Method for preparing nickel coating on ceramic surface by using in-situ reduction method
The present invention discloses a method for preparing a nickel coating on a ceramic surface by using an in-situ reduction method. The method comprises: coating a roughened ceramic surface with PVA sol; preserving heat in a heating furnace under a temperature of 80-100 DEG C; then raising the temper...
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creator | LUO RONG WENG YANWEI SANG KEZHENG ZHANG YONG |
description | The present invention discloses a method for preparing a nickel coating on a ceramic surface by using an in-situ reduction method. The method comprises: coating a roughened ceramic surface with PVA sol; preserving heat in a heating furnace under a temperature of 80-100 DEG C; then raising the temperature to 600 DEG C and preserving the heat, so as to completely decompose PVA; then vacuuming the heating furnace; under the condition of argon protection, introducing hydrogen into a heating box to perform in-situ reduction, and meanwhile raising the temperature to 900-1000 DEG C, and preserving the heat. According to the present invention, by a sol-gel method, required raw materials are mixed uniformly in a liquid phase, and compared with particles, the sol has fluidity, film forming property and a property so that the sol can be continuously, uniformly and compactly attached to ceramic matrixes with various complex shapes; a PVA film comprising NiCl2 is prepared on the ceramic surface, then the ceramic surface is coated precisely, continuously and uniformly with the nickel coating by the in-situ reduction method; and by adjusting the mass fraction of nickel salt in the PVA sol, the thickness of the obtained coating is controllable, and the bonding force with the matrix is favorable. |
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The method comprises: coating a roughened ceramic surface with PVA sol; preserving heat in a heating furnace under a temperature of 80-100 DEG C; then raising the temperature to 600 DEG C and preserving the heat, so as to completely decompose PVA; then vacuuming the heating furnace; under the condition of argon protection, introducing hydrogen into a heating box to perform in-situ reduction, and meanwhile raising the temperature to 900-1000 DEG C, and preserving the heat. According to the present invention, by a sol-gel method, required raw materials are mixed uniformly in a liquid phase, and compared with particles, the sol has fluidity, film forming property and a property so that the sol can be continuously, uniformly and compactly attached to ceramic matrixes with various complex shapes; a PVA film comprising NiCl2 is prepared on the ceramic surface, then the ceramic surface is coated precisely, continuously and uniformly with the nickel coating by the in-situ reduction method; and by adjusting the mass fraction of nickel salt in the PVA sol, the thickness of the obtained coating is controllable, and the bonding force with the matrix is favorable.</description><language>eng</language><subject>ARTIFICIAL STONE ; CEMENTS ; CERAMICS ; CHEMISTRY ; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDINGMATERIALS ; CONCRETE ; LIME, MAGNESIA ; METALLURGY ; REFRACTORIES ; SLAG ; TREATMENT OF NATURAL STONE</subject><creationdate>2015</creationdate><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&date=20151021&DB=EPODOC&CC=CN&NR=104987134A$$EHTML$$P50$$Gepo$$Hfree_for_read</linktohtml><link.rule.ids>230,308,776,881,25542,76290</link.rule.ids><linktorsrc>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&date=20151021&DB=EPODOC&CC=CN&NR=104987134A$$EView_record_in_European_Patent_Office$$FView_record_in_$$GEuropean_Patent_Office$$Hfree_for_read</linktorsrc></links><search><creatorcontrib>LUO RONG</creatorcontrib><creatorcontrib>WENG YANWEI</creatorcontrib><creatorcontrib>SANG KEZHENG</creatorcontrib><creatorcontrib>ZHANG YONG</creatorcontrib><title>Method for preparing nickel coating on ceramic surface by using in-situ reduction method</title><description>The present invention discloses a method for preparing a nickel coating on a ceramic surface by using an in-situ reduction method. The method comprises: coating a roughened ceramic surface with PVA sol; preserving heat in a heating furnace under a temperature of 80-100 DEG C; then raising the temperature to 600 DEG C and preserving the heat, so as to completely decompose PVA; then vacuuming the heating furnace; under the condition of argon protection, introducing hydrogen into a heating box to perform in-situ reduction, and meanwhile raising the temperature to 900-1000 DEG C, and preserving the heat. According to the present invention, by a sol-gel method, required raw materials are mixed uniformly in a liquid phase, and compared with particles, the sol has fluidity, film forming property and a property so that the sol can be continuously, uniformly and compactly attached to ceramic matrixes with various complex shapes; a PVA film comprising NiCl2 is prepared on the ceramic surface, then the ceramic surface is coated precisely, continuously and uniformly with the nickel coating by the in-situ reduction method; and by adjusting the mass fraction of nickel salt in the PVA sol, the thickness of the obtained coating is controllable, and the bonding force with the matrix is favorable.</description><subject>ARTIFICIAL STONE</subject><subject>CEMENTS</subject><subject>CERAMICS</subject><subject>CHEMISTRY</subject><subject>COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDINGMATERIALS</subject><subject>CONCRETE</subject><subject>LIME, MAGNESIA</subject><subject>METALLURGY</subject><subject>REFRACTORIES</subject><subject>SLAG</subject><subject>TREATMENT OF NATURAL STONE</subject><fulltext>true</fulltext><rsrctype>patent</rsrctype><creationdate>2015</creationdate><recordtype>patent</recordtype><sourceid>EVB</sourceid><recordid>eNrjZIjwTS3JyE9RSMsvUigoSi1ILMrMS1fIy0zOTs1RSM5PLAFx8_MUklOLEnMzkxWKS4vSEpNTFZIqFUqLQXKZebrFmSWlCkWpKaXJJZlApblgE3kYWNMSc4pTeaE0N4Oim2uIs4duakF-fGpxAdCQvNSSeGc_QwMTSwtzQ2MTR2Ni1AAAk3M6Rg</recordid><startdate>20151021</startdate><enddate>20151021</enddate><creator>LUO RONG</creator><creator>WENG YANWEI</creator><creator>SANG KEZHENG</creator><creator>ZHANG YONG</creator><scope>EVB</scope></search><sort><creationdate>20151021</creationdate><title>Method for preparing nickel coating on ceramic surface by using in-situ reduction method</title><author>LUO RONG ; WENG YANWEI ; SANG KEZHENG ; ZHANG YONG</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-epo_espacenet_CN104987134A3</frbrgroupid><rsrctype>patents</rsrctype><prefilter>patents</prefilter><language>eng</language><creationdate>2015</creationdate><topic>ARTIFICIAL STONE</topic><topic>CEMENTS</topic><topic>CERAMICS</topic><topic>CHEMISTRY</topic><topic>COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDINGMATERIALS</topic><topic>CONCRETE</topic><topic>LIME, MAGNESIA</topic><topic>METALLURGY</topic><topic>REFRACTORIES</topic><topic>SLAG</topic><topic>TREATMENT OF NATURAL STONE</topic><toplevel>online_resources</toplevel><creatorcontrib>LUO RONG</creatorcontrib><creatorcontrib>WENG YANWEI</creatorcontrib><creatorcontrib>SANG KEZHENG</creatorcontrib><creatorcontrib>ZHANG YONG</creatorcontrib><collection>esp@cenet</collection></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext_linktorsrc</fulltext></delivery><addata><au>LUO RONG</au><au>WENG YANWEI</au><au>SANG KEZHENG</au><au>ZHANG YONG</au><format>patent</format><genre>patent</genre><ristype>GEN</ristype><title>Method for preparing nickel coating on ceramic surface by using in-situ reduction method</title><date>2015-10-21</date><risdate>2015</risdate><abstract>The present invention discloses a method for preparing a nickel coating on a ceramic surface by using an in-situ reduction method. The method comprises: coating a roughened ceramic surface with PVA sol; preserving heat in a heating furnace under a temperature of 80-100 DEG C; then raising the temperature to 600 DEG C and preserving the heat, so as to completely decompose PVA; then vacuuming the heating furnace; under the condition of argon protection, introducing hydrogen into a heating box to perform in-situ reduction, and meanwhile raising the temperature to 900-1000 DEG C, and preserving the heat. According to the present invention, by a sol-gel method, required raw materials are mixed uniformly in a liquid phase, and compared with particles, the sol has fluidity, film forming property and a property so that the sol can be continuously, uniformly and compactly attached to ceramic matrixes with various complex shapes; a PVA film comprising NiCl2 is prepared on the ceramic surface, then the ceramic surface is coated precisely, continuously and uniformly with the nickel coating by the in-situ reduction method; and by adjusting the mass fraction of nickel salt in the PVA sol, the thickness of the obtained coating is controllable, and the bonding force with the matrix is favorable.</abstract><oa>free_for_read</oa></addata></record> |
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title | Method for preparing nickel coating on ceramic surface by using in-situ reduction method |
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