MoSi2-coated Nb core-shell structure material and preparation method thereof

The invention discloses a MoSi2-coated Nb core-shell structure material and a preparation method thereof. The preparation method comprises the following steps: S1, mixing SDS, MoSi2 and water, and mechanically stirring to form a first suspension; s2, CTAB, Nb and water are mixed and mechanically sti...

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Bibliographische Detailangaben
Hauptverfasser: LUO JIAJUN, LIANG BINGLIANG, CHEN WEIHUA, QUAN CIWANG, ZHANG JIANJUN, WANG ZIQIAO
Format: Patent
Sprache:chi ; eng
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Zusammenfassung:The invention discloses a MoSi2-coated Nb core-shell structure material and a preparation method thereof. The preparation method comprises the following steps: S1, mixing SDS, MoSi2 and water, and mechanically stirring to form a first suspension; s2, CTAB, Nb and water are mixed and mechanically stirred into second suspension liquid; s3, mixing the first suspension and the second suspension, and mechanically stirring to obtain a third suspension; s4, carrying out suction filtration, drying and calcining on the third suspension, washing, carrying out suction filtration and drying, mixing the obtained powder with SDS and water, and mechanically stirring to obtain a fourth suspension; s5, carrying out suction filtration, drying and calcining on the fourth suspension, washing, carrying out suction filtration and drying, mixing the obtained powder with CTAB and water, and mechanically stirring to obtain a fifth suspension; and S6, drying the fifth suspension, calcining, washing, carrying out suction filtration, dr