Preparing method and application of chitosan grafted mesoporous silica nanofiber membrane

The invention discloses a preparing method and application of a chitosan grafted mesoporous silica nanofiber membrane. The nanofiber membrane is used for adsorbing heavy metal materials in water. A nanofiber membrane is obtained by conducting electrostatic spinning with polyvinyl alcohol and tetraet...

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Hauptverfasser: NIE JUN, ZHANG LU, PENG CHAOYUN, MA GUIPING
Format: Patent
Sprache:chi ; eng
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Zusammenfassung:The invention discloses a preparing method and application of a chitosan grafted mesoporous silica nanofiber membrane. The nanofiber membrane is used for adsorbing heavy metal materials in water. A nanofiber membrane is obtained by conducting electrostatic spinning with polyvinyl alcohol and tetraethoxysilane (TEOS) hydrolysate as the spinning solution and put into a muffle furnace to be calcinated, and the silica nanofiber membrane without polyvinyl alcohol is obtained. The nanofiber membrane is soaked in chitosan acetone dispersion liquid for 10 hours after the surface of the nanofiber membrane is coated with a silicane epoxide coupling agent KH-560 to obtain the chitosan surface-grafted silica nanofiber membrane. The method is simple in process and easy to operate, and the obtained nanofiber membrane is high in specific surface area, can be recycled, has the mesoporous silica and chitosan duplex adsorption function, can effectively adsorb heavy metal ions in water and has broad prospects on the aspect of w