Preparation method for efficiently synthesizing ferrocene tetrafluoroborate

Preparation method for efficiently synthesizing ferrocene tetrafluoroborate

The invention relates to the technical field of ferrocene tetrafluoroborate, and discloses a preparation method for efficiently synthesizing ferrocene tetrafluoroborate, which comprises the following steps: at normal temperature, adding ferrocene and p-benzoquinone into a round-bottom flask filled w...

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Hauptverfasser: XU YINGYU, WU GUOYIN, ZHANG LEBO, NIU ZUORAN
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Sprache:chi ; eng
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ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAININGELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN,SULFUR, SELENIUM OR TELLURIUM
CHEMISTRY
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ORGANIC CHEMISTRY
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creator XU YINGYU
WU GUOYIN
ZHANG LEBO
NIU ZUORAN
description The invention relates to the technical field of ferrocene tetrafluoroborate, and discloses a preparation method for efficiently synthesizing ferrocene tetrafluoroborate, which comprises the following steps: at normal temperature, adding ferrocene and p-benzoquinone into a round-bottom flask filled with an absolute ether solution, stirring for 20-50 minutes, then continuously dropwise adding a tetrafluoroborate-diethyl ether complex into the round-bottom flask, stirring, filtering, washing, and drying to obtain the ferrocene tetrafluoroborate. The preparation method comprises the following steps: reacting for 30-60 minutes to generate a bluish violet precipitate in a round-bottom flask, filtering a solution obtained in the round-bottom flask to obtain the bluish violet precipitate, stirring and dissolving the obtained bluish violet precipitate in a round-bottom beaker filled with acetone, then adding absolute ether, separating out the bluish violet precipitate, repeating the step for 3-6 times, filtering the o
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The preparation method comprises the following steps: reacting for 30-60 minutes to generate a bluish violet precipitate in a round-bottom flask, filtering a solution obtained in the round-bottom flask to obtain the bluish violet precipitate, stirring and dissolving the obtained bluish violet precipitate in a round-bottom beaker filled with acetone, then adding absolute ether, separating out the bluish violet precipitate, repeating the step for 3-6 times, filtering the o</abstract><oa>free_for_read</oa></addata></record>
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subjects ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAININGELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN,SULFUR, SELENIUM OR TELLURIUM
CHEMISTRY
METALLURGY
ORGANIC CHEMISTRY
title Preparation method for efficiently synthesizing ferrocene tetrafluoroborate
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