Meso-tetrakis(3,4-dioxoacetoethylphenyl)porphyrin and preparation method thereof
The invention discloses Meso-tetrakis(3,4-dioxoacetoethylphenyl)porphyrin and a preparation method thereof, and relates to the technical field of chemical synthesis and detection. According to the Meso-tetrakis(3,4-dioxoacetoethylphenyl)porphyrin preparation method provided by the invention, the fol...
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| creator | YUAN JIAN CHEN XIAOTING TONG SHANLING YAN YAN WU YAHONG YE FEI LIN HUI |
| description | The invention discloses Meso-tetrakis(3,4-dioxoacetoethylphenyl)porphyrin and a preparation method thereof, and relates to the technical field of chemical synthesis and detection. According to the Meso-tetrakis(3,4-dioxoacetoethylphenyl)porphyrin preparation method provided by the invention, the following raw materials are adopted: 1.5g of 3,4-dihydroxybenzaldehyde, 1.3mL of pyrrole, 80mL of nitrobenzene, 7.5mL of isobutyric acid, 0.149g of potassium carbonate, 0.22g of tetrabutylammonium bromide, 35mL of THF, and 0.71mL of ethyl chloroacetate. The Meso-tetrakis(3,4-dioxoacetoethylphenyl)porphyrin preparation method provided by the invention is simple, and the yield of obtained Meso-tetrakis(3,4-dioxoacetoethylphenyl)porphyrin is high.
本发明公开了种Meso-四(3,4-二氧乙酸乙酯基苯基)卟啉及其制备方法，属于化学合成与检测技术领域。本发明的Meso-四(3,4-二氧乙酸乙酯基苯基)卟啉的制备方法，采用的原料比例为：3,4-二羟基苯甲醛1.5g；吡咯1.3mL；硝基苯80mL；异丁酸7.5mL；碳酸钾0.149g、四丁基溴化铵0.22g；THF 35mL；氯乙酸乙酯0.71mL。本发明提供了的Meso-四(3,4-二氧乙酸乙酯基苯基)卟啉的制备方法简单，获得的Meso-四(3,4-二氧乙酸乙酯基苯基)卟啉的收率高。 |
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本发明公开了种Meso-四(3,4-二氧乙酸乙酯基苯基)卟啉及其制备方法，属于化学合成与检测技术领域。本发明的Meso-四(3,4-二氧乙酸乙酯基苯基)卟啉的制备方法，采用的原料比例为：3,4-二羟基苯甲醛1.5g；吡咯1.3mL；硝基苯80mL；异丁酸7.5mL；碳酸钾0.149g、四丁基溴化铵0.22g；THF 35mL；氯乙酸乙酯0.71mL。本发明提供了的Meso-四(3,4-二氧乙酸乙酯基苯基)卟啉的制备方法简单，获得的Meso-四(3,4-二氧乙酸乙酯基苯基)卟啉的收率高。</description><language>chi ; eng</language><subject>CHEMISTRY ; HETEROCYCLIC COMPOUNDS ; METALLURGY ; ORGANIC CHEMISTRY</subject><creationdate>2017</creationdate><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&date=20170215&DB=EPODOC&CC=CN&NR=106397447A$$EHTML$$P50$$Gepo$$Hfree_for_read</linktohtml><link.rule.ids>230,308,776,881,25542,76289</link.rule.ids><linktorsrc>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&date=20170215&DB=EPODOC&CC=CN&NR=106397447A$$EView_record_in_European_Patent_Office$$FView_record_in_$$GEuropean_Patent_Office$$Hfree_for_read</linktorsrc></links><search><creatorcontrib>YUAN JIAN</creatorcontrib><creatorcontrib>CHEN XIAOTING</creatorcontrib><creatorcontrib>TONG SHANLING</creatorcontrib><creatorcontrib>YAN YAN</creatorcontrib><creatorcontrib>WU YAHONG</creatorcontrib><creatorcontrib>YE FEI</creatorcontrib><creatorcontrib>LIN HUI</creatorcontrib><title>Meso-tetrakis(3,4-dioxoacetoethylphenyl)porphyrin and preparation method thereof</title><description>The invention discloses Meso-tetrakis(3,4-dioxoacetoethylphenyl)porphyrin and a preparation method thereof, and relates to the technical field of chemical synthesis and detection. According to the Meso-tetrakis(3,4-dioxoacetoethylphenyl)porphyrin preparation method provided by the invention, the following raw materials are adopted: 1.5g of 3,4-dihydroxybenzaldehyde, 1.3mL of pyrrole, 80mL of nitrobenzene, 7.5mL of isobutyric acid, 0.149g of potassium carbonate, 0.22g of tetrabutylammonium bromide, 35mL of THF, and 0.71mL of ethyl chloroacetate. The Meso-tetrakis(3,4-dioxoacetoethylphenyl)porphyrin preparation method provided by the invention is simple, and the yield of obtained Meso-tetrakis(3,4-dioxoacetoethylphenyl)porphyrin is high.
本发明公开了种Meso-四(3,4-二氧乙酸乙酯基苯基)卟啉及其制备方法，属于化学合成与检测技术领域。本发明的Meso-四(3,4-二氧乙酸乙酯基苯基)卟啉的制备方法，采用的原料比例为：3,4-二羟基苯甲醛1.5g；吡咯1.3mL；硝基苯80mL；异丁酸7.5mL；碳酸钾0.149g、四丁基溴化铵0.22g；THF 35mL；氯乙酸乙酯0.71mL。本发明提供了的Meso-四(3,4-二氧乙酸乙酯基苯基)卟啉的制备方法简单，获得的Meso-四(3,4-二氧乙酸乙酯基苯基)卟啉的收率高。</description><subject>CHEMISTRY</subject><subject>HETEROCYCLIC COMPOUNDS</subject><subject>METALLURGY</subject><subject>ORGANIC CHEMISTRY</subject><fulltext>true</fulltext><rsrctype>patent</rsrctype><creationdate>2017</creationdate><recordtype>patent</recordtype><sourceid>EVB</sourceid><recordid>eNqNzDEKAjEQQNFtLES9Q-wUDCgJLpayKDaKhf0ymFkSjJkhmcLc3i08gNVvHn_a3K9YSAtKhlcoK7Ox2gX6EDxRCMXXyB5TjWumzL7mkBQkpzgjQwYJlNR7ZOSUeMxIw7yZDBALLn6dNcvz6dFdNDL1WHgcJ5S-u-22e3NorW2P5h_zBefxOBg</recordid><startdate>20170215</startdate><enddate>20170215</enddate><creator>YUAN JIAN</creator><creator>CHEN XIAOTING</creator><creator>TONG SHANLING</creator><creator>YAN YAN</creator><creator>WU YAHONG</creator><creator>YE FEI</creator><creator>LIN HUI</creator><scope>EVB</scope></search><sort><creationdate>20170215</creationdate><title>Meso-tetrakis(3,4-dioxoacetoethylphenyl)porphyrin and preparation method thereof</title><author>YUAN JIAN ; CHEN XIAOTING ; TONG SHANLING ; YAN YAN ; WU YAHONG ; YE FEI ; LIN HUI</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-epo_espacenet_CN106397447A3</frbrgroupid><rsrctype>patents</rsrctype><prefilter>patents</prefilter><language>chi ; eng</language><creationdate>2017</creationdate><topic>CHEMISTRY</topic><topic>HETEROCYCLIC COMPOUNDS</topic><topic>METALLURGY</topic><topic>ORGANIC CHEMISTRY</topic><toplevel>online_resources</toplevel><creatorcontrib>YUAN JIAN</creatorcontrib><creatorcontrib>CHEN XIAOTING</creatorcontrib><creatorcontrib>TONG SHANLING</creatorcontrib><creatorcontrib>YAN YAN</creatorcontrib><creatorcontrib>WU YAHONG</creatorcontrib><creatorcontrib>YE FEI</creatorcontrib><creatorcontrib>LIN HUI</creatorcontrib><collection>esp@cenet</collection></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext_linktorsrc</fulltext></delivery><addata><au>YUAN JIAN</au><au>CHEN XIAOTING</au><au>TONG SHANLING</au><au>YAN YAN</au><au>WU YAHONG</au><au>YE FEI</au><au>LIN HUI</au><format>patent</format><genre>patent</genre><ristype>GEN</ristype><title>Meso-tetrakis(3,4-dioxoacetoethylphenyl)porphyrin and preparation method thereof</title><date>2017-02-15</date><risdate>2017</risdate><abstract>The invention discloses Meso-tetrakis(3,4-dioxoacetoethylphenyl)porphyrin and a preparation method thereof, and relates to the technical field of chemical synthesis and detection. According to the Meso-tetrakis(3,4-dioxoacetoethylphenyl)porphyrin preparation method provided by the invention, the following raw materials are adopted: 1.5g of 3,4-dihydroxybenzaldehyde, 1.3mL of pyrrole, 80mL of nitrobenzene, 7.5mL of isobutyric acid, 0.149g of potassium carbonate, 0.22g of tetrabutylammonium bromide, 35mL of THF, and 0.71mL of ethyl chloroacetate. The Meso-tetrakis(3,4-dioxoacetoethylphenyl)porphyrin preparation method provided by the invention is simple, and the yield of obtained Meso-tetrakis(3,4-dioxoacetoethylphenyl)porphyrin is high.
本发明公开了种Meso-四(3,4-二氧乙酸乙酯基苯基)卟啉及其制备方法，属于化学合成与检测技术领域。本发明的Meso-四(3,4-二氧乙酸乙酯基苯基)卟啉的制备方法，采用的原料比例为：3,4-二羟基苯甲醛1.5g；吡咯1.3mL；硝基苯80mL；异丁酸7.5mL；碳酸钾0.149g、四丁基溴化铵0.22g；THF 35mL；氯乙酸乙酯0.71mL。本发明提供了的Meso-四(3,4-二氧乙酸乙酯基苯基)卟啉的制备方法简单，获得的Meso-四(3,4-二氧乙酸乙酯基苯基)卟啉的收率高。</abstract><oa>free_for_read</oa></addata></record> |
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| title | Meso-tetrakis(3,4-dioxoacetoethylphenyl)porphyrin and preparation method thereof |
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