Method for separating out spessartite crystals on surfaces of ZTA particles
The invention provides a method for separating out spessartite crystals on the surfaces of ZTA particles, which comprises the following steps: melting a crystallization agent, quickly cooling, and ball-milling to obtain glass powder; coating the surfaces of the ZTA particles with the glass powder; r...
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Format: | Patent |
Sprache: | chi ; eng |
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Zusammenfassung: | The invention provides a method for separating out spessartite crystals on the surfaces of ZTA particles, which comprises the following steps: melting a crystallization agent, quickly cooling, and ball-milling to obtain glass powder; coating the surfaces of the ZTA particles with the glass powder; raising the temperature of the ZTA particles coated with the glass powder to 850-900 DEG C, and keeping the temperature, so that spessartite crystals are separated out from the surfaces of the ZTA particles; the crystallization agent comprises 60 to 65 wt% of boron glass powder, 10 to 15 wt% of ammonium dihydrogen phosphate, 10 to 15 wt% of sodium carbonate, 8 to 12 wt% of manganese dioxide and 5 to 8 wt% of calcium fluoride.
本发明提供了一种在ZTA颗粒表面析出锰铝榴石晶体的方法,包括如下步骤:将析晶剂熔融后,快速冷却后球磨,得到玻璃粉体;将玻璃粉体包覆于ZTA颗粒表面;将包覆有所述玻璃粉体的ZTA颗粒升温至850-900℃下保温,使ZTA颗粒表面析出锰铝榴石晶体;所述析晶剂包括60-65wt%的硼玻璃粉、10-15wt%磷酸二氢铵、10-15wt%碳酸钠、8-12wt%二氧化锰和5-8wt%氟化钙。 |
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