Method for simultaneously determining pesticides and antibiotics in soil and marine sediments
The invention discloses a method for simultaneously determining pesticides and antibiotics in soil and marine sediments, which comprises the following steps of: firstly, extracting compounds in a purified soil sample or marine sediment sample by using an improved solid-phase extraction method, and t...
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Format: | Patent |
Sprache: | chi ; eng |
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Zusammenfassung: | The invention discloses a method for simultaneously determining pesticides and antibiotics in soil and marine sediments, which comprises the following steps of: firstly, extracting compounds in a purified soil sample or marine sediment sample by using an improved solid-phase extraction method, and taking supernate as a tested sample; then, analyzing the matrix matching standard solution by using an ultra-high performance liquid chromatography-tandem mass spectrometer, drawing a matrix matching standard curve by taking the peak area of the quantitative ion mass chromatogram of the compound as a vertical coordinate and the mass concentration corresponding to the compound in the matrix matching standard solution as a horizontal coordinate, and determining the linear range of quantitative determination of each compound; and finally, carrying out qualitative analysis on the tested sample by using an ultra-high performance liquid chromatography-tandem mass spectrometer to determine whether the target compound exist |
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