Fullerene-loaded non-noble metal electrocatalyst as well as preparation method and application thereof

Fullerene-loaded non-noble metal electrocatalyst as well as preparation method and application thereof

The invention belongs to the technical field of electrochemistry, and particularly relates to a fullerene-loaded non-noble metal electrocatalyst and a preparation method and application thereof.The preparation method comprises the following steps that fullerene and pyrazole are dissolved in an organ...

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Hauptverfasser: CAO LIYUN, HUO XUEMENG, HU YUZHU, HUANG JIANFENG, LUO TIANMI, LIU WANWAN, FENG YONGQIANG, YUAN CHENGKE
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APPARATUS THEREFOR
CHEMISTRY
ELECTROLYTIC OR ELECTROPHORETIC PROCESSES
ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTIONOF COMPOUNDS OR NON-METALS
METALLURGY
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creator CAO LIYUN
HUO XUEMENG
HU YUZHU
HUANG JIANFENG
LUO TIANMI
LIU WANWAN
FENG YONGQIANG
YUAN CHENGKE
description The invention belongs to the technical field of electrochemistry, and particularly relates to a fullerene-loaded non-noble metal electrocatalyst and a preparation method and application thereof.The preparation method comprises the following steps that fullerene and pyrazole are dissolved in an organic solvent, and a solution A is prepared; dissolving non-noble metal chloride in ethanol to prepare a solution B; mixing the solution A and the solution B, carrying out oil bath reaction at 150-200 DEG C in a nitrogen atmosphere and under a stirring condition, and then cooling to room temperature; carrying out rotary evaporation concentration on the reaction system to prepare a precursor; and carrying out staged heating heat treatment on the precursor in an inert gas atmosphere. The precursor is prepared by adopting an oil bath-condensation reflux method, a container is uniformly heated in a controllable range, and meanwhile, the loss of reactants is avoided; the metal can promote the stability of fullerene in the
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subjects APPARATUS THEREFOR
CHEMISTRY
ELECTROLYTIC OR ELECTROPHORETIC PROCESSES
ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTIONOF COMPOUNDS OR NON-METALS
METALLURGY
title Fullerene-loaded non-noble metal electrocatalyst as well as preparation method and application thereof
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