialysis, and concentrating and drying dialysate to obtain an anhydrous organic titanium cross-linking agent concentrated solution. The invention also provides a cross-linking type integrated suspension fracturing fluid containing the anhydrous organic titanium cross-linking agent concentrated solution. According to the anhydrous organic titanium cross-linking agent concentrated solution provided by the invention, a synthesized triethanolamine lactic acid titanium organic cross-linking agent is subjected to impurity removal through a dialysis process and then is concentrated and purifi
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The invention also provides a cross-linking type integrated suspension fracturing fluid containing the anhydrous organic titanium cross-linking agent concentrated solution. 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subjects ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAININGELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN,SULFUR, SELENIUM OR TELLURIUM
ADHESIVES
CHEMISTRY
DYES
MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FORELSEWHERE
METALLURGY
MISCELLANEOUS APPLICATIONS OF MATERIALS
MISCELLANEOUS COMPOSITIONS
NATURAL RESINS
ORGANIC CHEMISTRY
PAINTS
POLISHES
title Preparation method of anhydrous organic titanium cross-linking agent concentrated solution and cross-linking type integrated suspension fracturing fluid
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