Preparation method of g-C3N4 catalyst for degrading tetracycline
The invention discloses a preparation method of a g-C3N4 catalyst for efficiently degrading tetracycline, which comprises the following steps: S1, mixing and stirring melamine and a cyanuric acid solution at room temperature to generate a precipitate, and filtering to obtain the precipitate; s2, the...
Gespeichert in:
Hauptverfasser: | , |
---|---|
Format: | Patent |
Sprache: | chi ; eng |
Schlagworte: | |
Online-Zugang: | Volltext bestellen |
Tags: |
Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
|
Zusammenfassung: | The invention discloses a preparation method of a g-C3N4 catalyst for efficiently degrading tetracycline, which comprises the following steps: S1, mixing and stirring melamine and a cyanuric acid solution at room temperature to generate a precipitate, and filtering to obtain the precipitate; s2, the obtained precipitate is washed and dried, and a g-C3N4 precursor is obtained; s3, the obtained g-C3N4 precursor is placed in a protective atmosphere, heating and pyrolysis are conducted, and the g-C3N4 catalyst of the disordered structure is obtained. Experimental results show that the g-C3N4 catalyst has an ultrathin sheet-shaped porous morphology and a large specific surface area, has higher photo-induced electron hole separation efficiency, and shows high catalytic activity when tetracycline is subjected to photocatalytic degradation.
本发明公开了一种用于高效降解四环素的g-C3N4催化剂的制备方法,包括以下步骤:S1、将三聚氰胺、三聚氰酸溶液室温下混合,搅拌,生成沉淀后过滤,得到沉淀物;S2、将所得沉淀物进行洗涤,干燥,得到g-C3N4前躯体;S3、将所得g-C3N4前躯体置于保护性气氛下,升温,热解,得到结构无序的g-C3N4催化剂。实验结果表明,该g-C3N4催化剂具有超薄片状的多 |
---|