Preparation method of beta-tricalcium phosphate nanometer coating
The invention discloses a preparation method of a beta-tricalcium phosphate nanometer coating. The preparation method comprises the following steps: (1) adding dispersant in a calcium source solution, uniformly stirring, adding a phosphorus source solution dropwise, and continuously stirring, ageing...
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creator | DENG CHUNLIN PANG DONGWEN |
description | The invention discloses a preparation method of a beta-tricalcium phosphate nanometer coating. The preparation method comprises the following steps: (1) adding dispersant in a calcium source solution, uniformly stirring, adding a phosphorus source solution dropwise, and continuously stirring, ageing, filtering, washing, freezing, drying and calcining the mixture to obtain a beta-tricalcium phosphate powder; (2) adding the prepared beta-tricalcium phosphate powder in ethanol, carrying out ball milling and standing to prepare a stable beta-tricalcium phosphate suspension; and (3) taking a gold sheet as a working electrode, a platinum electrode as a counter electrode and the beta-tricalcium phosphate suspension as an electrolyte, applying direct current between the electrodes, and carrying out electrophoretic deposition on the surface of the gold sheet to obtain the beta-tricalcium phosphate nanometer coating. According to the preparation method, phase change and embrittlement caused in the high temperature proc |
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The preparation method comprises the following steps: (1) adding dispersant in a calcium source solution, uniformly stirring, adding a phosphorus source solution dropwise, and continuously stirring, ageing, filtering, washing, freezing, drying and calcining the mixture to obtain a beta-tricalcium phosphate powder; (2) adding the prepared beta-tricalcium phosphate powder in ethanol, carrying out ball milling and standing to prepare a stable beta-tricalcium phosphate suspension; and (3) taking a gold sheet as a working electrode, a platinum electrode as a counter electrode and the beta-tricalcium phosphate suspension as an electrolyte, applying direct current between the electrodes, and carrying out electrophoretic deposition on the surface of the gold sheet to obtain the beta-tricalcium phosphate nanometer coating. According to the preparation method, phase change and embrittlement caused in the high temperature proc</description><language>chi ; eng</language><subject>APPARATUS THEREFOR ; CHEMISTRY ; ELECTROFORMING ; ELECTROLYTIC OR ELECTROPHORETIC PROCESSES ; METALLURGY ; PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTIONOF COATINGS</subject><creationdate>2017</creationdate><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&date=20170426&DB=EPODOC&CC=CN&NR=106591923A$$EHTML$$P50$$Gepo$$Hfree_for_read</linktohtml><link.rule.ids>230,308,777,882,25545,76296</link.rule.ids><linktorsrc>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&date=20170426&DB=EPODOC&CC=CN&NR=106591923A$$EView_record_in_European_Patent_Office$$FView_record_in_$$GEuropean_Patent_Office$$Hfree_for_read</linktorsrc></links><search><creatorcontrib>DENG CHUNLIN</creatorcontrib><creatorcontrib>PANG DONGWEN</creatorcontrib><title>Preparation method of beta-tricalcium phosphate nanometer coating</title><description>The invention discloses a preparation method of a beta-tricalcium phosphate nanometer coating. The preparation method comprises the following steps: (1) adding dispersant in a calcium source solution, uniformly stirring, adding a phosphorus source solution dropwise, and continuously stirring, ageing, filtering, washing, freezing, drying and calcining the mixture to obtain a beta-tricalcium phosphate powder; (2) adding the prepared beta-tricalcium phosphate powder in ethanol, carrying out ball milling and standing to prepare a stable beta-tricalcium phosphate suspension; and (3) taking a gold sheet as a working electrode, a platinum electrode as a counter electrode and the beta-tricalcium phosphate suspension as an electrolyte, applying direct current between the electrodes, and carrying out electrophoretic deposition on the surface of the gold sheet to obtain the beta-tricalcium phosphate nanometer coating. 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The preparation method comprises the following steps: (1) adding dispersant in a calcium source solution, uniformly stirring, adding a phosphorus source solution dropwise, and continuously stirring, ageing, filtering, washing, freezing, drying and calcining the mixture to obtain a beta-tricalcium phosphate powder; (2) adding the prepared beta-tricalcium phosphate powder in ethanol, carrying out ball milling and standing to prepare a stable beta-tricalcium phosphate suspension; and (3) taking a gold sheet as a working electrode, a platinum electrode as a counter electrode and the beta-tricalcium phosphate suspension as an electrolyte, applying direct current between the electrodes, and carrying out electrophoretic deposition on the surface of the gold sheet to obtain the beta-tricalcium phosphate nanometer coating. According to the preparation method, phase change and embrittlement caused in the high temperature proc</abstract><oa>free_for_read</oa></addata></record> |
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subjects | APPARATUS THEREFOR CHEMISTRY ELECTROFORMING ELECTROLYTIC OR ELECTROPHORETIC PROCESSES METALLURGY PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTIONOF COATINGS |
title | Preparation method of beta-tricalcium phosphate nanometer coating |
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