Method for preparing nickel coating on ceramic surface by using in-situ reduction method

The present invention discloses a method for preparing a nickel coating on a ceramic surface by using an in-situ reduction method. The method comprises: coating a roughened ceramic surface with PVA sol; preserving heat in a heating furnace under a temperature of 80-100 DEG C; then raising the temper...

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Hauptverfasser: LUO RONG, WENG YANWEI, SANG KEZHENG, ZHANG YONG
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creator LUO RONG
WENG YANWEI
SANG KEZHENG
ZHANG YONG
description The present invention discloses a method for preparing a nickel coating on a ceramic surface by using an in-situ reduction method. The method comprises: coating a roughened ceramic surface with PVA sol; preserving heat in a heating furnace under a temperature of 80-100 DEG C; then raising the temperature to 600 DEG C and preserving the heat, so as to completely decompose PVA; then vacuuming the heating furnace; under the condition of argon protection, introducing hydrogen into a heating box to perform in-situ reduction, and meanwhile raising the temperature to 900-1000 DEG C, and preserving the heat. According to the present invention, by a sol-gel method, required raw materials are mixed uniformly in a liquid phase, and compared with particles, the sol has fluidity, film forming property and a property so that the sol can be continuously, uniformly and compactly attached to ceramic matrixes with various complex shapes; a PVA film comprising NiCl2 is prepared on the ceramic surface, then the ceramic surface is coated precisely, continuously and uniformly with the nickel coating by the in-situ reduction method; and by adjusting the mass fraction of nickel salt in the PVA sol, the thickness of the obtained coating is controllable, and the bonding force with the matrix is favorable.
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According to the present invention, by a sol-gel method, required raw materials are mixed uniformly in a liquid phase, and compared with particles, the sol has fluidity, film forming property and a property so that the sol can be continuously, uniformly and compactly attached to ceramic matrixes with various complex shapes; a PVA film comprising NiCl2 is prepared on the ceramic surface, then the ceramic surface is coated precisely, continuously and uniformly with the nickel coating by the in-situ reduction method; and by adjusting the mass fraction of nickel salt in the PVA sol, the thickness of the obtained coating is controllable, and the bonding force with the matrix is favorable.</description><language>eng</language><subject>ARTIFICIAL STONE ; CEMENTS ; CERAMICS ; CHEMISTRY ; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDINGMATERIALS ; CONCRETE ; LIME, MAGNESIA ; METALLURGY ; REFRACTORIES ; SLAG ; TREATMENT OF NATURAL STONE</subject><creationdate>2015</creationdate><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&amp;date=20151021&amp;DB=EPODOC&amp;CC=CN&amp;NR=104987134A$$EHTML$$P50$$Gepo$$Hfree_for_read</linktohtml><link.rule.ids>230,308,776,881,25542,76290</link.rule.ids><linktorsrc>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&amp;date=20151021&amp;DB=EPODOC&amp;CC=CN&amp;NR=104987134A$$EView_record_in_European_Patent_Office$$FView_record_in_$$GEuropean_Patent_Office$$Hfree_for_read</linktorsrc></links><search><creatorcontrib>LUO RONG</creatorcontrib><creatorcontrib>WENG YANWEI</creatorcontrib><creatorcontrib>SANG KEZHENG</creatorcontrib><creatorcontrib>ZHANG YONG</creatorcontrib><title>Method for preparing nickel coating on ceramic surface by using in-situ reduction method</title><description>The present invention discloses a method for preparing a nickel coating on a ceramic surface by using an in-situ reduction method. 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subjects ARTIFICIAL STONE
CEMENTS
CERAMICS
CHEMISTRY
COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDINGMATERIALS
CONCRETE
LIME, MAGNESIA
METALLURGY
REFRACTORIES
SLAG
TREATMENT OF NATURAL STONE
title Method for preparing nickel coating on ceramic surface by using in-situ reduction method
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