Silver/gold nanometer cavity dendritic crystal containing interior label molecule, preparation method and application thereof
The invention relates to a silver/gold nanometer cavity dendritic crystal containing an interior label molecule, a preparation method and an application thereof. The preparation steps are as follows: alternately ultrasonic washing a copper simple substance with ethyl alcohol and pure water for 3-5 t...
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Format: | Patent |
Sprache: | chi ; eng |
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Zusammenfassung: | The invention relates to a silver/gold nanometer cavity dendritic crystal containing an interior label molecule, a preparation method and an application thereof. The preparation steps are as follows: alternately ultrasonic washing a copper simple substance with ethyl alcohol and pure water for 3-5 times, and then blowing with a nitrogen flow, putting into a beaker for later use; adding excessive silver nitrate solution, stirring, reacting and ageing; centrifugally cleaning the reaction products and ultrasonically dispersing in a PVP solution; adding the interior label molecule containing nitrogen and sulfur atoms; performing oscillatory reaction, thereby acquiring a silver dendritic crystal with a micro-nano structure; centrifugally cleaning and then re-dispersing in the PVP solution; adding aqueous alkali for regulating pH; and lastly, adding into a growth solution and reacting, thereby acquiring the silver/gold nanometer cavity dendritic crystal containing an interior label molecule. The preparation of the |
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