Method for preparing high-performance cementing material through negative-pressure anaerobic thermal cracking of phosphogypsum
The invention discloses a method for preparing a high-performance cementing material by negative-pressure anaerobic thermal cracking of ardealite, which comprises the following steps: adding water into ardealite, fully stirring to obtain slurry, placing the slurry in a nitrogen environment, and heat...
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creator | QIU CHEN SHI SIHUI QUAN SICHEN LI HONGLIANG ZHAO ZHIMAN |
description | The invention discloses a method for preparing a high-performance cementing material by negative-pressure anaerobic thermal cracking of ardealite, which comprises the following steps: adding water into ardealite, fully stirring to obtain slurry, placing the slurry in a nitrogen environment, and heating the slurry to 50-60 DEG C under the pressure of 0.04-0.06 MPa; the reaction container is rotated at the speed of 30-50 r/min, the temperature of the slurry is maintained at 200-300 DEG C, and the reaction is performed for 60-120 min; and drying and collecting the materials in the reaction container to obtain the gypsum-based cementing material. The material cracking and heating are uniform, the gypsum phase composition is simple, the removal effect on impurities in phosphogypsum is stable, free phosphoric acid and other impurities which have great influence on the performance are removed through over-cracking, and repeated tests prove that the prepared gypsum cementing material is simple in gypsum phase, good i |
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The material cracking and heating are uniform, the gypsum phase composition is simple, the removal effect on impurities in phosphogypsum is stable, free phosphoric acid and other impurities which have great influence on the performance are removed through over-cracking, and repeated tests prove that the prepared gypsum cementing material is simple in gypsum phase, good i</description><language>chi ; eng</language><subject>ARTIFICIAL STONE ; CEMENTS ; CERAMICS ; CHEMISTRY ; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDINGMATERIALS ; CONCRETE ; LIME, MAGNESIA ; METALLURGY ; REFRACTORIES ; SLAG ; TREATMENT OF NATURAL STONE</subject><creationdate>2022</creationdate><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&date=20220624&DB=EPODOC&CC=CN&NR=114656179A$$EHTML$$P50$$Gepo$$Hfree_for_read</linktohtml><link.rule.ids>230,308,780,885,25564,76419</link.rule.ids><linktorsrc>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&date=20220624&DB=EPODOC&CC=CN&NR=114656179A$$EView_record_in_European_Patent_Office$$FView_record_in_$$GEuropean_Patent_Office$$Hfree_for_read</linktorsrc></links><search><creatorcontrib>QIU CHEN</creatorcontrib><creatorcontrib>SHI SIHUI</creatorcontrib><creatorcontrib>QUAN SICHEN</creatorcontrib><creatorcontrib>LI HONGLIANG</creatorcontrib><creatorcontrib>ZHAO ZHIMAN</creatorcontrib><title>Method for preparing high-performance cementing material through negative-pressure anaerobic thermal cracking of phosphogypsum</title><description>The invention discloses a method for preparing a high-performance cementing material by negative-pressure anaerobic thermal cracking of ardealite, which comprises the following steps: adding water into ardealite, fully stirring to obtain slurry, placing the slurry in a nitrogen environment, and heating the slurry to 50-60 DEG C under the pressure of 0.04-0.06 MPa; the reaction container is rotated at the speed of 30-50 r/min, the temperature of the slurry is maintained at 200-300 DEG C, and the reaction is performed for 60-120 min; and drying and collecting the materials in the reaction container to obtain the gypsum-based cementing material. The material cracking and heating are uniform, the gypsum phase composition is simple, the removal effect on impurities in phosphogypsum is stable, free phosphoric acid and other impurities which have great influence on the performance are removed through over-cracking, and repeated tests prove that the prepared gypsum cementing material is simple in gypsum phase, good i</description><subject>ARTIFICIAL STONE</subject><subject>CEMENTS</subject><subject>CERAMICS</subject><subject>CHEMISTRY</subject><subject>COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDINGMATERIALS</subject><subject>CONCRETE</subject><subject>LIME, MAGNESIA</subject><subject>METALLURGY</subject><subject>REFRACTORIES</subject><subject>SLAG</subject><subject>TREATMENT OF NATURAL STONE</subject><fulltext>true</fulltext><rsrctype>patent</rsrctype><creationdate>2022</creationdate><recordtype>patent</recordtype><sourceid>EVB</sourceid><recordid>eNqNjD0OwjAUg7swIOAOjwN0qPgTI6pALDCxV4_gJhFtEr2kSCycnVTiAAyWJfuzp8XngmT8g1ovFASBxTpNxmpTBkhOe3YKpNDDpbHqOUEsd5SM-EEbctCc7Atlnsc4CIgdQ_zdqswgH3SkhNVzXPuWgvExS79DHPp5MWm5i1j8fFYsT8dbfS4RfIMYWMEhNfW1qtbbzbba7Q-rf5gvY7NKFQ</recordid><startdate>20220624</startdate><enddate>20220624</enddate><creator>QIU CHEN</creator><creator>SHI SIHUI</creator><creator>QUAN SICHEN</creator><creator>LI HONGLIANG</creator><creator>ZHAO ZHIMAN</creator><scope>EVB</scope></search><sort><creationdate>20220624</creationdate><title>Method for preparing high-performance cementing material through negative-pressure anaerobic thermal cracking of phosphogypsum</title><author>QIU CHEN ; SHI SIHUI ; QUAN SICHEN ; LI HONGLIANG ; ZHAO ZHIMAN</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-epo_espacenet_CN114656179A3</frbrgroupid><rsrctype>patents</rsrctype><prefilter>patents</prefilter><language>chi ; eng</language><creationdate>2022</creationdate><topic>ARTIFICIAL STONE</topic><topic>CEMENTS</topic><topic>CERAMICS</topic><topic>CHEMISTRY</topic><topic>COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDINGMATERIALS</topic><topic>CONCRETE</topic><topic>LIME, MAGNESIA</topic><topic>METALLURGY</topic><topic>REFRACTORIES</topic><topic>SLAG</topic><topic>TREATMENT OF NATURAL STONE</topic><toplevel>online_resources</toplevel><creatorcontrib>QIU CHEN</creatorcontrib><creatorcontrib>SHI SIHUI</creatorcontrib><creatorcontrib>QUAN SICHEN</creatorcontrib><creatorcontrib>LI HONGLIANG</creatorcontrib><creatorcontrib>ZHAO ZHIMAN</creatorcontrib><collection>esp@cenet</collection></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext_linktorsrc</fulltext></delivery><addata><au>QIU CHEN</au><au>SHI SIHUI</au><au>QUAN SICHEN</au><au>LI HONGLIANG</au><au>ZHAO ZHIMAN</au><format>patent</format><genre>patent</genre><ristype>GEN</ristype><title>Method for preparing high-performance cementing material through negative-pressure anaerobic thermal cracking of phosphogypsum</title><date>2022-06-24</date><risdate>2022</risdate><abstract>The invention discloses a method for preparing a high-performance cementing material by negative-pressure anaerobic thermal cracking of ardealite, which comprises the following steps: adding water into ardealite, fully stirring to obtain slurry, placing the slurry in a nitrogen environment, and heating the slurry to 50-60 DEG C under the pressure of 0.04-0.06 MPa; the reaction container is rotated at the speed of 30-50 r/min, the temperature of the slurry is maintained at 200-300 DEG C, and the reaction is performed for 60-120 min; and drying and collecting the materials in the reaction container to obtain the gypsum-based cementing material. The material cracking and heating are uniform, the gypsum phase composition is simple, the removal effect on impurities in phosphogypsum is stable, free phosphoric acid and other impurities which have great influence on the performance are removed through over-cracking, and repeated tests prove that the prepared gypsum cementing material is simple in gypsum phase, good i</abstract><oa>free_for_read</oa></addata></record> |
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subjects | ARTIFICIAL STONE CEMENTS CERAMICS CHEMISTRY COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDINGMATERIALS CONCRETE LIME, MAGNESIA METALLURGY REFRACTORIES SLAG TREATMENT OF NATURAL STONE |
title | Method for preparing high-performance cementing material through negative-pressure anaerobic thermal cracking of phosphogypsum |
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