Extraction method of polycyclic aromatic hydrocarbons in PBT/PET product

The invention discloses an extraction method of polycyclic aromatic hydrocarbons in a PBT/PET product. The extraction method comprises the following steps of a, crushing the PBT or PET product into particles; b, weighing a preset amount of the crushed PBT or PET particle sample, putting the crushed...

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Bibliographische Detailangaben
Hauptverfasser: XIA JIE, JIANG CHENZHOU, FU JIAPING, ZHANG CHIZHONG, ZHU YI
Format: Patent
Sprache:chi ; eng
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Zusammenfassung:The invention discloses an extraction method of polycyclic aromatic hydrocarbons in a PBT/PET product. The extraction method comprises the following steps of a, crushing the PBT or PET product into particles; b, weighing a preset amount of the crushed PBT or PET particle sample, putting the crushed PBT or PET particle sample in a headspace jaw bottle, adding 98 percent concentrated sulfuric acid and a 2,5-di-tert-butyl hydroquinone solution with the mass percent concentration being 10 percent, and performing ultrasonic dissolution under a 35-45 DEG C water bath to obtain a first sample to be treated; and c, mixing water, acetonitrile, cyclohexane and an SCX filler, rapidly adding a mixture in the first sample to be treated, performing vortex mixing, and centrifugally extracting an upper layer organic phase. The extraction method provided by the invention has the characteristics of rapidness, simpleness, convenience, low cost, less interference, small loss to instrument and the like. 本发明公开了种PBT/PET制品中多环芳烃的提取方法