Glufosinate-phosphonic acid hydrate single crystal and preparation method thereof
The invention discloses a glufosinate-phosphonic acid hydrate single crystal and a preparation method thereof. The glufosinate-phosphonic acid hydrate single crystal belongs to an orthorhombic system,and has a space group of P2 2 2 , and the following cell parameters: alpha=90 degrees, beta=90 degre...
Gespeichert in:
| Hauptverfasser: | , , , , , , , , , , |
|---|---|
| Format: | Patent |
| Sprache: | chi ; eng |
| Schlagworte: | |
| Online-Zugang: | Volltext bestellen |
| Tags: |
Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
|
| container_end_page | |
|---|---|
| container_issue | |
| container_start_page | |
| container_title | |
| container_volume | |
| creator | LIU JUN CHAI HONGWEI ZUO BOJUN HAN JINTAO XIE YINPING DONG WENKAI LI XUKUN WANG MINGGANG JIANG AIZHONG WANG YINGXIU LI LEI |
| description | The invention discloses a glufosinate-phosphonic acid hydrate single crystal and a preparation method thereof. The glufosinate-phosphonic acid hydrate single crystal belongs to an orthorhombic system,and has a space group of P2 2 2 , and the following cell parameters: alpha=90 degrees, beta=90 degrees and gamma=90 degrees, the unit cell volume is that 4 molecules of glufosinate-phosphonic acid and 4 molecules of water contained in per unit cell. The preparation method comprises the following steps: dissolving the glufosinate-phosphonic acid into a solvent, performing cooling, allowing the cooled solution to stand, slowly evaporating the solvent, and performing crystallization to obtain the glufosinate-phosphonic acid hydrate single crystal. The glufosinate-phosphonic acid hydrate single crystal provided by the invention belongs to the orthorhombic system and is a novel monohydrate crystal different from a current technology, and the preparation method is simple and has a green and environmentally-friendly pre |
| format | Patent |
| fullrecord | <record><control><sourceid>epo_EVB</sourceid><recordid>TN_cdi_epo_espacenet_CN110437276A</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><sourcerecordid>CN110437276A</sourcerecordid><originalsourceid>FETCH-epo_espacenet_CN110437276A3</originalsourceid><addsrcrecordid>eNqNijsKAjEURdNYiLqH5wIGHEecWgY_lSDYD4_kjgnEvJDEYnZvChdgcTlwzl2qx9V_JskucEETreS64DSxdobsbFL1VPPLg3Sac2FPHAzFhMg1Ogn0RrFiqFgkyLRWi4l9xubHldpezs_h1iDKiBxZI6CMw71td4eu3_fHU_fP5ws9CThr</addsrcrecordid><sourcetype>Open Access Repository</sourcetype><iscdi>true</iscdi><recordtype>patent</recordtype></control><display><type>patent</type><title>Glufosinate-phosphonic acid hydrate single crystal and preparation method thereof</title><source>esp@cenet</source><creator>LIU JUN ; CHAI HONGWEI ; ZUO BOJUN ; HAN JINTAO ; XIE YINPING ; DONG WENKAI ; LI XUKUN ; WANG MINGGANG ; JIANG AIZHONG ; WANG YINGXIU ; LI LEI</creator><creatorcontrib>LIU JUN ; CHAI HONGWEI ; ZUO BOJUN ; HAN JINTAO ; XIE YINPING ; DONG WENKAI ; LI XUKUN ; WANG MINGGANG ; JIANG AIZHONG ; WANG YINGXIU ; LI LEI</creatorcontrib><description>The invention discloses a glufosinate-phosphonic acid hydrate single crystal and a preparation method thereof. The glufosinate-phosphonic acid hydrate single crystal belongs to an orthorhombic system,and has a space group of P2 2 2 , and the following cell parameters: alpha=90 degrees, beta=90 degrees and gamma=90 degrees, the unit cell volume is that 4 molecules of glufosinate-phosphonic acid and 4 molecules of water contained in per unit cell. The preparation method comprises the following steps: dissolving the glufosinate-phosphonic acid into a solvent, performing cooling, allowing the cooled solution to stand, slowly evaporating the solvent, and performing crystallization to obtain the glufosinate-phosphonic acid hydrate single crystal. The glufosinate-phosphonic acid hydrate single crystal provided by the invention belongs to the orthorhombic system and is a novel monohydrate crystal different from a current technology, and the preparation method is simple and has a green and environmentally-friendly pre</description><language>chi ; eng</language><subject>ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAININGELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN,SULFUR, SELENIUM OR TELLURIUM ; CHEMISTRY ; METALLURGY ; ORGANIC CHEMISTRY</subject><creationdate>2019</creationdate><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&date=20191112&DB=EPODOC&CC=CN&NR=110437276A$$EHTML$$P50$$Gepo$$Hfree_for_read</linktohtml><link.rule.ids>230,308,776,881,25543,76293</link.rule.ids><linktorsrc>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&date=20191112&DB=EPODOC&CC=CN&NR=110437276A$$EView_record_in_European_Patent_Office$$FView_record_in_$$GEuropean_Patent_Office$$Hfree_for_read</linktorsrc></links><search><creatorcontrib>LIU JUN</creatorcontrib><creatorcontrib>CHAI HONGWEI</creatorcontrib><creatorcontrib>ZUO BOJUN</creatorcontrib><creatorcontrib>HAN JINTAO</creatorcontrib><creatorcontrib>XIE YINPING</creatorcontrib><creatorcontrib>DONG WENKAI</creatorcontrib><creatorcontrib>LI XUKUN</creatorcontrib><creatorcontrib>WANG MINGGANG</creatorcontrib><creatorcontrib>JIANG AIZHONG</creatorcontrib><creatorcontrib>WANG YINGXIU</creatorcontrib><creatorcontrib>LI LEI</creatorcontrib><title>Glufosinate-phosphonic acid hydrate single crystal and preparation method thereof</title><description>The invention discloses a glufosinate-phosphonic acid hydrate single crystal and a preparation method thereof. The glufosinate-phosphonic acid hydrate single crystal belongs to an orthorhombic system,and has a space group of P2 2 2 , and the following cell parameters: alpha=90 degrees, beta=90 degrees and gamma=90 degrees, the unit cell volume is that 4 molecules of glufosinate-phosphonic acid and 4 molecules of water contained in per unit cell. The preparation method comprises the following steps: dissolving the glufosinate-phosphonic acid into a solvent, performing cooling, allowing the cooled solution to stand, slowly evaporating the solvent, and performing crystallization to obtain the glufosinate-phosphonic acid hydrate single crystal. The glufosinate-phosphonic acid hydrate single crystal provided by the invention belongs to the orthorhombic system and is a novel monohydrate crystal different from a current technology, and the preparation method is simple and has a green and environmentally-friendly pre</description><subject>ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAININGELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN,SULFUR, SELENIUM OR TELLURIUM</subject><subject>CHEMISTRY</subject><subject>METALLURGY</subject><subject>ORGANIC CHEMISTRY</subject><fulltext>true</fulltext><rsrctype>patent</rsrctype><creationdate>2019</creationdate><recordtype>patent</recordtype><sourceid>EVB</sourceid><recordid>eNqNijsKAjEURdNYiLqH5wIGHEecWgY_lSDYD4_kjgnEvJDEYnZvChdgcTlwzl2qx9V_JskucEETreS64DSxdobsbFL1VPPLg3Sac2FPHAzFhMg1Ogn0RrFiqFgkyLRWi4l9xubHldpezs_h1iDKiBxZI6CMw71td4eu3_fHU_fP5ws9CThr</recordid><startdate>20191112</startdate><enddate>20191112</enddate><creator>LIU JUN</creator><creator>CHAI HONGWEI</creator><creator>ZUO BOJUN</creator><creator>HAN JINTAO</creator><creator>XIE YINPING</creator><creator>DONG WENKAI</creator><creator>LI XUKUN</creator><creator>WANG MINGGANG</creator><creator>JIANG AIZHONG</creator><creator>WANG YINGXIU</creator><creator>LI LEI</creator><scope>EVB</scope></search><sort><creationdate>20191112</creationdate><title>Glufosinate-phosphonic acid hydrate single crystal and preparation method thereof</title><author>LIU JUN ; CHAI HONGWEI ; ZUO BOJUN ; HAN JINTAO ; XIE YINPING ; DONG WENKAI ; LI XUKUN ; WANG MINGGANG ; JIANG AIZHONG ; WANG YINGXIU ; LI LEI</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-epo_espacenet_CN110437276A3</frbrgroupid><rsrctype>patents</rsrctype><prefilter>patents</prefilter><language>chi ; eng</language><creationdate>2019</creationdate><topic>ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAININGELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN,SULFUR, SELENIUM OR TELLURIUM</topic><topic>CHEMISTRY</topic><topic>METALLURGY</topic><topic>ORGANIC CHEMISTRY</topic><toplevel>online_resources</toplevel><creatorcontrib>LIU JUN</creatorcontrib><creatorcontrib>CHAI HONGWEI</creatorcontrib><creatorcontrib>ZUO BOJUN</creatorcontrib><creatorcontrib>HAN JINTAO</creatorcontrib><creatorcontrib>XIE YINPING</creatorcontrib><creatorcontrib>DONG WENKAI</creatorcontrib><creatorcontrib>LI XUKUN</creatorcontrib><creatorcontrib>WANG MINGGANG</creatorcontrib><creatorcontrib>JIANG AIZHONG</creatorcontrib><creatorcontrib>WANG YINGXIU</creatorcontrib><creatorcontrib>LI LEI</creatorcontrib><collection>esp@cenet</collection></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext_linktorsrc</fulltext></delivery><addata><au>LIU JUN</au><au>CHAI HONGWEI</au><au>ZUO BOJUN</au><au>HAN JINTAO</au><au>XIE YINPING</au><au>DONG WENKAI</au><au>LI XUKUN</au><au>WANG MINGGANG</au><au>JIANG AIZHONG</au><au>WANG YINGXIU</au><au>LI LEI</au><format>patent</format><genre>patent</genre><ristype>GEN</ristype><title>Glufosinate-phosphonic acid hydrate single crystal and preparation method thereof</title><date>2019-11-12</date><risdate>2019</risdate><abstract>The invention discloses a glufosinate-phosphonic acid hydrate single crystal and a preparation method thereof. The glufosinate-phosphonic acid hydrate single crystal belongs to an orthorhombic system,and has a space group of P2 2 2 , and the following cell parameters: alpha=90 degrees, beta=90 degrees and gamma=90 degrees, the unit cell volume is that 4 molecules of glufosinate-phosphonic acid and 4 molecules of water contained in per unit cell. The preparation method comprises the following steps: dissolving the glufosinate-phosphonic acid into a solvent, performing cooling, allowing the cooled solution to stand, slowly evaporating the solvent, and performing crystallization to obtain the glufosinate-phosphonic acid hydrate single crystal. The glufosinate-phosphonic acid hydrate single crystal provided by the invention belongs to the orthorhombic system and is a novel monohydrate crystal different from a current technology, and the preparation method is simple and has a green and environmentally-friendly pre</abstract><oa>free_for_read</oa></addata></record> |
| fulltext | fulltext_linktorsrc |
| identifier | |
| ispartof | |
| issn | |
| language | chi ; eng |
| recordid | cdi_epo_espacenet_CN110437276A |
| source | esp@cenet |
| subjects | ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAININGELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN,SULFUR, SELENIUM OR TELLURIUM CHEMISTRY METALLURGY ORGANIC CHEMISTRY |
| title | Glufosinate-phosphonic acid hydrate single crystal and preparation method thereof |
| url | https://sfx.bib-bvb.de/sfx_tum?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2025-01-24T23%3A27%3A54IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-epo_EVB&rft_val_fmt=info:ofi/fmt:kev:mtx:patent&rft.genre=patent&rft.au=LIU%20JUN&rft.date=2019-11-12&rft_id=info:doi/&rft_dat=%3Cepo_EVB%3ECN110437276A%3C/epo_EVB%3E%3Curl%3E%3C/url%3E&disable_directlink=true&sfx.directlink=off&sfx.report_link=0&rft_id=info:oai/&rft_id=info:pmid/&rfr_iscdi=true |