Process for preparing 1-nitronaphthalene through continuous low-temperature nitration
The invention discloses a process for preparing 1-nitronaphthalene through continuous low-temperature nitration, wherein the process mainly comprises nitration, pre-washing, neutralization and washing procedures; a nitration device is formed by connecting three nitration kettles, a waste acid extrac...
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creator | QI QIANKUN LI CAOYUE SHI PENGFEI XU GUOXIANG WANG SUGUANG JIANG QIN GAO CHUNYUAN |
description | The invention discloses a process for preparing 1-nitronaphthalene through continuous low-temperature nitration, wherein the process mainly comprises nitration, pre-washing, neutralization and washing procedures; a nitration device is formed by connecting three nitration kettles, a waste acid extraction kettle, two pre-washing kettles, two neutralization kettles and two washing kettles in series; the three nitration kettles comprise a 1# nitration kettle, a 2# nitration kettle and a 3# nitration kettle; the two pre-washing kettles comprise a 1# pre-washing kettle and a 2# pre-washing kettle; the two neutralization kettles comprise a 1# neutralization kettle and a 2# neutralization kettle; and the two washing kettles comprise a 1# washing kettle and a 2# washing kettle. The process parameters are stable, the yield and quality of the product are improved and stabilized, safety production is facilitated, and automatic control is easy to achieve.
本发明公开了连续低温硝化制备1-硝基萘的工艺,主要包含有硝化、预洗、中和、洗涤工序,硝化装置由三台硝化釜、一台废酸萃取釜、两台预洗釜、 |
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本发明公开了连续低温硝化制备1-硝基萘的工艺,主要包含有硝化、预洗、中和、洗涤工序,硝化装置由三台硝化釜、一台废酸萃取釜、两台预洗釜、</description><language>chi ; eng</language><subject>ACYCLIC OR CARBOCYCLIC COMPOUNDS ; CHEMISTRY ; METALLURGY ; ORGANIC CHEMISTRY</subject><creationdate>2021</creationdate><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&date=20211231&DB=EPODOC&CC=CN&NR=113861033A$$EHTML$$P50$$Gepo$$Hfree_for_read</linktohtml><link.rule.ids>230,308,776,881,25542,76289</link.rule.ids><linktorsrc>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&date=20211231&DB=EPODOC&CC=CN&NR=113861033A$$EView_record_in_European_Patent_Office$$FView_record_in_$$GEuropean_Patent_Office$$Hfree_for_read</linktorsrc></links><search><creatorcontrib>QI QIANKUN</creatorcontrib><creatorcontrib>LI CAOYUE</creatorcontrib><creatorcontrib>SHI PENGFEI</creatorcontrib><creatorcontrib>XU GUOXIANG</creatorcontrib><creatorcontrib>WANG SUGUANG</creatorcontrib><creatorcontrib>JIANG QIN</creatorcontrib><creatorcontrib>GAO CHUNYUAN</creatorcontrib><title>Process for preparing 1-nitronaphthalene through continuous low-temperature nitration</title><description>The invention discloses a process for preparing 1-nitronaphthalene through continuous low-temperature nitration, wherein the process mainly comprises nitration, pre-washing, neutralization and washing procedures; a nitration device is formed by connecting three nitration kettles, a waste acid extraction kettle, two pre-washing kettles, two neutralization kettles and two washing kettles in series; the three nitration kettles comprise a 1# nitration kettle, a 2# nitration kettle and a 3# nitration kettle; the two pre-washing kettles comprise a 1# pre-washing kettle and a 2# pre-washing kettle; the two neutralization kettles comprise a 1# neutralization kettle and a 2# neutralization kettle; and the two washing kettles comprise a 1# washing kettle and a 2# washing kettle. The process parameters are stable, the yield and quality of the product are improved and stabilized, safety production is facilitated, and automatic control is easy to achieve.
本发明公开了连续低温硝化制备1-硝基萘的工艺,主要包含有硝化、预洗、中和、洗涤工序,硝化装置由三台硝化釜、一台废酸萃取釜、两台预洗釜、</description><subject>ACYCLIC OR CARBOCYCLIC COMPOUNDS</subject><subject>CHEMISTRY</subject><subject>METALLURGY</subject><subject>ORGANIC CHEMISTRY</subject><fulltext>true</fulltext><rsrctype>patent</rsrctype><creationdate>2021</creationdate><recordtype>patent</recordtype><sourceid>EVB</sourceid><recordid>eNqNjDEKAjEQAK-xEPUP6wMChoDYyqFYiYXWx3LsXQJxN2w2-H0VfIDVNDOz7B43lZFqhUkUilJBTTyDd5xMhbFEi5iJCSyqtDnCKGyJm7QKWV7O6FlI0ZoSfBu0JLzuFhPmSpsfV932fLr3F0dFBqoFx8_Rhv7qfTjs_S6EY_jHeQNvBDpt</recordid><startdate>20211231</startdate><enddate>20211231</enddate><creator>QI QIANKUN</creator><creator>LI CAOYUE</creator><creator>SHI PENGFEI</creator><creator>XU GUOXIANG</creator><creator>WANG SUGUANG</creator><creator>JIANG QIN</creator><creator>GAO CHUNYUAN</creator><scope>EVB</scope></search><sort><creationdate>20211231</creationdate><title>Process for preparing 1-nitronaphthalene through continuous low-temperature nitration</title><author>QI QIANKUN ; LI CAOYUE ; SHI PENGFEI ; XU GUOXIANG ; WANG SUGUANG ; JIANG QIN ; GAO CHUNYUAN</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-epo_espacenet_CN113861033A3</frbrgroupid><rsrctype>patents</rsrctype><prefilter>patents</prefilter><language>chi ; eng</language><creationdate>2021</creationdate><topic>ACYCLIC OR CARBOCYCLIC COMPOUNDS</topic><topic>CHEMISTRY</topic><topic>METALLURGY</topic><topic>ORGANIC CHEMISTRY</topic><toplevel>online_resources</toplevel><creatorcontrib>QI QIANKUN</creatorcontrib><creatorcontrib>LI CAOYUE</creatorcontrib><creatorcontrib>SHI PENGFEI</creatorcontrib><creatorcontrib>XU GUOXIANG</creatorcontrib><creatorcontrib>WANG SUGUANG</creatorcontrib><creatorcontrib>JIANG QIN</creatorcontrib><creatorcontrib>GAO CHUNYUAN</creatorcontrib><collection>esp@cenet</collection></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext_linktorsrc</fulltext></delivery><addata><au>QI QIANKUN</au><au>LI CAOYUE</au><au>SHI PENGFEI</au><au>XU GUOXIANG</au><au>WANG SUGUANG</au><au>JIANG QIN</au><au>GAO CHUNYUAN</au><format>patent</format><genre>patent</genre><ristype>GEN</ristype><title>Process for preparing 1-nitronaphthalene through continuous low-temperature nitration</title><date>2021-12-31</date><risdate>2021</risdate><abstract>The invention discloses a process for preparing 1-nitronaphthalene through continuous low-temperature nitration, wherein the process mainly comprises nitration, pre-washing, neutralization and washing procedures; a nitration device is formed by connecting three nitration kettles, a waste acid extraction kettle, two pre-washing kettles, two neutralization kettles and two washing kettles in series; the three nitration kettles comprise a 1# nitration kettle, a 2# nitration kettle and a 3# nitration kettle; the two pre-washing kettles comprise a 1# pre-washing kettle and a 2# pre-washing kettle; the two neutralization kettles comprise a 1# neutralization kettle and a 2# neutralization kettle; and the two washing kettles comprise a 1# washing kettle and a 2# washing kettle. The process parameters are stable, the yield and quality of the product are improved and stabilized, safety production is facilitated, and automatic control is easy to achieve.
本发明公开了连续低温硝化制备1-硝基萘的工艺,主要包含有硝化、预洗、中和、洗涤工序,硝化装置由三台硝化釜、一台废酸萃取釜、两台预洗釜、</abstract><oa>free_for_read</oa></addata></record> |
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title | Process for preparing 1-nitronaphthalene through continuous low-temperature nitration |
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