Method and production line for continuously synthesizing isoproturon by static mixer

The invention relates to a method for continuously synthesizing isoproturon by using a static mixer and a production line thereof, the method comprises the following steps: preparing a p-isopropylaniline solution, pumping the p-isopropylaniline solution into the static mixer, introducing phosgene, g...

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Hauptverfasser: SHI LIQIANG, CHEN HUA, HE XIAOJIE, WANG WEIHUA, CAI YONGFENG, LIU JIANJUN, QIAN MAOGONG, TIAN QINGHAI
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creator SHI LIQIANG
CHEN HUA
HE XIAOJIE
WANG WEIHUA
CAI YONGFENG
LIU JIANJUN
QIAN MAOGONG
TIAN QINGHAI
description The invention relates to a method for continuously synthesizing isoproturon by using a static mixer and a production line thereof, the method comprises the following steps: preparing a p-isopropylaniline solution, pumping the p-isopropylaniline solution into the static mixer, introducing phosgene, generating p-isopropylaniline, feeding the p-isopropylaniline solution into a thermal decomposition tower, overflowing feed liquid reaction liquid into a phosgene driving tower through a U-shaped balance pipe at the bottom, and additionally arranging an online analyzer on the U-shaped balance pipe, enabling the p-isopropyl phenyl isocyanate toluene solution qualified in light driving to pass through a static mixer, enabling synthesized isoproturon feed liquid to enter a continuous crystallization kettle, and separating and drying to obtain the isoproturon with the purity of 98.5% or above. The method provided by the invention realizes whole-course continuous generation of isoproturon, reduces the byproduct hydrochlo
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subjects ACYCLIC OR CARBOCYCLIC COMPOUNDS
AGRICULTURE
ANIMAL HUSBANDRY
CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOIDCHEMISTRY
CHEMISTRY
FISHING
FORESTRY
HUMAN NECESSITIES
HUNTING
METALLURGY
MIXING, e.g. DISSOLVING, EMULSIFYING, DISPERSING
ORGANIC CHEMISTRY
PERFORMING OPERATIONS
PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
THEIR RELEVANT APPARATUS
TRANSPORTING
TRAPPING
title Method and production line for continuously synthesizing isoproturon by static mixer
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