Quality control method of climacteric tablet
The invention relates to drug detection, in particular to a high performance liquid chromatography fingerprint spectrum of climacteric tablet and establishment of the fingerprint spectrum. According to the detection method, 2, 3, 5, 4 '-tetrahydroxystilbene-2-O-beta-D-glucoside is adopted as a...
Gespeichert in:
| Hauptverfasser: | , , , |
|---|---|
| Format: | Patent |
| Sprache: | chi ; eng |
| Schlagworte: | |
| Online-Zugang: | Volltext bestellen |
| Tags: |
Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
|
| container_end_page | |
|---|---|
| container_issue | |
| container_start_page | |
| container_title | |
| container_volume | |
| creator | LI YUNLI CAO JIANJUN XUE HUANGE LIANG YAFEN |
| description | The invention relates to drug detection, in particular to a high performance liquid chromatography fingerprint spectrum of climacteric tablet and establishment of the fingerprint spectrum. According to the detection method, 2, 3, 5, 4 '-tetrahydroxystilbene-2-O-beta-D-glucoside is adopted as a reference substance, high performance liquid chromatography is carried out, and the chromatographic conditions are as follows: octadecylsilane chemically bonded silica is used as a filler; the detection wavelength is 260 to 296 nm; methanol is used as a mobile phase A, a 0.1% phosphoric acid solution is used as a mobile phase B, gradient elution is carried out, the flow velocity is 0.8-1.2 ml/min, and the column temperature is 20-30 DEG C. According to the method, the stability, the consistency and the controllability of the quality of the traditional Chinese medicine tablets can be ensured, so that the safety and the effectiveness of the medicine are ensured.
本发明涉及药品检测，具体地涉及更年安片的高效液相色谱指纹图谱及指纹图谱的建立。本发明的检测方法采用的参照品为2,3,5, |
| format | Patent |
| fullrecord | <record><control><sourceid>epo_EVB</sourceid><recordid>TN_cdi_epo_espacenet_CN114965802A</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><sourcerecordid>CN114965802A</sourcerecordid><originalsourceid>FETCH-epo_espacenet_CN114965802A3</originalsourceid><addsrcrecordid>eNrjZNAJLE3MySypVEjOzyspys9RyE0tychPUchPU0jOycxNTC5JLcpMVihJTMpJLeFhYE1LzClO5YXS3AyKbq4hzh66qQX58anFBYnJqXmpJfHOfoaGJpZmphYGRo7GxKgBAKg_Kfc</addsrcrecordid><sourcetype>Open Access Repository</sourcetype><iscdi>true</iscdi><recordtype>patent</recordtype></control><display><type>patent</type><title>Quality control method of climacteric tablet</title><source>esp@cenet</source><creator>LI YUNLI ; CAO JIANJUN ; XUE HUANGE ; LIANG YAFEN</creator><creatorcontrib>LI YUNLI ; CAO JIANJUN ; XUE HUANGE ; LIANG YAFEN</creatorcontrib><description>The invention relates to drug detection, in particular to a high performance liquid chromatography fingerprint spectrum of climacteric tablet and establishment of the fingerprint spectrum. According to the detection method, 2, 3, 5, 4 '-tetrahydroxystilbene-2-O-beta-D-glucoside is adopted as a reference substance, high performance liquid chromatography is carried out, and the chromatographic conditions are as follows: octadecylsilane chemically bonded silica is used as a filler; the detection wavelength is 260 to 296 nm; methanol is used as a mobile phase A, a 0.1% phosphoric acid solution is used as a mobile phase B, gradient elution is carried out, the flow velocity is 0.8-1.2 ml/min, and the column temperature is 20-30 DEG C. According to the method, the stability, the consistency and the controllability of the quality of the traditional Chinese medicine tablets can be ensured, so that the safety and the effectiveness of the medicine are ensured.
本发明涉及药品检测，具体地涉及更年安片的高效液相色谱指纹图谱及指纹图谱的建立。本发明的检测方法采用的参照品为2,3,5,</description><language>chi ; eng</language><subject>INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIRCHEMICAL OR PHYSICAL PROPERTIES ; MEASURING ; PHYSICS ; TESTING</subject><creationdate>2022</creationdate><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&date=20220830&DB=EPODOC&CC=CN&NR=114965802A$$EHTML$$P50$$Gepo$$Hfree_for_read</linktohtml><link.rule.ids>230,308,776,881,25543,76293</link.rule.ids><linktorsrc>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&date=20220830&DB=EPODOC&CC=CN&NR=114965802A$$EView_record_in_European_Patent_Office$$FView_record_in_$$GEuropean_Patent_Office$$Hfree_for_read</linktorsrc></links><search><creatorcontrib>LI YUNLI</creatorcontrib><creatorcontrib>CAO JIANJUN</creatorcontrib><creatorcontrib>XUE HUANGE</creatorcontrib><creatorcontrib>LIANG YAFEN</creatorcontrib><title>Quality control method of climacteric tablet</title><description>The invention relates to drug detection, in particular to a high performance liquid chromatography fingerprint spectrum of climacteric tablet and establishment of the fingerprint spectrum. According to the detection method, 2, 3, 5, 4 '-tetrahydroxystilbene-2-O-beta-D-glucoside is adopted as a reference substance, high performance liquid chromatography is carried out, and the chromatographic conditions are as follows: octadecylsilane chemically bonded silica is used as a filler; the detection wavelength is 260 to 296 nm; methanol is used as a mobile phase A, a 0.1% phosphoric acid solution is used as a mobile phase B, gradient elution is carried out, the flow velocity is 0.8-1.2 ml/min, and the column temperature is 20-30 DEG C. According to the method, the stability, the consistency and the controllability of the quality of the traditional Chinese medicine tablets can be ensured, so that the safety and the effectiveness of the medicine are ensured.
本发明涉及药品检测，具体地涉及更年安片的高效液相色谱指纹图谱及指纹图谱的建立。本发明的检测方法采用的参照品为2,3,5,</description><subject>INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIRCHEMICAL OR PHYSICAL PROPERTIES</subject><subject>MEASURING</subject><subject>PHYSICS</subject><subject>TESTING</subject><fulltext>true</fulltext><rsrctype>patent</rsrctype><creationdate>2022</creationdate><recordtype>patent</recordtype><sourceid>EVB</sourceid><recordid>eNrjZNAJLE3MySypVEjOzyspys9RyE0tychPUchPU0jOycxNTC5JLcpMVihJTMpJLeFhYE1LzClO5YXS3AyKbq4hzh66qQX58anFBYnJqXmpJfHOfoaGJpZmphYGRo7GxKgBAKg_Kfc</recordid><startdate>20220830</startdate><enddate>20220830</enddate><creator>LI YUNLI</creator><creator>CAO JIANJUN</creator><creator>XUE HUANGE</creator><creator>LIANG YAFEN</creator><scope>EVB</scope></search><sort><creationdate>20220830</creationdate><title>Quality control method of climacteric tablet</title><author>LI YUNLI ; CAO JIANJUN ; XUE HUANGE ; LIANG YAFEN</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-epo_espacenet_CN114965802A3</frbrgroupid><rsrctype>patents</rsrctype><prefilter>patents</prefilter><language>chi ; eng</language><creationdate>2022</creationdate><topic>INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIRCHEMICAL OR PHYSICAL PROPERTIES</topic><topic>MEASURING</topic><topic>PHYSICS</topic><topic>TESTING</topic><toplevel>online_resources</toplevel><creatorcontrib>LI YUNLI</creatorcontrib><creatorcontrib>CAO JIANJUN</creatorcontrib><creatorcontrib>XUE HUANGE</creatorcontrib><creatorcontrib>LIANG YAFEN</creatorcontrib><collection>esp@cenet</collection></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext_linktorsrc</fulltext></delivery><addata><au>LI YUNLI</au><au>CAO JIANJUN</au><au>XUE HUANGE</au><au>LIANG YAFEN</au><format>patent</format><genre>patent</genre><ristype>GEN</ristype><title>Quality control method of climacteric tablet</title><date>2022-08-30</date><risdate>2022</risdate><abstract>The invention relates to drug detection, in particular to a high performance liquid chromatography fingerprint spectrum of climacteric tablet and establishment of the fingerprint spectrum. According to the detection method, 2, 3, 5, 4 '-tetrahydroxystilbene-2-O-beta-D-glucoside is adopted as a reference substance, high performance liquid chromatography is carried out, and the chromatographic conditions are as follows: octadecylsilane chemically bonded silica is used as a filler; the detection wavelength is 260 to 296 nm; methanol is used as a mobile phase A, a 0.1% phosphoric acid solution is used as a mobile phase B, gradient elution is carried out, the flow velocity is 0.8-1.2 ml/min, and the column temperature is 20-30 DEG C. According to the method, the stability, the consistency and the controllability of the quality of the traditional Chinese medicine tablets can be ensured, so that the safety and the effectiveness of the medicine are ensured.
本发明涉及药品检测，具体地涉及更年安片的高效液相色谱指纹图谱及指纹图谱的建立。本发明的检测方法采用的参照品为2,3,5,</abstract><oa>free_for_read</oa></addata></record> |
| fulltext | fulltext_linktorsrc |
| identifier | |
| ispartof | |
| issn | |
| language | chi ; eng |
| recordid | cdi_epo_espacenet_CN114965802A |
| source | esp@cenet |
| subjects | INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIRCHEMICAL OR PHYSICAL PROPERTIES MEASURING PHYSICS TESTING |
| title | Quality control method of climacteric tablet |
| url | https://sfx.bib-bvb.de/sfx_tum?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2025-01-24T02%3A06%3A24IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-epo_EVB&rft_val_fmt=info:ofi/fmt:kev:mtx:patent&rft.genre=patent&rft.au=LI%20YUNLI&rft.date=2022-08-30&rft_id=info:doi/&rft_dat=%3Cepo_EVB%3ECN114965802A%3C/epo_EVB%3E%3Curl%3E%3C/url%3E&disable_directlink=true&sfx.directlink=off&sfx.report_link=0&rft_id=info:oai/&rft_id=info:pmid/&rfr_iscdi=true |