Preparation method of degradable high-strength closed-cell polylactic acid foam material
The invention provides a preparation method of a degradable high-strength closed-cell polylactic acid foam material, and belongs to the technical field of high polymer materials. Comprising the following steps: A, preparing modified nano SiO2 particles grafted with acrylic acid; b, mechanically crus...
Gespeichert in:
Hauptverfasser: | , , , , |
---|---|
Format: | Patent |
Sprache: | chi ; eng |
Schlagworte: | |
Online-Zugang: | Volltext bestellen |
Tags: |
Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
|
container_end_page | |
---|---|
container_issue | |
container_start_page | |
container_title | |
container_volume | |
creator | ZHANG LEI YANG CHENGUANG GUO QINGSHI JIANG XIANGYANG SUN HUIQING |
description | The invention provides a preparation method of a degradable high-strength closed-cell polylactic acid foam material, and belongs to the technical field of high polymer materials. Comprising the following steps: A, preparing modified nano SiO2 particles grafted with acrylic acid; b, mechanically crushing the toughening grade PLA resin particles; c, the refined PLA, thermoplastic starch and modified nano SiO2 particles are mechanically stirred and pre-dispersed in an ethanol solution according to the proportion of 20: 79: 1; d, putting the mixture pre-dispersed in the step C into a fuming cupboard for pumping, and then drying in a drying oven to obtain a mixed material; e, the mixed material obtained in the step D and a certain amount of dispersing agent are processed and granulated through double screws, a modified plate is prepared through a vulcanization forming machine, then the modified plate is placed in a limited foaming mold, the mold is placed in a high-pressure foaming reaction kettle to be subjected |
format | Patent |
fullrecord | <record><control><sourceid>epo_EVB</sourceid><recordid>TN_cdi_epo_espacenet_CN115926260A</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><sourcerecordid>CN115926260A</sourcerecordid><originalsourceid>FETCH-epo_espacenet_CN115926260A3</originalsourceid><addsrcrecordid>eNqNyjEKwkAQBdA0FqLeYTxAQCMGLCUoVmJhYRfG3Z_swiSz7E7j7W08gNVr3rJ6PTISZ7aoM02woJ50II8xs-e3gEIcQ10sYx4tkBMt8LWDCCWVj7Cz6Ihd9DQoTzSxIUeWdbUYWAo2P1fV9np5drcaSXuUxA4zrO_u-_3x1LRNuzsf_jlfueg6bw</addsrcrecordid><sourcetype>Open Access Repository</sourcetype><iscdi>true</iscdi><recordtype>patent</recordtype></control><display><type>patent</type><title>Preparation method of degradable high-strength closed-cell polylactic acid foam material</title><source>esp@cenet</source><creator>ZHANG LEI ; YANG CHENGUANG ; GUO QINGSHI ; JIANG XIANGYANG ; SUN HUIQING</creator><creatorcontrib>ZHANG LEI ; YANG CHENGUANG ; GUO QINGSHI ; JIANG XIANGYANG ; SUN HUIQING</creatorcontrib><description>The invention provides a preparation method of a degradable high-strength closed-cell polylactic acid foam material, and belongs to the technical field of high polymer materials. Comprising the following steps: A, preparing modified nano SiO2 particles grafted with acrylic acid; b, mechanically crushing the toughening grade PLA resin particles; c, the refined PLA, thermoplastic starch and modified nano SiO2 particles are mechanically stirred and pre-dispersed in an ethanol solution according to the proportion of 20: 79: 1; d, putting the mixture pre-dispersed in the step C into a fuming cupboard for pumping, and then drying in a drying oven to obtain a mixed material; e, the mixed material obtained in the step D and a certain amount of dispersing agent are processed and granulated through double screws, a modified plate is prepared through a vulcanization forming machine, then the modified plate is placed in a limited foaming mold, the mold is placed in a high-pressure foaming reaction kettle to be subjected</description><language>chi ; eng</language><subject>AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F,C08G ; CHEMISTRY ; COMPOSITIONS BASED THEREON ; COMPOSITIONS OF MACROMOLECULAR COMPOUNDS ; GENERAL PROCESSES OF COMPOUNDING ; METALLURGY ; ORGANIC MACROMOLECULAR COMPOUNDS ; THEIR PREPARATION OR CHEMICAL WORKING-UP ; USE OF INORGANIC OR NON-MACROMOLECULAR ORGANIC SUBSTANCES ASCOMPOUNDING INGREDIENTS ; WORKING-UP</subject><creationdate>2023</creationdate><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&date=20230407&DB=EPODOC&CC=CN&NR=115926260A$$EHTML$$P50$$Gepo$$Hfree_for_read</linktohtml><link.rule.ids>230,308,780,885,25564,76547</link.rule.ids><linktorsrc>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&date=20230407&DB=EPODOC&CC=CN&NR=115926260A$$EView_record_in_European_Patent_Office$$FView_record_in_$$GEuropean_Patent_Office$$Hfree_for_read</linktorsrc></links><search><creatorcontrib>ZHANG LEI</creatorcontrib><creatorcontrib>YANG CHENGUANG</creatorcontrib><creatorcontrib>GUO QINGSHI</creatorcontrib><creatorcontrib>JIANG XIANGYANG</creatorcontrib><creatorcontrib>SUN HUIQING</creatorcontrib><title>Preparation method of degradable high-strength closed-cell polylactic acid foam material</title><description>The invention provides a preparation method of a degradable high-strength closed-cell polylactic acid foam material, and belongs to the technical field of high polymer materials. Comprising the following steps: A, preparing modified nano SiO2 particles grafted with acrylic acid; b, mechanically crushing the toughening grade PLA resin particles; c, the refined PLA, thermoplastic starch and modified nano SiO2 particles are mechanically stirred and pre-dispersed in an ethanol solution according to the proportion of 20: 79: 1; d, putting the mixture pre-dispersed in the step C into a fuming cupboard for pumping, and then drying in a drying oven to obtain a mixed material; e, the mixed material obtained in the step D and a certain amount of dispersing agent are processed and granulated through double screws, a modified plate is prepared through a vulcanization forming machine, then the modified plate is placed in a limited foaming mold, the mold is placed in a high-pressure foaming reaction kettle to be subjected</description><subject>AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F,C08G</subject><subject>CHEMISTRY</subject><subject>COMPOSITIONS BASED THEREON</subject><subject>COMPOSITIONS OF MACROMOLECULAR COMPOUNDS</subject><subject>GENERAL PROCESSES OF COMPOUNDING</subject><subject>METALLURGY</subject><subject>ORGANIC MACROMOLECULAR COMPOUNDS</subject><subject>THEIR PREPARATION OR CHEMICAL WORKING-UP</subject><subject>USE OF INORGANIC OR NON-MACROMOLECULAR ORGANIC SUBSTANCES ASCOMPOUNDING INGREDIENTS</subject><subject>WORKING-UP</subject><fulltext>true</fulltext><rsrctype>patent</rsrctype><creationdate>2023</creationdate><recordtype>patent</recordtype><sourceid>EVB</sourceid><recordid>eNqNyjEKwkAQBdA0FqLeYTxAQCMGLCUoVmJhYRfG3Z_swiSz7E7j7W08gNVr3rJ6PTISZ7aoM02woJ50II8xs-e3gEIcQ10sYx4tkBMt8LWDCCWVj7Cz6Ihd9DQoTzSxIUeWdbUYWAo2P1fV9np5drcaSXuUxA4zrO_u-_3x1LRNuzsf_jlfueg6bw</recordid><startdate>20230407</startdate><enddate>20230407</enddate><creator>ZHANG LEI</creator><creator>YANG CHENGUANG</creator><creator>GUO QINGSHI</creator><creator>JIANG XIANGYANG</creator><creator>SUN HUIQING</creator><scope>EVB</scope></search><sort><creationdate>20230407</creationdate><title>Preparation method of degradable high-strength closed-cell polylactic acid foam material</title><author>ZHANG LEI ; YANG CHENGUANG ; GUO QINGSHI ; JIANG XIANGYANG ; SUN HUIQING</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-epo_espacenet_CN115926260A3</frbrgroupid><rsrctype>patents</rsrctype><prefilter>patents</prefilter><language>chi ; eng</language><creationdate>2023</creationdate><topic>AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F,C08G</topic><topic>CHEMISTRY</topic><topic>COMPOSITIONS BASED THEREON</topic><topic>COMPOSITIONS OF MACROMOLECULAR COMPOUNDS</topic><topic>GENERAL PROCESSES OF COMPOUNDING</topic><topic>METALLURGY</topic><topic>ORGANIC MACROMOLECULAR COMPOUNDS</topic><topic>THEIR PREPARATION OR CHEMICAL WORKING-UP</topic><topic>USE OF INORGANIC OR NON-MACROMOLECULAR ORGANIC SUBSTANCES ASCOMPOUNDING INGREDIENTS</topic><topic>WORKING-UP</topic><toplevel>online_resources</toplevel><creatorcontrib>ZHANG LEI</creatorcontrib><creatorcontrib>YANG CHENGUANG</creatorcontrib><creatorcontrib>GUO QINGSHI</creatorcontrib><creatorcontrib>JIANG XIANGYANG</creatorcontrib><creatorcontrib>SUN HUIQING</creatorcontrib><collection>esp@cenet</collection></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext_linktorsrc</fulltext></delivery><addata><au>ZHANG LEI</au><au>YANG CHENGUANG</au><au>GUO QINGSHI</au><au>JIANG XIANGYANG</au><au>SUN HUIQING</au><format>patent</format><genre>patent</genre><ristype>GEN</ristype><title>Preparation method of degradable high-strength closed-cell polylactic acid foam material</title><date>2023-04-07</date><risdate>2023</risdate><abstract>The invention provides a preparation method of a degradable high-strength closed-cell polylactic acid foam material, and belongs to the technical field of high polymer materials. Comprising the following steps: A, preparing modified nano SiO2 particles grafted with acrylic acid; b, mechanically crushing the toughening grade PLA resin particles; c, the refined PLA, thermoplastic starch and modified nano SiO2 particles are mechanically stirred and pre-dispersed in an ethanol solution according to the proportion of 20: 79: 1; d, putting the mixture pre-dispersed in the step C into a fuming cupboard for pumping, and then drying in a drying oven to obtain a mixed material; e, the mixed material obtained in the step D and a certain amount of dispersing agent are processed and granulated through double screws, a modified plate is prepared through a vulcanization forming machine, then the modified plate is placed in a limited foaming mold, the mold is placed in a high-pressure foaming reaction kettle to be subjected</abstract><oa>free_for_read</oa></addata></record> |
fulltext | fulltext_linktorsrc |
identifier | |
ispartof | |
issn | |
language | chi ; eng |
recordid | cdi_epo_espacenet_CN115926260A |
source | esp@cenet |
subjects | AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F,C08G CHEMISTRY COMPOSITIONS BASED THEREON COMPOSITIONS OF MACROMOLECULAR COMPOUNDS GENERAL PROCESSES OF COMPOUNDING METALLURGY ORGANIC MACROMOLECULAR COMPOUNDS THEIR PREPARATION OR CHEMICAL WORKING-UP USE OF INORGANIC OR NON-MACROMOLECULAR ORGANIC SUBSTANCES ASCOMPOUNDING INGREDIENTS WORKING-UP |
title | Preparation method of degradable high-strength closed-cell polylactic acid foam material |
url | https://sfx.bib-bvb.de/sfx_tum?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2025-01-07T01%3A19%3A41IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-epo_EVB&rft_val_fmt=info:ofi/fmt:kev:mtx:patent&rft.genre=patent&rft.au=ZHANG%20LEI&rft.date=2023-04-07&rft_id=info:doi/&rft_dat=%3Cepo_EVB%3ECN115926260A%3C/epo_EVB%3E%3Curl%3E%3C/url%3E&disable_directlink=true&sfx.directlink=off&sfx.report_link=0&rft_id=info:oai/&rft_id=info:pmid/&rfr_iscdi=true |