Process for manufacture of isophorone diamines

Process for manufacture of isophorone diamines

The invention relates to a method for producing IPDA, comprising the following steps: V. converting IPN into IPDA with ammonia and hydrogen, VI. Removing hydrogen and/or ammonia from the effluent from step I; vII. The effluent from step II is separated in one or more steps into (v) a fraction compri...

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Hauptverfasser: SCHRU DER, MARC, HERRMANN ANDREAS EDGAR, GOUVENIER HUBERT F, KRAUSE, ANDREAS
Format: Patent
Sprache:chi ; eng
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ACYCLIC OR CARBOCYCLIC COMPOUNDS
CHEMISTRY
METALLURGY
ORGANIC CHEMISTRY
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creator SCHRU DER, MARC
HERRMANN ANDREAS EDGAR
GOUVENIER HUBERT F
KRAUSE, ANDREAS
description The invention relates to a method for producing IPDA, comprising the following steps: V. converting IPN into IPDA with ammonia and hydrogen, VI. Removing hydrogen and/or ammonia from the effluent from step I; vII. The effluent from step II is separated in one or more steps into (v) a fraction comprising an organic phase having a boiling point lower than IPDA, (vi) a fraction comprising an aqueous phase having a boiling point lower than IPDA, (vii) a fraction comprising IPDA, (viii) a fraction comprising components having a boiling point higher than IPDA; and VIII. Subjecting fraction (ii) to one or more wastewater pretreatment steps selected from evaporation, oxidation and adsorption. 本发明涉及一种生产IPDA的方法，包括下列步骤：V.用氨和氢气将IPN转化为IPDA，VI.从来自步骤I的流出物除去氢气和/或氨；VII.在一个或多个步骤中将来自步骤II的流出物分离为(v)包含沸点低于IPDA的有机相的馏分，(vi)包含沸点低于IPDA的水相的馏分，(vii)包含IPDA的馏分，(viii)包含沸点高于IPDA的组分的馏分；以及VIII.使馏分(ii)经历一个或多个选自蒸发、氧化和吸附的废水预处理步骤。
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CHEMISTRY
METALLURGY
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title Process for manufacture of isophorone diamines
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