Method for detecting 3-acetyl-2, 5-dimethylfuran in food

The invention belongs to the field of analysis and detection, and relates to a method for detecting 3-acetyl-2, 5-dimethylfuran in food, which comprises the following steps: taking a proper amount of sample in a centrifuge tube, adding n-heptane for ultrasonic extraction, centrifuging, freezing, pur...

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Hauptverfasser: SUN MENG, XIAO JINJIN, NAN QIAN, HAN JIANXUN, WEI HAIYAN, FU YU
Format: Patent
Sprache:chi ; eng
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Zusammenfassung:The invention belongs to the field of analysis and detection, and relates to a method for detecting 3-acetyl-2, 5-dimethylfuran in food, which comprises the following steps: taking a proper amount of sample in a centrifuge tube, adding n-heptane for ultrasonic extraction, centrifuging, freezing, purifying and filtering the extracting solution for GC-MS (Gas Chromatography-Mass Spectrometer) analysis. The method is simple to operate and high in accuracy and precision, and can be used for determining the 3-acetyl-2, 5-dimethylfuran in food. 本发明属于分析检测领域,涉及一种食品中3-乙酰基-2,5-二甲基呋喃的检测方法,包括以下步骤:取适量样品于离心管中,加入正庚烷超声提取,提取液经离心、冷冻、净化、过滤后供GC-MS分析。该方法操作简单,准确度精密度高,可用于食品中3-乙酰基-2,5-二甲基呋喃的测定。