Blue MOFs/cast nylon nanometer composite material as well as preparation method and application thereof
The invention discloses a blue MOFs/cast nylon nanometer composite material as well as a preparation method and application thereof. The preparation method comprises the following steps: adding blue MOF and an aprotic polar solvent into a kettle A contained with caprolactam monomers, heating to the...
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| creator | LIU XIAOCHAO LAI DENGWANG LI YUHUA LIU YUEJUN YANG JUN ZHAO TIAN |
| description | The invention discloses a blue MOFs/cast nylon nanometer composite material as well as a preparation method and application thereof. The preparation method comprises the following steps: adding blue MOF and an aprotic polar solvent into a kettle A contained with caprolactam monomers, heating to the temperature of 70-85 DEG C, stirring for 0.5-2 hours, vacuumizing for 15-60 minutes, heating to the temperature of 130-140 DEG C, and adding an initiator for carrying out a vacuum reaction for 15-30 minutes; heating a kettle B filled with caprolactam monomers, heating to a dissolved state, vacuumizing, totally melting the monomers, adding a catalyst, heating to the temperature of 130-140 DEG C, and vacuumizing for 10-15 minutes; and finally, mixing the kettle A and the kettle B, pouring into a mold of 150-170 DEG C for performing polymerization molding, maintaining the temperature of 10-60 minutes, and demolding. By utilizing the color of blue MOFs and the frame structure, the blue MOFs and nylon matrix have a phys |
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The preparation method comprises the following steps: adding blue MOF and an aprotic polar solvent into a kettle A contained with caprolactam monomers, heating to the temperature of 70-85 DEG C, stirring for 0.5-2 hours, vacuumizing for 15-60 minutes, heating to the temperature of 130-140 DEG C, and adding an initiator for carrying out a vacuum reaction for 15-30 minutes; heating a kettle B filled with caprolactam monomers, heating to a dissolved state, vacuumizing, totally melting the monomers, adding a catalyst, heating to the temperature of 130-140 DEG C, and vacuumizing for 10-15 minutes; and finally, mixing the kettle A and the kettle B, pouring into a mold of 150-170 DEG C for performing polymerization molding, maintaining the temperature of 10-60 minutes, and demolding. 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| subjects | CHEMISTRY COMPOSITIONS BASED THEREON COMPOSITIONS OF MACROMOLECULAR COMPOUNDS MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONSONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS METALLURGY ORGANIC MACROMOLECULAR COMPOUNDS THEIR PREPARATION OR CHEMICAL WORKING-UP |
| title | Blue MOFs/cast nylon nanometer composite material as well as preparation method and application thereof |
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