Method for preparing high-performance cementing material through negative-pressure anaerobic thermal cracking of phosphogypsum

The invention discloses a method for preparing a high-performance cementing material by negative-pressure anaerobic thermal cracking of ardealite, which comprises the following steps: adding water into ardealite, fully stirring to obtain slurry, placing the slurry in a nitrogen environment, and heat...

Ausführliche Beschreibung

Gespeichert in:
Bibliographische Detailangaben
Hauptverfasser: QIU CHEN, SHI SIHUI, QUAN SICHEN, LI HONGLIANG, ZHAO ZHIMAN
Format: Patent
Sprache:chi ; eng
Schlagworte:
Online-Zugang:Volltext bestellen
Tags: Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
container_end_page
container_issue
container_start_page
container_title
container_volume
creator QIU CHEN
SHI SIHUI
QUAN SICHEN
LI HONGLIANG
ZHAO ZHIMAN
description The invention discloses a method for preparing a high-performance cementing material by negative-pressure anaerobic thermal cracking of ardealite, which comprises the following steps: adding water into ardealite, fully stirring to obtain slurry, placing the slurry in a nitrogen environment, and heating the slurry to 50-60 DEG C under the pressure of 0.04-0.06 MPa; the reaction container is rotated at the speed of 30-50 r/min, the temperature of the slurry is maintained at 200-300 DEG C, and the reaction is performed for 60-120 min; and drying and collecting the materials in the reaction container to obtain the gypsum-based cementing material. The material cracking and heating are uniform, the gypsum phase composition is simple, the removal effect on impurities in phosphogypsum is stable, free phosphoric acid and other impurities which have great influence on the performance are removed through over-cracking, and repeated tests prove that the prepared gypsum cementing material is simple in gypsum phase, good i
format Patent
fullrecord <record><control><sourceid>epo_EVB</sourceid><recordid>TN_cdi_epo_espacenet_CN114656179A</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><sourcerecordid>CN114656179A</sourcerecordid><originalsourceid>FETCH-epo_espacenet_CN114656179A3</originalsourceid><addsrcrecordid>eNqNjD0OwjAUg7swIOAOjwN0qPgTI6pALDCxV4_gJhFtEr2kSCycnVTiAAyWJfuzp8XngmT8g1ovFASBxTpNxmpTBkhOe3YKpNDDpbHqOUEsd5SM-EEbctCc7Atlnsc4CIgdQ_zdqswgH3SkhNVzXPuWgvExS79DHPp5MWm5i1j8fFYsT8dbfS4RfIMYWMEhNfW1qtbbzbba7Q-rf5gvY7NKFQ</addsrcrecordid><sourcetype>Open Access Repository</sourcetype><iscdi>true</iscdi><recordtype>patent</recordtype></control><display><type>patent</type><title>Method for preparing high-performance cementing material through negative-pressure anaerobic thermal cracking of phosphogypsum</title><source>esp@cenet</source><creator>QIU CHEN ; SHI SIHUI ; QUAN SICHEN ; LI HONGLIANG ; ZHAO ZHIMAN</creator><creatorcontrib>QIU CHEN ; SHI SIHUI ; QUAN SICHEN ; LI HONGLIANG ; ZHAO ZHIMAN</creatorcontrib><description>The invention discloses a method for preparing a high-performance cementing material by negative-pressure anaerobic thermal cracking of ardealite, which comprises the following steps: adding water into ardealite, fully stirring to obtain slurry, placing the slurry in a nitrogen environment, and heating the slurry to 50-60 DEG C under the pressure of 0.04-0.06 MPa; the reaction container is rotated at the speed of 30-50 r/min, the temperature of the slurry is maintained at 200-300 DEG C, and the reaction is performed for 60-120 min; and drying and collecting the materials in the reaction container to obtain the gypsum-based cementing material. The material cracking and heating are uniform, the gypsum phase composition is simple, the removal effect on impurities in phosphogypsum is stable, free phosphoric acid and other impurities which have great influence on the performance are removed through over-cracking, and repeated tests prove that the prepared gypsum cementing material is simple in gypsum phase, good i</description><language>chi ; eng</language><subject>ARTIFICIAL STONE ; CEMENTS ; CERAMICS ; CHEMISTRY ; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDINGMATERIALS ; CONCRETE ; LIME, MAGNESIA ; METALLURGY ; REFRACTORIES ; SLAG ; TREATMENT OF NATURAL STONE</subject><creationdate>2022</creationdate><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&amp;date=20220624&amp;DB=EPODOC&amp;CC=CN&amp;NR=114656179A$$EHTML$$P50$$Gepo$$Hfree_for_read</linktohtml><link.rule.ids>230,308,780,885,25564,76419</link.rule.ids><linktorsrc>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&amp;date=20220624&amp;DB=EPODOC&amp;CC=CN&amp;NR=114656179A$$EView_record_in_European_Patent_Office$$FView_record_in_$$GEuropean_Patent_Office$$Hfree_for_read</linktorsrc></links><search><creatorcontrib>QIU CHEN</creatorcontrib><creatorcontrib>SHI SIHUI</creatorcontrib><creatorcontrib>QUAN SICHEN</creatorcontrib><creatorcontrib>LI HONGLIANG</creatorcontrib><creatorcontrib>ZHAO ZHIMAN</creatorcontrib><title>Method for preparing high-performance cementing material through negative-pressure anaerobic thermal cracking of phosphogypsum</title><description>The invention discloses a method for preparing a high-performance cementing material by negative-pressure anaerobic thermal cracking of ardealite, which comprises the following steps: adding water into ardealite, fully stirring to obtain slurry, placing the slurry in a nitrogen environment, and heating the slurry to 50-60 DEG C under the pressure of 0.04-0.06 MPa; the reaction container is rotated at the speed of 30-50 r/min, the temperature of the slurry is maintained at 200-300 DEG C, and the reaction is performed for 60-120 min; and drying and collecting the materials in the reaction container to obtain the gypsum-based cementing material. The material cracking and heating are uniform, the gypsum phase composition is simple, the removal effect on impurities in phosphogypsum is stable, free phosphoric acid and other impurities which have great influence on the performance are removed through over-cracking, and repeated tests prove that the prepared gypsum cementing material is simple in gypsum phase, good i</description><subject>ARTIFICIAL STONE</subject><subject>CEMENTS</subject><subject>CERAMICS</subject><subject>CHEMISTRY</subject><subject>COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDINGMATERIALS</subject><subject>CONCRETE</subject><subject>LIME, MAGNESIA</subject><subject>METALLURGY</subject><subject>REFRACTORIES</subject><subject>SLAG</subject><subject>TREATMENT OF NATURAL STONE</subject><fulltext>true</fulltext><rsrctype>patent</rsrctype><creationdate>2022</creationdate><recordtype>patent</recordtype><sourceid>EVB</sourceid><recordid>eNqNjD0OwjAUg7swIOAOjwN0qPgTI6pALDCxV4_gJhFtEr2kSCycnVTiAAyWJfuzp8XngmT8g1ovFASBxTpNxmpTBkhOe3YKpNDDpbHqOUEsd5SM-EEbctCc7Atlnsc4CIgdQ_zdqswgH3SkhNVzXPuWgvExS79DHPp5MWm5i1j8fFYsT8dbfS4RfIMYWMEhNfW1qtbbzbba7Q-rf5gvY7NKFQ</recordid><startdate>20220624</startdate><enddate>20220624</enddate><creator>QIU CHEN</creator><creator>SHI SIHUI</creator><creator>QUAN SICHEN</creator><creator>LI HONGLIANG</creator><creator>ZHAO ZHIMAN</creator><scope>EVB</scope></search><sort><creationdate>20220624</creationdate><title>Method for preparing high-performance cementing material through negative-pressure anaerobic thermal cracking of phosphogypsum</title><author>QIU CHEN ; SHI SIHUI ; QUAN SICHEN ; LI HONGLIANG ; ZHAO ZHIMAN</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-epo_espacenet_CN114656179A3</frbrgroupid><rsrctype>patents</rsrctype><prefilter>patents</prefilter><language>chi ; eng</language><creationdate>2022</creationdate><topic>ARTIFICIAL STONE</topic><topic>CEMENTS</topic><topic>CERAMICS</topic><topic>CHEMISTRY</topic><topic>COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDINGMATERIALS</topic><topic>CONCRETE</topic><topic>LIME, MAGNESIA</topic><topic>METALLURGY</topic><topic>REFRACTORIES</topic><topic>SLAG</topic><topic>TREATMENT OF NATURAL STONE</topic><toplevel>online_resources</toplevel><creatorcontrib>QIU CHEN</creatorcontrib><creatorcontrib>SHI SIHUI</creatorcontrib><creatorcontrib>QUAN SICHEN</creatorcontrib><creatorcontrib>LI HONGLIANG</creatorcontrib><creatorcontrib>ZHAO ZHIMAN</creatorcontrib><collection>esp@cenet</collection></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext_linktorsrc</fulltext></delivery><addata><au>QIU CHEN</au><au>SHI SIHUI</au><au>QUAN SICHEN</au><au>LI HONGLIANG</au><au>ZHAO ZHIMAN</au><format>patent</format><genre>patent</genre><ristype>GEN</ristype><title>Method for preparing high-performance cementing material through negative-pressure anaerobic thermal cracking of phosphogypsum</title><date>2022-06-24</date><risdate>2022</risdate><abstract>The invention discloses a method for preparing a high-performance cementing material by negative-pressure anaerobic thermal cracking of ardealite, which comprises the following steps: adding water into ardealite, fully stirring to obtain slurry, placing the slurry in a nitrogen environment, and heating the slurry to 50-60 DEG C under the pressure of 0.04-0.06 MPa; the reaction container is rotated at the speed of 30-50 r/min, the temperature of the slurry is maintained at 200-300 DEG C, and the reaction is performed for 60-120 min; and drying and collecting the materials in the reaction container to obtain the gypsum-based cementing material. The material cracking and heating are uniform, the gypsum phase composition is simple, the removal effect on impurities in phosphogypsum is stable, free phosphoric acid and other impurities which have great influence on the performance are removed through over-cracking, and repeated tests prove that the prepared gypsum cementing material is simple in gypsum phase, good i</abstract><oa>free_for_read</oa></addata></record>
fulltext fulltext_linktorsrc
identifier
ispartof
issn
language chi ; eng
recordid cdi_epo_espacenet_CN114656179A
source esp@cenet
subjects ARTIFICIAL STONE
CEMENTS
CERAMICS
CHEMISTRY
COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDINGMATERIALS
CONCRETE
LIME, MAGNESIA
METALLURGY
REFRACTORIES
SLAG
TREATMENT OF NATURAL STONE
title Method for preparing high-performance cementing material through negative-pressure anaerobic thermal cracking of phosphogypsum
url https://sfx.bib-bvb.de/sfx_tum?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2025-01-07T16%3A38%3A52IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-epo_EVB&rft_val_fmt=info:ofi/fmt:kev:mtx:patent&rft.genre=patent&rft.au=QIU%20CHEN&rft.date=2022-06-24&rft_id=info:doi/&rft_dat=%3Cepo_EVB%3ECN114656179A%3C/epo_EVB%3E%3Curl%3E%3C/url%3E&disable_directlink=true&sfx.directlink=off&sfx.report_link=0&rft_id=info:oai/&rft_id=info:pmid/&rfr_iscdi=true