Fingerprint spectrum detection method for Jianshou capsules, control fingerprint spectrum and application
The invention relates to a finger-print detection method of a Fulonan capsule, a control finger-print and application. According to the method, an ultra-high performance liquid chromatograph equipped with a diode array detector is adopted for detection, and the chromatographic conditions are as foll...
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| creator | CHE LI LIN YU GUAN BIN YOU TIANNI YANG LIHUA XU WEI LIAO GENJIE |
| description | The invention relates to a finger-print detection method of a Fulonan capsule, a control finger-print and application. According to the method, an ultra-high performance liquid chromatograph equipped with a diode array detector is adopted for detection, and the chromatographic conditions are as follows: the chromatographic column is Welch Ultimate UPLC AQ-C18, 2.1 mm * 150 mm, 1.8 [mu] m, or Welch Ultimate UPLC XB-C18, 2.1 mm * 150 mm, 1.8 [mu] m, and the column temperature is 25-35 DEG C; the flow velocity is 0.25 mL/min to 0.35 mL/min; the detection wavelength is 254 nm; the sample size is 1-3 [mu] L; a mobile phase is methanol (A)-0.1% formic acid aqueous solution (B); and gradient elution. The obtained control fingerprint spectrum of the Fulonan capsules can be used for quality control of the Fulonan capsules.
本发明涉及福寿胶囊指纹图谱检测方法、对照指纹图谱和应用。所述方法采用配备有二极管阵列检测器的超高效液相色谱仪进行检测，色谱条件如下：色谱柱为Welch Ultimate UPLC AQ-C18，2.1mm×150mm，1.8μm，或Welch Ultimate UPLC XB-C18，2.1mm×150mm，1.8μm，柱温25℃-35℃；流速0.25mL/min～0.35mL/min；检测波 |
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本发明涉及福寿胶囊指纹图谱检测方法、对照指纹图谱和应用。所述方法采用配备有二极管阵列检测器的超高效液相色谱仪进行检测，色谱条件如下：色谱柱为Welch Ultimate UPLC AQ-C18，2.1mm×150mm，1.8μm，或Welch Ultimate UPLC XB-C18，2.1mm×150mm，1.8μm，柱温25℃-35℃；流速0.25mL/min～0.35mL/min；检测波</description><language>chi ; eng</language><subject>INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIRCHEMICAL OR PHYSICAL PROPERTIES ; MEASURING ; PHYSICS ; TESTING</subject><creationdate>2023</creationdate><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&date=20230203&DB=EPODOC&CC=CN&NR=115684427A$$EHTML$$P50$$Gepo$$Hfree_for_read</linktohtml><link.rule.ids>230,308,780,885,25564,76547</link.rule.ids><linktorsrc>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&date=20230203&DB=EPODOC&CC=CN&NR=115684427A$$EView_record_in_European_Patent_Office$$FView_record_in_$$GEuropean_Patent_Office$$Hfree_for_read</linktorsrc></links><search><creatorcontrib>CHE LI</creatorcontrib><creatorcontrib>LIN YU</creatorcontrib><creatorcontrib>GUAN BIN</creatorcontrib><creatorcontrib>YOU TIANNI</creatorcontrib><creatorcontrib>YANG LIHUA</creatorcontrib><creatorcontrib>XU WEI</creatorcontrib><creatorcontrib>LIAO GENJIE</creatorcontrib><title>Fingerprint spectrum detection method for Jianshou capsules, control fingerprint spectrum and application</title><description>The invention relates to a finger-print detection method of a Fulonan capsule, a control finger-print and application. According to the method, an ultra-high performance liquid chromatograph equipped with a diode array detector is adopted for detection, and the chromatographic conditions are as follows: the chromatographic column is Welch Ultimate UPLC AQ-C18, 2.1 mm * 150 mm, 1.8 [mu] m, or Welch Ultimate UPLC XB-C18, 2.1 mm * 150 mm, 1.8 [mu] m, and the column temperature is 25-35 DEG C; the flow velocity is 0.25 mL/min to 0.35 mL/min; the detection wavelength is 254 nm; the sample size is 1-3 [mu] L; a mobile phase is methanol (A)-0.1% formic acid aqueous solution (B); and gradient elution. The obtained control fingerprint spectrum of the Fulonan capsules can be used for quality control of the Fulonan capsules.
本发明涉及福寿胶囊指纹图谱检测方法、对照指纹图谱和应用。所述方法采用配备有二极管阵列检测器的超高效液相色谱仪进行检测，色谱条件如下：色谱柱为Welch Ultimate UPLC AQ-C18，2.1mm×150mm，1.8μm，或Welch Ultimate UPLC XB-C18，2.1mm×150mm，1.8μm，柱温25℃-35℃；流速0.25mL/min～0.35mL/min；检测波</description><subject>INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIRCHEMICAL OR PHYSICAL PROPERTIES</subject><subject>MEASURING</subject><subject>PHYSICS</subject><subject>TESTING</subject><fulltext>true</fulltext><rsrctype>patent</rsrctype><creationdate>2023</creationdate><recordtype>patent</recordtype><sourceid>EVB</sourceid><recordid>eNqNjLsKwkAQAK-xEPUf1l6LaHy0EgxiYWUflstecnDZXe7x_ypYWljNFMPMjW89DxQ1es6QlGyOZYKe8tu8MEyUR-nBSYS7R06jFLCoqQRKG7DCOUoA92uC3AOqBm_xs1qamcOQaPXlwqzb67O5bUmlo6RoiSl3zaOqDsdzXe9Ol_0_zQvzDEHu</recordid><startdate>20230203</startdate><enddate>20230203</enddate><creator>CHE LI</creator><creator>LIN YU</creator><creator>GUAN BIN</creator><creator>YOU TIANNI</creator><creator>YANG LIHUA</creator><creator>XU WEI</creator><creator>LIAO GENJIE</creator><scope>EVB</scope></search><sort><creationdate>20230203</creationdate><title>Fingerprint spectrum detection method for Jianshou capsules, control fingerprint spectrum and application</title><author>CHE LI ; LIN YU ; GUAN BIN ; YOU TIANNI ; YANG LIHUA ; XU WEI ; LIAO GENJIE</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-epo_espacenet_CN115684427A3</frbrgroupid><rsrctype>patents</rsrctype><prefilter>patents</prefilter><language>chi ; eng</language><creationdate>2023</creationdate><topic>INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIRCHEMICAL OR PHYSICAL PROPERTIES</topic><topic>MEASURING</topic><topic>PHYSICS</topic><topic>TESTING</topic><toplevel>online_resources</toplevel><creatorcontrib>CHE LI</creatorcontrib><creatorcontrib>LIN YU</creatorcontrib><creatorcontrib>GUAN BIN</creatorcontrib><creatorcontrib>YOU TIANNI</creatorcontrib><creatorcontrib>YANG LIHUA</creatorcontrib><creatorcontrib>XU WEI</creatorcontrib><creatorcontrib>LIAO GENJIE</creatorcontrib><collection>esp@cenet</collection></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext_linktorsrc</fulltext></delivery><addata><au>CHE LI</au><au>LIN YU</au><au>GUAN BIN</au><au>YOU TIANNI</au><au>YANG LIHUA</au><au>XU WEI</au><au>LIAO GENJIE</au><format>patent</format><genre>patent</genre><ristype>GEN</ristype><title>Fingerprint spectrum detection method for Jianshou capsules, control fingerprint spectrum and application</title><date>2023-02-03</date><risdate>2023</risdate><abstract>The invention relates to a finger-print detection method of a Fulonan capsule, a control finger-print and application. According to the method, an ultra-high performance liquid chromatograph equipped with a diode array detector is adopted for detection, and the chromatographic conditions are as follows: the chromatographic column is Welch Ultimate UPLC AQ-C18, 2.1 mm * 150 mm, 1.8 [mu] m, or Welch Ultimate UPLC XB-C18, 2.1 mm * 150 mm, 1.8 [mu] m, and the column temperature is 25-35 DEG C; the flow velocity is 0.25 mL/min to 0.35 mL/min; the detection wavelength is 254 nm; the sample size is 1-3 [mu] L; a mobile phase is methanol (A)-0.1% formic acid aqueous solution (B); and gradient elution. The obtained control fingerprint spectrum of the Fulonan capsules can be used for quality control of the Fulonan capsules.
本发明涉及福寿胶囊指纹图谱检测方法、对照指纹图谱和应用。所述方法采用配备有二极管阵列检测器的超高效液相色谱仪进行检测，色谱条件如下：色谱柱为Welch Ultimate UPLC AQ-C18，2.1mm×150mm，1.8μm，或Welch Ultimate UPLC XB-C18，2.1mm×150mm，1.8μm，柱温25℃-35℃；流速0.25mL/min～0.35mL/min；检测波</abstract><oa>free_for_read</oa></addata></record> |
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| title | Fingerprint spectrum detection method for Jianshou capsules, control fingerprint spectrum and application |
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