Method and production line for continuously synthesizing isoproturon by static mixer
The invention relates to a method for continuously synthesizing isoproturon by using a static mixer and a production line thereof, the method comprises the following steps: preparing a p-isopropylaniline solution, pumping the p-isopropylaniline solution into the static mixer, introducing phosgene, g...
Gespeichert in:
Hauptverfasser: | , , , , , , , |
---|---|
Format: | Patent |
Sprache: | chi ; eng |
Schlagworte: | |
Online-Zugang: | Volltext bestellen |
Tags: |
Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
|
container_end_page | |
---|---|
container_issue | |
container_start_page | |
container_title | |
container_volume | |
creator | SHI LIQIANG CHEN HUA HE XIAOJIE WANG WEIHUA CAI YONGFENG LIU JIANJUN QIAN MAOGONG TIAN QINGHAI |
description | The invention relates to a method for continuously synthesizing isoproturon by using a static mixer and a production line thereof, the method comprises the following steps: preparing a p-isopropylaniline solution, pumping the p-isopropylaniline solution into the static mixer, introducing phosgene, generating p-isopropylaniline, feeding the p-isopropylaniline solution into a thermal decomposition tower, overflowing feed liquid reaction liquid into a phosgene driving tower through a U-shaped balance pipe at the bottom, and additionally arranging an online analyzer on the U-shaped balance pipe, enabling the p-isopropyl phenyl isocyanate toluene solution qualified in light driving to pass through a static mixer, enabling synthesized isoproturon feed liquid to enter a continuous crystallization kettle, and separating and drying to obtain the isoproturon with the purity of 98.5% or above. The method provided by the invention realizes whole-course continuous generation of isoproturon, reduces the byproduct hydrochlo |
format | Patent |
fullrecord | <record><control><sourceid>epo_EVB</sourceid><recordid>TN_cdi_epo_espacenet_CN114957047A</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><sourcerecordid>CN114957047A</sourcerecordid><originalsourceid>FETCH-epo_espacenet_CN114957047A3</originalsourceid><addsrcrecordid>eNqNizEKwkAQAK-xEPUP6wMEg5FgKUGx0Sp9OO82ycK5G-72wPh6U_gAqylmZmmaO-ogHix7GKP47JSEIRAjdBLBCStxlpzCBGliHTDRh7gHSjIPmuOcP2enVsnBi94Y12bR2ZBw8-PKbK-Xpr7tcJQW02gdMmpbP4qiPB2rfVmdD_80XzB_Ohg</addsrcrecordid><sourcetype>Open Access Repository</sourcetype><iscdi>true</iscdi><recordtype>patent</recordtype></control><display><type>patent</type><title>Method and production line for continuously synthesizing isoproturon by static mixer</title><source>esp@cenet</source><creator>SHI LIQIANG ; CHEN HUA ; HE XIAOJIE ; WANG WEIHUA ; CAI YONGFENG ; LIU JIANJUN ; QIAN MAOGONG ; TIAN QINGHAI</creator><creatorcontrib>SHI LIQIANG ; CHEN HUA ; HE XIAOJIE ; WANG WEIHUA ; CAI YONGFENG ; LIU JIANJUN ; QIAN MAOGONG ; TIAN QINGHAI</creatorcontrib><description>The invention relates to a method for continuously synthesizing isoproturon by using a static mixer and a production line thereof, the method comprises the following steps: preparing a p-isopropylaniline solution, pumping the p-isopropylaniline solution into the static mixer, introducing phosgene, generating p-isopropylaniline, feeding the p-isopropylaniline solution into a thermal decomposition tower, overflowing feed liquid reaction liquid into a phosgene driving tower through a U-shaped balance pipe at the bottom, and additionally arranging an online analyzer on the U-shaped balance pipe, enabling the p-isopropyl phenyl isocyanate toluene solution qualified in light driving to pass through a static mixer, enabling synthesized isoproturon feed liquid to enter a continuous crystallization kettle, and separating and drying to obtain the isoproturon with the purity of 98.5% or above. The method provided by the invention realizes whole-course continuous generation of isoproturon, reduces the byproduct hydrochlo</description><language>chi ; eng</language><subject>ACYCLIC OR CARBOCYCLIC COMPOUNDS ; AGRICULTURE ; ANIMAL HUSBANDRY ; CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOIDCHEMISTRY ; CHEMISTRY ; FISHING ; FORESTRY ; HUMAN NECESSITIES ; HUNTING ; METALLURGY ; MIXING, e.g. DISSOLVING, EMULSIFYING, DISPERSING ; ORGANIC CHEMISTRY ; PERFORMING OPERATIONS ; PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL ; THEIR RELEVANT APPARATUS ; TRANSPORTING ; TRAPPING</subject><creationdate>2022</creationdate><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&date=20220830&DB=EPODOC&CC=CN&NR=114957047A$$EHTML$$P50$$Gepo$$Hfree_for_read</linktohtml><link.rule.ids>230,308,780,885,25563,76418</link.rule.ids><linktorsrc>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&date=20220830&DB=EPODOC&CC=CN&NR=114957047A$$EView_record_in_European_Patent_Office$$FView_record_in_$$GEuropean_Patent_Office$$Hfree_for_read</linktorsrc></links><search><creatorcontrib>SHI LIQIANG</creatorcontrib><creatorcontrib>CHEN HUA</creatorcontrib><creatorcontrib>HE XIAOJIE</creatorcontrib><creatorcontrib>WANG WEIHUA</creatorcontrib><creatorcontrib>CAI YONGFENG</creatorcontrib><creatorcontrib>LIU JIANJUN</creatorcontrib><creatorcontrib>QIAN MAOGONG</creatorcontrib><creatorcontrib>TIAN QINGHAI</creatorcontrib><title>Method and production line for continuously synthesizing isoproturon by static mixer</title><description>The invention relates to a method for continuously synthesizing isoproturon by using a static mixer and a production line thereof, the method comprises the following steps: preparing a p-isopropylaniline solution, pumping the p-isopropylaniline solution into the static mixer, introducing phosgene, generating p-isopropylaniline, feeding the p-isopropylaniline solution into a thermal decomposition tower, overflowing feed liquid reaction liquid into a phosgene driving tower through a U-shaped balance pipe at the bottom, and additionally arranging an online analyzer on the U-shaped balance pipe, enabling the p-isopropyl phenyl isocyanate toluene solution qualified in light driving to pass through a static mixer, enabling synthesized isoproturon feed liquid to enter a continuous crystallization kettle, and separating and drying to obtain the isoproturon with the purity of 98.5% or above. The method provided by the invention realizes whole-course continuous generation of isoproturon, reduces the byproduct hydrochlo</description><subject>ACYCLIC OR CARBOCYCLIC COMPOUNDS</subject><subject>AGRICULTURE</subject><subject>ANIMAL HUSBANDRY</subject><subject>CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOIDCHEMISTRY</subject><subject>CHEMISTRY</subject><subject>FISHING</subject><subject>FORESTRY</subject><subject>HUMAN NECESSITIES</subject><subject>HUNTING</subject><subject>METALLURGY</subject><subject>MIXING, e.g. DISSOLVING, EMULSIFYING, DISPERSING</subject><subject>ORGANIC CHEMISTRY</subject><subject>PERFORMING OPERATIONS</subject><subject>PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL</subject><subject>THEIR RELEVANT APPARATUS</subject><subject>TRANSPORTING</subject><subject>TRAPPING</subject><fulltext>true</fulltext><rsrctype>patent</rsrctype><creationdate>2022</creationdate><recordtype>patent</recordtype><sourceid>EVB</sourceid><recordid>eNqNizEKwkAQAK-xEPUP6wMEg5FgKUGx0Sp9OO82ycK5G-72wPh6U_gAqylmZmmaO-ogHix7GKP47JSEIRAjdBLBCStxlpzCBGliHTDRh7gHSjIPmuOcP2enVsnBi94Y12bR2ZBw8-PKbK-Xpr7tcJQW02gdMmpbP4qiPB2rfVmdD_80XzB_Ohg</recordid><startdate>20220830</startdate><enddate>20220830</enddate><creator>SHI LIQIANG</creator><creator>CHEN HUA</creator><creator>HE XIAOJIE</creator><creator>WANG WEIHUA</creator><creator>CAI YONGFENG</creator><creator>LIU JIANJUN</creator><creator>QIAN MAOGONG</creator><creator>TIAN QINGHAI</creator><scope>EVB</scope></search><sort><creationdate>20220830</creationdate><title>Method and production line for continuously synthesizing isoproturon by static mixer</title><author>SHI LIQIANG ; CHEN HUA ; HE XIAOJIE ; WANG WEIHUA ; CAI YONGFENG ; LIU JIANJUN ; QIAN MAOGONG ; TIAN QINGHAI</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-epo_espacenet_CN114957047A3</frbrgroupid><rsrctype>patents</rsrctype><prefilter>patents</prefilter><language>chi ; eng</language><creationdate>2022</creationdate><topic>ACYCLIC OR CARBOCYCLIC COMPOUNDS</topic><topic>AGRICULTURE</topic><topic>ANIMAL HUSBANDRY</topic><topic>CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOIDCHEMISTRY</topic><topic>CHEMISTRY</topic><topic>FISHING</topic><topic>FORESTRY</topic><topic>HUMAN NECESSITIES</topic><topic>HUNTING</topic><topic>METALLURGY</topic><topic>MIXING, e.g. DISSOLVING, EMULSIFYING, DISPERSING</topic><topic>ORGANIC CHEMISTRY</topic><topic>PERFORMING OPERATIONS</topic><topic>PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL</topic><topic>THEIR RELEVANT APPARATUS</topic><topic>TRANSPORTING</topic><topic>TRAPPING</topic><toplevel>online_resources</toplevel><creatorcontrib>SHI LIQIANG</creatorcontrib><creatorcontrib>CHEN HUA</creatorcontrib><creatorcontrib>HE XIAOJIE</creatorcontrib><creatorcontrib>WANG WEIHUA</creatorcontrib><creatorcontrib>CAI YONGFENG</creatorcontrib><creatorcontrib>LIU JIANJUN</creatorcontrib><creatorcontrib>QIAN MAOGONG</creatorcontrib><creatorcontrib>TIAN QINGHAI</creatorcontrib><collection>esp@cenet</collection></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext_linktorsrc</fulltext></delivery><addata><au>SHI LIQIANG</au><au>CHEN HUA</au><au>HE XIAOJIE</au><au>WANG WEIHUA</au><au>CAI YONGFENG</au><au>LIU JIANJUN</au><au>QIAN MAOGONG</au><au>TIAN QINGHAI</au><format>patent</format><genre>patent</genre><ristype>GEN</ristype><title>Method and production line for continuously synthesizing isoproturon by static mixer</title><date>2022-08-30</date><risdate>2022</risdate><abstract>The invention relates to a method for continuously synthesizing isoproturon by using a static mixer and a production line thereof, the method comprises the following steps: preparing a p-isopropylaniline solution, pumping the p-isopropylaniline solution into the static mixer, introducing phosgene, generating p-isopropylaniline, feeding the p-isopropylaniline solution into a thermal decomposition tower, overflowing feed liquid reaction liquid into a phosgene driving tower through a U-shaped balance pipe at the bottom, and additionally arranging an online analyzer on the U-shaped balance pipe, enabling the p-isopropyl phenyl isocyanate toluene solution qualified in light driving to pass through a static mixer, enabling synthesized isoproturon feed liquid to enter a continuous crystallization kettle, and separating and drying to obtain the isoproturon with the purity of 98.5% or above. The method provided by the invention realizes whole-course continuous generation of isoproturon, reduces the byproduct hydrochlo</abstract><oa>free_for_read</oa></addata></record> |
fulltext | fulltext_linktorsrc |
identifier | |
ispartof | |
issn | |
language | chi ; eng |
recordid | cdi_epo_espacenet_CN114957047A |
source | esp@cenet |
subjects | ACYCLIC OR CARBOCYCLIC COMPOUNDS AGRICULTURE ANIMAL HUSBANDRY CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOIDCHEMISTRY CHEMISTRY FISHING FORESTRY HUMAN NECESSITIES HUNTING METALLURGY MIXING, e.g. DISSOLVING, EMULSIFYING, DISPERSING ORGANIC CHEMISTRY PERFORMING OPERATIONS PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL THEIR RELEVANT APPARATUS TRANSPORTING TRAPPING |
title | Method and production line for continuously synthesizing isoproturon by static mixer |
url | https://sfx.bib-bvb.de/sfx_tum?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2025-01-09T08%3A25%3A19IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-epo_EVB&rft_val_fmt=info:ofi/fmt:kev:mtx:patent&rft.genre=patent&rft.au=SHI%20LIQIANG&rft.date=2022-08-30&rft_id=info:doi/&rft_dat=%3Cepo_EVB%3ECN114957047A%3C/epo_EVB%3E%3Curl%3E%3C/url%3E&disable_directlink=true&sfx.directlink=off&sfx.report_link=0&rft_id=info:oai/&rft_id=info:pmid/&rfr_iscdi=true |