Extraction and rectification method for separating mixture of cyclohexane and n-propanol

The invention discloses an extraction and rectification method for separating a mixture of cyclohexane and n-propanol. A mixture of dimethyl sulfoxide and N,N-dimethyl acetamide is taken as the extractant, a mixture of cyclohexane and n-propanol enters a extraction and rectification tower with 30 to...

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Bibliographische Detailangaben
Hauptverfasser: CHEN ZHIRONG, YIN HONG, GAO ZIZI, YUAN SHENFENG
Format: Patent
Sprache:eng
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Beschreibung
Zusammenfassung:The invention discloses an extraction and rectification method for separating a mixture of cyclohexane and n-propanol. A mixture of dimethyl sulfoxide and N,N-dimethyl acetamide is taken as the extractant, a mixture of cyclohexane and n-propanol enters a extraction and rectification tower with 30 to 60 theoretical plates from the 15th-40th theoretical plate, the extractant enters the tower from the 5th-20th theoretical plate, the cyclohexane is discharged from the top of the extraction and rectification tower, the mixture of extractant and n-propanol is discharged from the bottom of the extraction and rectification tower and then fed into an extractant recovery tower with 15 to 30 theoretical plates from the 10th-20th plate, n-propanol is discharged from the top of the extractant recovery tower, and the extractant is discharged from the bottom of the extractant recovery tower and recovered. The method has the advantages of low energy consumption, high purity, high yield, simple technology, safety, environment-friendliness, and no pollution, and is capable of achieving clean production.