Biphenyl compound, and preparation method and application thereof
The invention discloses a biphenyl compound, and a preparation method and application thereof. The compound has a structure as shown in a formula (I) in the specification. The preparation method of the compound comprises the steps of reacting 4'-chloro-2-aminobiphenyl as a starting material wit...
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creator | WANG WEI ZHENG XIAORUI WANG LIEPING NING BINKE LIU KANGYUN ZHANG YUANYUAN HUANG XIAOYING ZHANG XIAOGUANG ZHANG JIANGONG |
description | The invention discloses a biphenyl compound, and a preparation method and application thereof. The compound has a structure as shown in a formula (I) in the specification. The preparation method of the compound comprises the steps of reacting 4'-chloro-2-aminobiphenyl as a starting material with substituted formyl chloride in solvent at a temperature of 20 DEG C to 120 DEG C under alkaline conditions to prepare the compound (I). The compound can be used as an active ingredient to prepare a pesticide bactericide, and has an 80% inhibition rate on Rhizoctonia solani, Botrytis cinerea and Alternaria solani at a dose of 50 [mu]g/L.
本发明公开了种联苯类化合物及制备方法和应用,该化合物结构如式(I)所示。其制备方法为以4′-氯-2-胺基联苯为起始原料与取代甲酰氯在溶剂中于20℃~120℃,在碱性条件下反应制得该化合物(I);该化合物可作为活性成分制备农药杀菌剂,在50μg/L剂量下对成立枯丝核菌、灰霉病菌和茄链格孢菌都有80%的抑制率。 |
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本发明公开了种联苯类化合物及制备方法和应用,该化合物结构如式(I)所示。其制备方法为以4′-氯-2-胺基联苯为起始原料与取代甲酰氯在溶剂中于20℃~120℃,在碱性条件下反应制得该化合物(I);该化合物可作为活性成分制备农药杀菌剂,在50μg/L剂量下对成立枯丝核菌、灰霉病菌和茄链格孢菌都有80%的抑制率。</description><language>chi ; eng</language><subject>ACYCLIC OR CARBOCYCLIC COMPOUNDS ; AGRICULTURE ; ANIMAL HUSBANDRY ; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES, AS HERBICIDES ; CHEMISTRY ; FISHING ; FORESTRY ; HETEROCYCLIC COMPOUNDS ; HUMAN NECESSITIES ; HUNTING ; METALLURGY ; ORGANIC CHEMISTRY ; PEST REPELLANTS OR ATTRACTANTS ; PLANT GROWTH REGULATORS ; PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTSTHEREOF ; TRAPPING</subject><creationdate>2019</creationdate><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&date=20190402&DB=EPODOC&CC=CN&NR=109553578A$$EHTML$$P50$$Gepo$$Hfree_for_read</linktohtml><link.rule.ids>230,308,780,885,25564,76547</link.rule.ids><linktorsrc>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&date=20190402&DB=EPODOC&CC=CN&NR=109553578A$$EView_record_in_European_Patent_Office$$FView_record_in_$$GEuropean_Patent_Office$$Hfree_for_read</linktorsrc></links><search><creatorcontrib>WANG WEI</creatorcontrib><creatorcontrib>ZHENG XIAORUI</creatorcontrib><creatorcontrib>WANG LIEPING</creatorcontrib><creatorcontrib>NING BINKE</creatorcontrib><creatorcontrib>LIU KANGYUN</creatorcontrib><creatorcontrib>ZHANG YUANYUAN</creatorcontrib><creatorcontrib>HUANG XIAOYING</creatorcontrib><creatorcontrib>ZHANG XIAOGUANG</creatorcontrib><creatorcontrib>ZHANG JIANGONG</creatorcontrib><title>Biphenyl compound, and preparation method and application thereof</title><description>The invention discloses a biphenyl compound, and a preparation method and application thereof. The compound has a structure as shown in a formula (I) in the specification. The preparation method of the compound comprises the steps of reacting 4'-chloro-2-aminobiphenyl as a starting material with substituted formyl chloride in solvent at a temperature of 20 DEG C to 120 DEG C under alkaline conditions to prepare the compound (I). The compound can be used as an active ingredient to prepare a pesticide bactericide, and has an 80% inhibition rate on Rhizoctonia solani, Botrytis cinerea and Alternaria solani at a dose of 50 [mu]g/L.
本发明公开了种联苯类化合物及制备方法和应用,该化合物结构如式(I)所示。其制备方法为以4′-氯-2-胺基联苯为起始原料与取代甲酰氯在溶剂中于20℃~120℃,在碱性条件下反应制得该化合物(I);该化合物可作为活性成分制备农药杀菌剂,在50μg/L剂量下对成立枯丝核菌、灰霉病菌和茄链格孢菌都有80%的抑制率。</description><subject>ACYCLIC OR CARBOCYCLIC COMPOUNDS</subject><subject>AGRICULTURE</subject><subject>ANIMAL HUSBANDRY</subject><subject>BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES, AS HERBICIDES</subject><subject>CHEMISTRY</subject><subject>FISHING</subject><subject>FORESTRY</subject><subject>HETEROCYCLIC COMPOUNDS</subject><subject>HUMAN NECESSITIES</subject><subject>HUNTING</subject><subject>METALLURGY</subject><subject>ORGANIC CHEMISTRY</subject><subject>PEST REPELLANTS OR ATTRACTANTS</subject><subject>PLANT GROWTH REGULATORS</subject><subject>PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTSTHEREOF</subject><subject>TRAPPING</subject><fulltext>true</fulltext><rsrctype>patent</rsrctype><creationdate>2019</creationdate><recordtype>patent</recordtype><sourceid>EVB</sourceid><recordid>eNrjZHB0yizISM2rzFFIzs8tyC_NS9FRSMxLUSgoSi1ILEosyczPU8hNLcnITwELJxYU5GQmQ4RLMlKLUvPTeBhY0xJzilN5oTQ3g6Kba4izh25qQX58anFBYnJqXmpJvLOfoYGlqamxqbmFozExagAcdzH3</recordid><startdate>20190402</startdate><enddate>20190402</enddate><creator>WANG WEI</creator><creator>ZHENG XIAORUI</creator><creator>WANG LIEPING</creator><creator>NING BINKE</creator><creator>LIU KANGYUN</creator><creator>ZHANG YUANYUAN</creator><creator>HUANG XIAOYING</creator><creator>ZHANG XIAOGUANG</creator><creator>ZHANG JIANGONG</creator><scope>EVB</scope></search><sort><creationdate>20190402</creationdate><title>Biphenyl compound, and preparation method and application thereof</title><author>WANG WEI ; ZHENG XIAORUI ; WANG LIEPING ; NING BINKE ; LIU KANGYUN ; ZHANG YUANYUAN ; HUANG XIAOYING ; ZHANG XIAOGUANG ; ZHANG JIANGONG</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-epo_espacenet_CN109553578A3</frbrgroupid><rsrctype>patents</rsrctype><prefilter>patents</prefilter><language>chi ; eng</language><creationdate>2019</creationdate><topic>ACYCLIC OR CARBOCYCLIC COMPOUNDS</topic><topic>AGRICULTURE</topic><topic>ANIMAL HUSBANDRY</topic><topic>BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES, AS HERBICIDES</topic><topic>CHEMISTRY</topic><topic>FISHING</topic><topic>FORESTRY</topic><topic>HETEROCYCLIC COMPOUNDS</topic><topic>HUMAN NECESSITIES</topic><topic>HUNTING</topic><topic>METALLURGY</topic><topic>ORGANIC CHEMISTRY</topic><topic>PEST REPELLANTS OR ATTRACTANTS</topic><topic>PLANT GROWTH REGULATORS</topic><topic>PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTSTHEREOF</topic><topic>TRAPPING</topic><toplevel>online_resources</toplevel><creatorcontrib>WANG WEI</creatorcontrib><creatorcontrib>ZHENG XIAORUI</creatorcontrib><creatorcontrib>WANG LIEPING</creatorcontrib><creatorcontrib>NING BINKE</creatorcontrib><creatorcontrib>LIU KANGYUN</creatorcontrib><creatorcontrib>ZHANG YUANYUAN</creatorcontrib><creatorcontrib>HUANG XIAOYING</creatorcontrib><creatorcontrib>ZHANG XIAOGUANG</creatorcontrib><creatorcontrib>ZHANG JIANGONG</creatorcontrib><collection>esp@cenet</collection></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext_linktorsrc</fulltext></delivery><addata><au>WANG WEI</au><au>ZHENG XIAORUI</au><au>WANG LIEPING</au><au>NING BINKE</au><au>LIU KANGYUN</au><au>ZHANG YUANYUAN</au><au>HUANG XIAOYING</au><au>ZHANG XIAOGUANG</au><au>ZHANG JIANGONG</au><format>patent</format><genre>patent</genre><ristype>GEN</ristype><title>Biphenyl compound, and preparation method and application thereof</title><date>2019-04-02</date><risdate>2019</risdate><abstract>The invention discloses a biphenyl compound, and a preparation method and application thereof. The compound has a structure as shown in a formula (I) in the specification. The preparation method of the compound comprises the steps of reacting 4'-chloro-2-aminobiphenyl as a starting material with substituted formyl chloride in solvent at a temperature of 20 DEG C to 120 DEG C under alkaline conditions to prepare the compound (I). The compound can be used as an active ingredient to prepare a pesticide bactericide, and has an 80% inhibition rate on Rhizoctonia solani, Botrytis cinerea and Alternaria solani at a dose of 50 [mu]g/L.
本发明公开了种联苯类化合物及制备方法和应用,该化合物结构如式(I)所示。其制备方法为以4′-氯-2-胺基联苯为起始原料与取代甲酰氯在溶剂中于20℃~120℃,在碱性条件下反应制得该化合物(I);该化合物可作为活性成分制备农药杀菌剂,在50μg/L剂量下对成立枯丝核菌、灰霉病菌和茄链格孢菌都有80%的抑制率。</abstract><oa>free_for_read</oa></addata></record> |
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subjects | ACYCLIC OR CARBOCYCLIC COMPOUNDS AGRICULTURE ANIMAL HUSBANDRY BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES, AS HERBICIDES CHEMISTRY FISHING FORESTRY HETEROCYCLIC COMPOUNDS HUMAN NECESSITIES HUNTING METALLURGY ORGANIC CHEMISTRY PEST REPELLANTS OR ATTRACTANTS PLANT GROWTH REGULATORS PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTSTHEREOF TRAPPING |
title | Biphenyl compound, and preparation method and application thereof |
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