Air entraining retaining type water reducing agent based on special molecular weight distribution and preparation method of air entraining retaining type water reducing agent

The invention discloses an air entraining retaining type water reducing agent based on special molecular weight distribution and a preparation method thereof. The water reducing agent is prepared from an isopentenol polyoxyethylene ether monomer, isoester, an unsaturated carboxylic acid monomer, a r...

Ausführliche Beschreibung

Gespeichert in:
Bibliographische Detailangaben
Hauptverfasser: TAO YUNGANG, LIAO JIANDU, CHEN YUCHAO, CHEN QINGMING, ZHAO SILI, HE SHUANGXI, WANG CHUNGUANG, NING QINGGONG, REN JUNXIAN, LIU ZITAI
Format: Patent
Sprache:chi ; eng
Schlagworte:
Online-Zugang:Volltext bestellen
Tags: Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
Beschreibung
Zusammenfassung:The invention discloses an air entraining retaining type water reducing agent based on special molecular weight distribution and a preparation method thereof. The water reducing agent is prepared from an isopentenol polyoxyethylene ether monomer, isoester, an unsaturated carboxylic acid monomer, a reducing agent, a chain transfer agent and an initiator through a free radical polymerization reaction. The preparation method comprises the following steps: firstly, adding a polyoxyethylene ether monomer and water into a reaction kettle, heating to 60-70 DEG C, stirring to obtain a monomer solution, adding half of an initiator, reacting for 1-2 hours at a constant temperature, dropwise adding a solution A prepared by mixing unsaturated carboxylic acid, isoester and water and a solution B prepared by mixing a reducing agent, a chain transfer agent and water at a constant speed, and reacting for 1-2 hours at a constant temperature; and uniformly adding the residual initiator in 3-5 times in the dropwise adding proce