Preparation method of perdeuterated benzene
The invention relates to a preparation method of perdeuterated benzene, and belongs to the field of organic chemical synthesis. According to the method, cheap deuterium water is used as a deuterium source, so that the use of an expensive deuterium source is avoided; hexabromo-benzene is used as a ra...
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creator | LI ENCI CAO CHENHUI SHUI XINFENG ZHANG HONGHAI |
description | The invention relates to a preparation method of perdeuterated benzene, and belongs to the field of organic chemical synthesis. According to the method, cheap deuterium water is used as a deuterium source, so that the use of an expensive deuterium source is avoided; hexabromo-benzene is used as a raw material, so that the technology of efficiently utilizing isotopes is realized; a non-deuterated organic solvent is used as a solvent, so that the use of an expensive deuterated reagent is avoided; cheap metal is used as a catalyst, and expensive metal is prevented from being used. The method is cheap, efficient, pollution-free and suitable for industrial production. The deuterated benzene can be used in the fields of organic photoelectricity, medicines, pesticides and the like.
本发明涉一种全氘代苯的制备方法,属于有机化学合成领域。所述方法以廉价的氘水为氘源,避免了昂贵氘源的使用;以六溴苯为原料,实现了高效利用同位素的技术;以非氘代有机溶剂为溶剂,避免使用昂贵氘代试剂;使用廉价金属作为催化剂,避免使用昂贵金属。该方法廉价、高效、无污染,适用于工业化生产。氘代苯可用于有机光电、医药农药等领域。 |
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本发明涉一种全氘代苯的制备方法,属于有机化学合成领域。所述方法以廉价的氘水为氘源,避免了昂贵氘源的使用;以六溴苯为原料,实现了高效利用同位素的技术;以非氘代有机溶剂为溶剂,避免使用昂贵氘代试剂;使用廉价金属作为催化剂,避免使用昂贵金属。该方法廉价、高效、无污染,适用于工业化生产。氘代苯可用于有机光电、医药农药等领域。</description><language>chi ; eng</language><subject>ACYCLIC OR CARBOCYCLIC COMPOUNDS ; APPARATUS THEREFOR ; CHEMISTRY ; GENERAL METHODS OF ORGANIC CHEMISTRY ; METALLURGY ; ORGANIC CHEMISTRY</subject><creationdate>2022</creationdate><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&date=20220322&DB=EPODOC&CC=CN&NR=114213205A$$EHTML$$P50$$Gepo$$Hfree_for_read</linktohtml><link.rule.ids>230,308,776,881,25543,76293</link.rule.ids><linktorsrc>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&date=20220322&DB=EPODOC&CC=CN&NR=114213205A$$EView_record_in_European_Patent_Office$$FView_record_in_$$GEuropean_Patent_Office$$Hfree_for_read</linktorsrc></links><search><creatorcontrib>LI ENCI</creatorcontrib><creatorcontrib>CAO CHENHUI</creatorcontrib><creatorcontrib>SHUI XINFENG</creatorcontrib><creatorcontrib>ZHANG HONGHAI</creatorcontrib><title>Preparation method of perdeuterated benzene</title><description>The invention relates to a preparation method of perdeuterated benzene, and belongs to the field of organic chemical synthesis. According to the method, cheap deuterium water is used as a deuterium source, so that the use of an expensive deuterium source is avoided; hexabromo-benzene is used as a raw material, so that the technology of efficiently utilizing isotopes is realized; a non-deuterated organic solvent is used as a solvent, so that the use of an expensive deuterated reagent is avoided; cheap metal is used as a catalyst, and expensive metal is prevented from being used. The method is cheap, efficient, pollution-free and suitable for industrial production. The deuterated benzene can be used in the fields of organic photoelectricity, medicines, pesticides and the like.
本发明涉一种全氘代苯的制备方法,属于有机化学合成领域。所述方法以廉价的氘水为氘源,避免了昂贵氘源的使用;以六溴苯为原料,实现了高效利用同位素的技术;以非氘代有机溶剂为溶剂,避免使用昂贵氘代试剂;使用廉价金属作为催化剂,避免使用昂贵金属。该方法廉价、高效、无污染,适用于工业化生产。氘代苯可用于有机光电、医药农药等领域。</description><subject>ACYCLIC OR CARBOCYCLIC COMPOUNDS</subject><subject>APPARATUS THEREFOR</subject><subject>CHEMISTRY</subject><subject>GENERAL METHODS OF ORGANIC CHEMISTRY</subject><subject>METALLURGY</subject><subject>ORGANIC CHEMISTRY</subject><fulltext>true</fulltext><rsrctype>patent</rsrctype><creationdate>2022</creationdate><recordtype>patent</recordtype><sourceid>EVB</sourceid><recordid>eNrjZNAOKEotSCxKLMnMz1PITS3JyE9RyE9TKEgtSkktLUkFSqSmKCSl5lWl5qXyMLCmJeYUp_JCaW4GRTfXEGcP3dSC_PjU4oLEZKCiknhnP0NDEyNDYyMDU0djYtQAAIccKag</recordid><startdate>20220322</startdate><enddate>20220322</enddate><creator>LI ENCI</creator><creator>CAO CHENHUI</creator><creator>SHUI XINFENG</creator><creator>ZHANG HONGHAI</creator><scope>EVB</scope></search><sort><creationdate>20220322</creationdate><title>Preparation method of perdeuterated benzene</title><author>LI ENCI ; CAO CHENHUI ; SHUI XINFENG ; ZHANG HONGHAI</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-epo_espacenet_CN114213205A3</frbrgroupid><rsrctype>patents</rsrctype><prefilter>patents</prefilter><language>chi ; eng</language><creationdate>2022</creationdate><topic>ACYCLIC OR CARBOCYCLIC COMPOUNDS</topic><topic>APPARATUS THEREFOR</topic><topic>CHEMISTRY</topic><topic>GENERAL METHODS OF ORGANIC CHEMISTRY</topic><topic>METALLURGY</topic><topic>ORGANIC CHEMISTRY</topic><toplevel>online_resources</toplevel><creatorcontrib>LI ENCI</creatorcontrib><creatorcontrib>CAO CHENHUI</creatorcontrib><creatorcontrib>SHUI XINFENG</creatorcontrib><creatorcontrib>ZHANG HONGHAI</creatorcontrib><collection>esp@cenet</collection></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext_linktorsrc</fulltext></delivery><addata><au>LI ENCI</au><au>CAO CHENHUI</au><au>SHUI XINFENG</au><au>ZHANG HONGHAI</au><format>patent</format><genre>patent</genre><ristype>GEN</ristype><title>Preparation method of perdeuterated benzene</title><date>2022-03-22</date><risdate>2022</risdate><abstract>The invention relates to a preparation method of perdeuterated benzene, and belongs to the field of organic chemical synthesis. According to the method, cheap deuterium water is used as a deuterium source, so that the use of an expensive deuterium source is avoided; hexabromo-benzene is used as a raw material, so that the technology of efficiently utilizing isotopes is realized; a non-deuterated organic solvent is used as a solvent, so that the use of an expensive deuterated reagent is avoided; cheap metal is used as a catalyst, and expensive metal is prevented from being used. The method is cheap, efficient, pollution-free and suitable for industrial production. The deuterated benzene can be used in the fields of organic photoelectricity, medicines, pesticides and the like.
本发明涉一种全氘代苯的制备方法,属于有机化学合成领域。所述方法以廉价的氘水为氘源,避免了昂贵氘源的使用;以六溴苯为原料,实现了高效利用同位素的技术;以非氘代有机溶剂为溶剂,避免使用昂贵氘代试剂;使用廉价金属作为催化剂,避免使用昂贵金属。该方法廉价、高效、无污染,适用于工业化生产。氘代苯可用于有机光电、医药农药等领域。</abstract><oa>free_for_read</oa></addata></record> |
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subjects | ACYCLIC OR CARBOCYCLIC COMPOUNDS APPARATUS THEREFOR CHEMISTRY GENERAL METHODS OF ORGANIC CHEMISTRY METALLURGY ORGANIC CHEMISTRY |
title | Preparation method of perdeuterated benzene |
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