Preparation method of immobilized catalytic particle metal felt for producing biodiesel
The invention discloses a preparation method of an immobilized catalytic particle metal felt for producing biodiesel, aiming at solving the problems of an existing catalyst that the stability is poor,the service life is short and the catalytic efficiency is low. The preparation method comprises the...
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| creator | SHI WENYING LI HONGBIN SUN MAOWEN QIN LONGWEI |
| description | The invention discloses a preparation method of an immobilized catalytic particle metal felt for producing biodiesel, aiming at solving the problems of an existing catalyst that the stability is poor,the service life is short and the catalytic efficiency is low. The preparation method comprises the following steps: carrying out ultrasonic washing on the metal felt with absolute ethyl alcohol andwater, and drying; preparing ZrOCl2.8H2O and nitrate into a mixed water solution; stirring and adding ammonia water until the pH (Potential of Hydrogen) is 9 to 10, so as to obtain flocculent sediment; standing at room temperature; then filtering and washing until no Cl exists so as to obtain a filter cake; drying and grinding to obtain a powdered material; adding the powdered material into anH2SO4 solution to form a mixture; adding the dried metal felt into the mixture; after immersing, drying; roasting under an inert atmosphere at 400 to 600 DEG C for 3 to 7h to obtain the immobilized catalytic particle metal felt |
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The preparation method comprises the following steps: carrying out ultrasonic washing on the metal felt with absolute ethyl alcohol andwater, and drying; preparing ZrOCl2.8H2O and nitrate into a mixed water solution; stirring and adding ammonia water until the pH (Potential of Hydrogen) is 9 to 10, so as to obtain flocculent sediment; standing at room temperature; then filtering and washing until no Cl<-> exists so as to obtain a filter cake; drying and grinding to obtain a powdered material; adding the powdered material into anH2SO4 solution to form a mixture; adding the dried metal felt into the mixture; after immersing, drying; roasting under an inert atmosphere at 400 to 600 DEG C for 3 to 7h to obtain the immobilized catalytic particle metal felt</description><language>chi ; eng</language><subject>ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE ORUNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL ; ANIMAL AND VEGETABLE OILS, FATS, FATTY SUBSTANCES AND WAXES ; CANDLES ; CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOIDCHEMISTRY ; CHEMISTRY ; DETERGENTS ; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS,OILS, OR FATTY ACIDS OBTAINED THEREFROM ; FATTY ACIDS FROM FATS, OILS OR WAXES ; FATTY ACIDS THEREFROM ; FIRELIGHTERS ; FUELS ; FUELS NOT OTHERWISE PROVIDED FOR ; LIQUEFIED PETROLEUM GAS ; LUBRICANTS ; METALLURGY ; NATURAL GAS ; PEAT ; PERFORMING OPERATIONS ; PETROLEUM, GAS OR COKE INDUSTRIES ; PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL ; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BYSUBCLASSES C10G, C10K ; TECHNICAL GASES CONTAINING CARBON MONOXIDE ; THEIR RELEVANT APPARATUS ; TRANSPORTING</subject><creationdate>2018</creationdate><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&date=20180629&DB=EPODOC&CC=CN&NR=108212179A$$EHTML$$P50$$Gepo$$Hfree_for_read</linktohtml><link.rule.ids>230,308,780,885,25564,76547</link.rule.ids><linktorsrc>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&date=20180629&DB=EPODOC&CC=CN&NR=108212179A$$EView_record_in_European_Patent_Office$$FView_record_in_$$GEuropean_Patent_Office$$Hfree_for_read</linktorsrc></links><search><creatorcontrib>SHI WENYING</creatorcontrib><creatorcontrib>LI HONGBIN</creatorcontrib><creatorcontrib>SUN MAOWEN</creatorcontrib><creatorcontrib>QIN LONGWEI</creatorcontrib><title>Preparation method of immobilized catalytic particle metal felt for producing biodiesel</title><description>The invention discloses a preparation method of an immobilized catalytic particle metal felt for producing biodiesel, aiming at solving the problems of an existing catalyst that the stability is poor,the service life is short and the catalytic efficiency is low. The preparation method comprises the following steps: carrying out ultrasonic washing on the metal felt with absolute ethyl alcohol andwater, and drying; preparing ZrOCl2.8H2O and nitrate into a mixed water solution; stirring and adding ammonia water until the pH (Potential of Hydrogen) is 9 to 10, so as to obtain flocculent sediment; standing at room temperature; then filtering and washing until no Cl<-> exists so as to obtain a filter cake; drying and grinding to obtain a powdered material; adding the powdered material into anH2SO4 solution to form a mixture; adding the dried metal felt into the mixture; after immersing, drying; roasting under an inert atmosphere at 400 to 600 DEG C for 3 to 7h to obtain the immobilized catalytic particle metal felt</description><subject>ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE ORUNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL</subject><subject>ANIMAL AND VEGETABLE OILS, FATS, FATTY SUBSTANCES AND WAXES</subject><subject>CANDLES</subject><subject>CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOIDCHEMISTRY</subject><subject>CHEMISTRY</subject><subject>DETERGENTS</subject><subject>FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS,OILS, OR FATTY ACIDS OBTAINED THEREFROM</subject><subject>FATTY ACIDS FROM FATS, OILS OR WAXES</subject><subject>FATTY ACIDS THEREFROM</subject><subject>FIRELIGHTERS</subject><subject>FUELS</subject><subject>FUELS NOT OTHERWISE PROVIDED FOR</subject><subject>LIQUEFIED PETROLEUM GAS</subject><subject>LUBRICANTS</subject><subject>METALLURGY</subject><subject>NATURAL GAS</subject><subject>PEAT</subject><subject>PERFORMING OPERATIONS</subject><subject>PETROLEUM, GAS OR COKE INDUSTRIES</subject><subject>PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL</subject><subject>SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BYSUBCLASSES C10G, C10K</subject><subject>TECHNICAL GASES CONTAINING CARBON MONOXIDE</subject><subject>THEIR RELEVANT APPARATUS</subject><subject>TRANSPORTING</subject><fulltext>true</fulltext><rsrctype>patent</rsrctype><creationdate>2018</creationdate><recordtype>patent</recordtype><sourceid>EVB</sourceid><recordid>eNqNyrEKwjAQANAsDqL-w_kBgqmDOkpRnMRBcCzX5FIPLr2QxkG_3gp-gNNb3tTcr5kSZiysPUQqD_WgAThGbVn4TR4cFpRXYQdjHBH6RhQIJAWCZkhZ_dNx30HL6pkGkrmZBJSBFj9nZnk63urzipI2NCR01FNp6otd7ypb2e3-sPnnfACuDDp-</recordid><startdate>20180629</startdate><enddate>20180629</enddate><creator>SHI WENYING</creator><creator>LI HONGBIN</creator><creator>SUN MAOWEN</creator><creator>QIN LONGWEI</creator><scope>EVB</scope></search><sort><creationdate>20180629</creationdate><title>Preparation method of immobilized catalytic particle metal felt for producing biodiesel</title><author>SHI WENYING ; 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The preparation method comprises the following steps: carrying out ultrasonic washing on the metal felt with absolute ethyl alcohol andwater, and drying; preparing ZrOCl2.8H2O and nitrate into a mixed water solution; stirring and adding ammonia water until the pH (Potential of Hydrogen) is 9 to 10, so as to obtain flocculent sediment; standing at room temperature; then filtering and washing until no Cl<-> exists so as to obtain a filter cake; drying and grinding to obtain a powdered material; adding the powdered material into anH2SO4 solution to form a mixture; adding the dried metal felt into the mixture; after immersing, drying; roasting under an inert atmosphere at 400 to 600 DEG C for 3 to 7h to obtain the immobilized catalytic particle metal felt</abstract><oa>free_for_read</oa></addata></record> |
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| subjects | ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE ORUNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL ANIMAL AND VEGETABLE OILS, FATS, FATTY SUBSTANCES AND WAXES CANDLES CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOIDCHEMISTRY CHEMISTRY DETERGENTS FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS,OILS, OR FATTY ACIDS OBTAINED THEREFROM FATTY ACIDS FROM FATS, OILS OR WAXES FATTY ACIDS THEREFROM FIRELIGHTERS FUELS FUELS NOT OTHERWISE PROVIDED FOR LIQUEFIED PETROLEUM GAS LUBRICANTS METALLURGY NATURAL GAS PEAT PERFORMING OPERATIONS PETROLEUM, GAS OR COKE INDUSTRIES PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BYSUBCLASSES C10G, C10K TECHNICAL GASES CONTAINING CARBON MONOXIDE THEIR RELEVANT APPARATUS TRANSPORTING |
| title | Preparation method of immobilized catalytic particle metal felt for producing biodiesel |
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