Composite hydrogen evolution negative pole with micropore hydrogen storage layer and preparing method for composite hydrogen evolution negative pole
The invention discloses a composite hydrogen evolution negative pole with a micropore hydrogen storage layer and a preparing method for the composite hydrogen evolution negative pole. The method includes the steps that (1) base body pretreatment, wherein a base body is subject to alkali soaking and...
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creator | SHEN CHENYAN ZHANG YANFENG HUANG XIAOBIN |
description | The invention discloses a composite hydrogen evolution negative pole with a micropore hydrogen storage layer and a preparing method for the composite hydrogen evolution negative pole. The method includes the steps that (1) base body pretreatment, wherein a base body is subject to alkali soaking and washing, and then sand blasting is carried out; (2) a hydrogen storage middle layer is prepared, wherein the step includes the steps: (2.1) plasma thermal spraying treatment is carried out, a Ni50A150 alloy and hydrogen storage alloy powder are evenly mixed according to the weight ratio being (0.95-0.8): (0.05-0.2), and a plasma spraying device is used for spraying; and (2.2) activating treatment is carried out, the base body treated in the step (2.1) is placed into a first alkaline solution to be soaked, excitation is carried out, and the micropore middle layer with the high specific surface area and the high hydrogen storage performance is obtained; and (3) a thermal decomposition method is adopted for preparing a catalyst layer on the hydrogen storage middle layer. The preparing method is simple and reliable in preparation process, the commercial process is easily achieved; and the prepared composite hydrogen evolution pole has the beneficial effects that the hydrogen evolution catalytic activity is high; during continuous electrolysis, the countercurrent resisting capacity is high, and the service life of the pole is long. |
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The method includes the steps that (1) base body pretreatment, wherein a base body is subject to alkali soaking and washing, and then sand blasting is carried out; (2) a hydrogen storage middle layer is prepared, wherein the step includes the steps: (2.1) plasma thermal spraying treatment is carried out, a Ni50A150 alloy and hydrogen storage alloy powder are evenly mixed according to the weight ratio being (0.95-0.8): (0.05-0.2), and a plasma spraying device is used for spraying; and (2.2) activating treatment is carried out, the base body treated in the step (2.1) is placed into a first alkaline solution to be soaked, excitation is carried out, and the micropore middle layer with the high specific surface area and the high hydrogen storage performance is obtained; and (3) a thermal decomposition method is adopted for preparing a catalyst layer on the hydrogen storage middle layer. The preparing method is simple and reliable in preparation process, the commercial process is easily achieved; and the prepared composite hydrogen evolution pole has the beneficial effects that the hydrogen evolution catalytic activity is high; during continuous electrolysis, the countercurrent resisting capacity is high, and the service life of the pole is long.</description><language>eng</language><subject>APPARATUS THEREFOR ; CHEMICAL SURFACE TREATMENT ; CHEMISTRY ; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATIONOR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL ; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY IONIMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL ; COATING MATERIAL WITH METALLIC MATERIAL ; COATING METALLIC MATERIAL ; DIFFUSION TREATMENT OF METALLIC MATERIAL ; ELECTROLYTIC OR ELECTROPHORETIC PROCESSES ; ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTIONOF COMPOUNDS OR NON-METALS ; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION INGENERAL ; METALLURGY ; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THESURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION</subject><creationdate>2016</creationdate><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&date=20160224&DB=EPODOC&CC=CN&NR=105350015A$$EHTML$$P50$$Gepo$$Hfree_for_read</linktohtml><link.rule.ids>230,308,776,881,25543,76293</link.rule.ids><linktorsrc>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&date=20160224&DB=EPODOC&CC=CN&NR=105350015A$$EView_record_in_European_Patent_Office$$FView_record_in_$$GEuropean_Patent_Office$$Hfree_for_read</linktorsrc></links><search><creatorcontrib>SHEN CHENYAN</creatorcontrib><creatorcontrib>ZHANG YANFENG</creatorcontrib><creatorcontrib>HUANG XIAOBIN</creatorcontrib><title>Composite hydrogen evolution negative pole with micropore hydrogen storage layer and preparing method for composite hydrogen evolution negative pole</title><description>The invention discloses a composite hydrogen evolution negative pole with a micropore hydrogen storage layer and a preparing method for the composite hydrogen evolution negative pole. The method includes the steps that (1) base body pretreatment, wherein a base body is subject to alkali soaking and washing, and then sand blasting is carried out; (2) a hydrogen storage middle layer is prepared, wherein the step includes the steps: (2.1) plasma thermal spraying treatment is carried out, a Ni50A150 alloy and hydrogen storage alloy powder are evenly mixed according to the weight ratio being (0.95-0.8): (0.05-0.2), and a plasma spraying device is used for spraying; and (2.2) activating treatment is carried out, the base body treated in the step (2.1) is placed into a first alkaline solution to be soaked, excitation is carried out, and the micropore middle layer with the high specific surface area and the high hydrogen storage performance is obtained; and (3) a thermal decomposition method is adopted for preparing a catalyst layer on the hydrogen storage middle layer. The preparing method is simple and reliable in preparation process, the commercial process is easily achieved; and the prepared composite hydrogen evolution pole has the beneficial effects that the hydrogen evolution catalytic activity is high; during continuous electrolysis, the countercurrent resisting capacity is high, and the service life of the pole is long.</description><subject>APPARATUS THEREFOR</subject><subject>CHEMICAL SURFACE TREATMENT</subject><subject>CHEMISTRY</subject><subject>COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATIONOR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL</subject><subject>COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY IONIMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL</subject><subject>COATING MATERIAL WITH METALLIC MATERIAL</subject><subject>COATING METALLIC MATERIAL</subject><subject>DIFFUSION TREATMENT OF METALLIC MATERIAL</subject><subject>ELECTROLYTIC OR ELECTROPHORETIC PROCESSES</subject><subject>ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTIONOF COMPOUNDS OR NON-METALS</subject><subject>INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION INGENERAL</subject><subject>METALLURGY</subject><subject>SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THESURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION</subject><fulltext>true</fulltext><rsrctype>patent</rsrctype><creationdate>2016</creationdate><recordtype>patent</recordtype><sourceid>EVB</sourceid><recordid>eNqNzTEKwkAQRuE0FqLeYTyAkBByAAmKlZV9GJLfzcJmZ5kdI7mHB7axsEz1mg_etvi0MiXJ3kDjMqg4RMIs4WVeIkU4Nj-DkgTQ29tIk-9VkuifzybKDhR4gRLHgZIisfroaIKNMtBTlPrVp32xeXLIOPy6K47Xy6O9nZCkQ07cI8K69l6VTd2UZdWc6zXmCxiCUno</recordid><startdate>20160224</startdate><enddate>20160224</enddate><creator>SHEN CHENYAN</creator><creator>ZHANG YANFENG</creator><creator>HUANG XIAOBIN</creator><scope>EVB</scope></search><sort><creationdate>20160224</creationdate><title>Composite hydrogen evolution negative pole with micropore hydrogen storage layer and preparing method for composite hydrogen evolution negative pole</title><author>SHEN CHENYAN ; ZHANG YANFENG ; HUANG XIAOBIN</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-epo_espacenet_CN105350015A3</frbrgroupid><rsrctype>patents</rsrctype><prefilter>patents</prefilter><language>eng</language><creationdate>2016</creationdate><topic>APPARATUS THEREFOR</topic><topic>CHEMICAL SURFACE TREATMENT</topic><topic>CHEMISTRY</topic><topic>COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATIONOR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL</topic><topic>COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY IONIMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL</topic><topic>COATING MATERIAL WITH METALLIC MATERIAL</topic><topic>COATING METALLIC MATERIAL</topic><topic>DIFFUSION TREATMENT OF METALLIC MATERIAL</topic><topic>ELECTROLYTIC OR ELECTROPHORETIC PROCESSES</topic><topic>ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTIONOF COMPOUNDS OR NON-METALS</topic><topic>INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION INGENERAL</topic><topic>METALLURGY</topic><topic>SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THESURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION</topic><toplevel>online_resources</toplevel><creatorcontrib>SHEN CHENYAN</creatorcontrib><creatorcontrib>ZHANG YANFENG</creatorcontrib><creatorcontrib>HUANG XIAOBIN</creatorcontrib><collection>esp@cenet</collection></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext_linktorsrc</fulltext></delivery><addata><au>SHEN CHENYAN</au><au>ZHANG YANFENG</au><au>HUANG XIAOBIN</au><format>patent</format><genre>patent</genre><ristype>GEN</ristype><title>Composite hydrogen evolution negative pole with micropore hydrogen storage layer and preparing method for composite hydrogen evolution negative pole</title><date>2016-02-24</date><risdate>2016</risdate><abstract>The invention discloses a composite hydrogen evolution negative pole with a micropore hydrogen storage layer and a preparing method for the composite hydrogen evolution negative pole. The method includes the steps that (1) base body pretreatment, wherein a base body is subject to alkali soaking and washing, and then sand blasting is carried out; (2) a hydrogen storage middle layer is prepared, wherein the step includes the steps: (2.1) plasma thermal spraying treatment is carried out, a Ni50A150 alloy and hydrogen storage alloy powder are evenly mixed according to the weight ratio being (0.95-0.8): (0.05-0.2), and a plasma spraying device is used for spraying; and (2.2) activating treatment is carried out, the base body treated in the step (2.1) is placed into a first alkaline solution to be soaked, excitation is carried out, and the micropore middle layer with the high specific surface area and the high hydrogen storage performance is obtained; and (3) a thermal decomposition method is adopted for preparing a catalyst layer on the hydrogen storage middle layer. The preparing method is simple and reliable in preparation process, the commercial process is easily achieved; and the prepared composite hydrogen evolution pole has the beneficial effects that the hydrogen evolution catalytic activity is high; during continuous electrolysis, the countercurrent resisting capacity is high, and the service life of the pole is long.</abstract><oa>free_for_read</oa></addata></record> |
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subjects | APPARATUS THEREFOR CHEMICAL SURFACE TREATMENT CHEMISTRY COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATIONOR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY IONIMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL COATING MATERIAL WITH METALLIC MATERIAL COATING METALLIC MATERIAL DIFFUSION TREATMENT OF METALLIC MATERIAL ELECTROLYTIC OR ELECTROPHORETIC PROCESSES ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTIONOF COMPOUNDS OR NON-METALS INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION INGENERAL METALLURGY SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THESURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION |
title | Composite hydrogen evolution negative pole with micropore hydrogen storage layer and preparing method for composite hydrogen evolution negative pole |
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