Method for preparing ultra-roughening liquid from regenerated liquid obtained after copper recovery and ultra-roughening method
The invention discloses a method for preparing an ultra-roughening solution from a regenerated solution obtained after copper recovery and an ultra-roughening method.The method for preparing the ultra-roughening solution comprises the following steps that ethyl alcohol and deionized water are added...
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creator | WANG XUAN HUANG MING'AN WANG BINGYI |
description | The invention discloses a method for preparing an ultra-roughening solution from a regenerated solution obtained after copper recovery and an ultra-roughening method.The method for preparing the ultra-roughening solution comprises the following steps that ethyl alcohol and deionized water are added into a silane coupling agent for hydrolysis, silane hydrolysate is prepared, and the volume percentage of the silane coupling agent to the ethyl alcohol to the deionized water is 5: 35: 60; adding the prepared silane hydrolysate into the regenerated liquid, wherein the addition amount of the silane hydrolysate is 2-3% of the volume of the regenerated liquid; formic acid is added into the regeneration liquid, the super-roughening liquid is prepared after uniform stirring, and the addition amount of the formic acid is 3-5% of the volume of the regeneration liquid. According to the super-roughening liquid prepared by the method, a micro adsorption layer is formed on a copper surface by using the coupling agent, and a |
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According to the super-roughening liquid prepared by the method, a micro adsorption layer is formed on a copper surface by using the coupling agent, and a</description><language>chi ; eng</language><subject>CHEMICAL SURFACE TREATMENT ; CHEMISTRY ; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATIONOR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL ; COATING MATERIAL WITH METALLIC MATERIAL ; COATING METALLIC MATERIAL ; DIFFUSION TREATMENT OF METALLIC MATERIAL ; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION INGENERAL ; METALLURGY ; MULTI-STEP PROCESSES FOR SURFACE TREATMENT OF METALLICMATERIAL INVOLVING AT LEAST ONE PROCESS PROVIDED FOR IN CLASSC23 AND AT LEAST ONEPROCESS COVERED BY SUBCLASS C21D OR C22F OR CLASS C25 ; NON-MECHANICAL REMOVAL OF METALLIC MATERIAL FROM SURFACE</subject><creationdate>2023</creationdate><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&date=20230707&DB=EPODOC&CC=CN&NR=116397229A$$EHTML$$P50$$Gepo$$Hfree_for_read</linktohtml><link.rule.ids>230,308,780,885,25564,76547</link.rule.ids><linktorsrc>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&date=20230707&DB=EPODOC&CC=CN&NR=116397229A$$EView_record_in_European_Patent_Office$$FView_record_in_$$GEuropean_Patent_Office$$Hfree_for_read</linktorsrc></links><search><creatorcontrib>WANG XUAN</creatorcontrib><creatorcontrib>HUANG MING'AN</creatorcontrib><creatorcontrib>WANG BINGYI</creatorcontrib><title>Method for preparing ultra-roughening liquid from regenerated liquid obtained after copper recovery and ultra-roughening method</title><description>The invention discloses a method for preparing an ultra-roughening solution from a regenerated solution obtained after copper recovery and an ultra-roughening method.The method for preparing the ultra-roughening solution comprises the following steps that ethyl alcohol and deionized water are added into a silane coupling agent for hydrolysis, silane hydrolysate is prepared, and the volume percentage of the silane coupling agent to the ethyl alcohol to the deionized water is 5: 35: 60; adding the prepared silane hydrolysate into the regenerated liquid, wherein the addition amount of the silane hydrolysate is 2-3% of the volume of the regenerated liquid; formic acid is added into the regeneration liquid, the super-roughening liquid is prepared after uniform stirring, and the addition amount of the formic acid is 3-5% of the volume of the regeneration liquid. 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According to the super-roughening liquid prepared by the method, a micro adsorption layer is formed on a copper surface by using the coupling agent, and a</abstract><oa>free_for_read</oa></addata></record> |
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subjects | CHEMICAL SURFACE TREATMENT CHEMISTRY COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATIONOR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL COATING MATERIAL WITH METALLIC MATERIAL COATING METALLIC MATERIAL DIFFUSION TREATMENT OF METALLIC MATERIAL INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION INGENERAL METALLURGY MULTI-STEP PROCESSES FOR SURFACE TREATMENT OF METALLICMATERIAL INVOLVING AT LEAST ONE PROCESS PROVIDED FOR IN CLASSC23 AND AT LEAST ONEPROCESS COVERED BY SUBCLASS C21D OR C22F OR CLASS C25 NON-MECHANICAL REMOVAL OF METALLIC MATERIAL FROM SURFACE |
title | Method for preparing ultra-roughening liquid from regenerated liquid obtained after copper recovery and ultra-roughening method |
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