Darunavir crystal form and preparation method thereof
The invention belongs to the field of chemical and pharmaceutical engineering, and relates to a darunavir crystal form and a preparation method thereof. A powder X-ray diffraction spectrum of the darunavir crystal form has characteristic peaks when a reflection angle 2theta is 7.50+/-0.2, 8.62+/-0.2...
Gespeichert in:
Hauptverfasser: | , , |
---|---|
Format: | Patent |
Sprache: | eng |
Schlagworte: | |
Online-Zugang: | Volltext bestellen |
Tags: |
Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
|
container_end_page | |
---|---|
container_issue | |
container_start_page | |
container_title | |
container_volume | |
creator | ZHU JIALONG YE MEIQI GUO PENG |
description | The invention belongs to the field of chemical and pharmaceutical engineering, and relates to a darunavir crystal form and a preparation method thereof. A powder X-ray diffraction spectrum of the darunavir crystal form has characteristic peaks when a reflection angle 2theta is 7.50+/-0.2, 8.62+/-0.2, 12.17+/-0.2, 13.64+/-0.2, 15.65+/-0.2 and 18.16+/-0.2, and an infrared spectrum has characteristic peaks at 1693cm, 3348cm and 3465 locations. Meanwhile, the invention also provides the preparation method of the crystal form. |
format | Patent |
fullrecord | <record><control><sourceid>epo_EVB</sourceid><recordid>TN_cdi_epo_espacenet_CN104744488A</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><sourcerecordid>CN104744488A</sourcerecordid><originalsourceid>FETCH-epo_espacenet_CN104744488A3</originalsourceid><addsrcrecordid>eNrjZDB1SSwqzUssyyxSSC6qLC5JzFFIyy_KVUjMS1EoKEotSCxKLMnMz1PITS3JyE9RKMlILUrNT-NhYE1LzClO5YXS3AyKbq4hzh66qQX58anFBYnJqXmpJfHOfoYGJuYmJiYWFo7GxKgBAJFLLZQ</addsrcrecordid><sourcetype>Open Access Repository</sourcetype><iscdi>true</iscdi><recordtype>patent</recordtype></control><display><type>patent</type><title>Darunavir crystal form and preparation method thereof</title><source>esp@cenet</source><creator>ZHU JIALONG ; YE MEIQI ; GUO PENG</creator><creatorcontrib>ZHU JIALONG ; YE MEIQI ; GUO PENG</creatorcontrib><description>The invention belongs to the field of chemical and pharmaceutical engineering, and relates to a darunavir crystal form and a preparation method thereof. A powder X-ray diffraction spectrum of the darunavir crystal form has characteristic peaks when a reflection angle 2theta is 7.50+/-0.2, 8.62+/-0.2, 12.17+/-0.2, 13.64+/-0.2, 15.65+/-0.2 and 18.16+/-0.2, and an infrared spectrum has characteristic peaks at 1693cm<-1>, 3348cm<-1> and 3465<-1> locations. Meanwhile, the invention also provides the preparation method of the crystal form.</description><language>eng</language><subject>APPARATUS THEREFOR ; CHEMISTRY ; GENERAL METHODS OF ORGANIC CHEMISTRY ; HETEROCYCLIC COMPOUNDS ; METALLURGY ; ORGANIC CHEMISTRY</subject><creationdate>2015</creationdate><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&date=20150701&DB=EPODOC&CC=CN&NR=104744488A$$EHTML$$P50$$Gepo$$Hfree_for_read</linktohtml><link.rule.ids>230,308,780,885,25564,76547</link.rule.ids><linktorsrc>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&date=20150701&DB=EPODOC&CC=CN&NR=104744488A$$EView_record_in_European_Patent_Office$$FView_record_in_$$GEuropean_Patent_Office$$Hfree_for_read</linktorsrc></links><search><creatorcontrib>ZHU JIALONG</creatorcontrib><creatorcontrib>YE MEIQI</creatorcontrib><creatorcontrib>GUO PENG</creatorcontrib><title>Darunavir crystal form and preparation method thereof</title><description>The invention belongs to the field of chemical and pharmaceutical engineering, and relates to a darunavir crystal form and a preparation method thereof. A powder X-ray diffraction spectrum of the darunavir crystal form has characteristic peaks when a reflection angle 2theta is 7.50+/-0.2, 8.62+/-0.2, 12.17+/-0.2, 13.64+/-0.2, 15.65+/-0.2 and 18.16+/-0.2, and an infrared spectrum has characteristic peaks at 1693cm<-1>, 3348cm<-1> and 3465<-1> locations. Meanwhile, the invention also provides the preparation method of the crystal form.</description><subject>APPARATUS THEREFOR</subject><subject>CHEMISTRY</subject><subject>GENERAL METHODS OF ORGANIC CHEMISTRY</subject><subject>HETEROCYCLIC COMPOUNDS</subject><subject>METALLURGY</subject><subject>ORGANIC CHEMISTRY</subject><fulltext>true</fulltext><rsrctype>patent</rsrctype><creationdate>2015</creationdate><recordtype>patent</recordtype><sourceid>EVB</sourceid><recordid>eNrjZDB1SSwqzUssyyxSSC6qLC5JzFFIyy_KVUjMS1EoKEotSCxKLMnMz1PITS3JyE9RKMlILUrNT-NhYE1LzClO5YXS3AyKbq4hzh66qQX58anFBYnJqXmpJfHOfoYGJuYmJiYWFo7GxKgBAJFLLZQ</recordid><startdate>20150701</startdate><enddate>20150701</enddate><creator>ZHU JIALONG</creator><creator>YE MEIQI</creator><creator>GUO PENG</creator><scope>EVB</scope></search><sort><creationdate>20150701</creationdate><title>Darunavir crystal form and preparation method thereof</title><author>ZHU JIALONG ; YE MEIQI ; GUO PENG</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-epo_espacenet_CN104744488A3</frbrgroupid><rsrctype>patents</rsrctype><prefilter>patents</prefilter><language>eng</language><creationdate>2015</creationdate><topic>APPARATUS THEREFOR</topic><topic>CHEMISTRY</topic><topic>GENERAL METHODS OF ORGANIC CHEMISTRY</topic><topic>HETEROCYCLIC COMPOUNDS</topic><topic>METALLURGY</topic><topic>ORGANIC CHEMISTRY</topic><toplevel>online_resources</toplevel><creatorcontrib>ZHU JIALONG</creatorcontrib><creatorcontrib>YE MEIQI</creatorcontrib><creatorcontrib>GUO PENG</creatorcontrib><collection>esp@cenet</collection></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext_linktorsrc</fulltext></delivery><addata><au>ZHU JIALONG</au><au>YE MEIQI</au><au>GUO PENG</au><format>patent</format><genre>patent</genre><ristype>GEN</ristype><title>Darunavir crystal form and preparation method thereof</title><date>2015-07-01</date><risdate>2015</risdate><abstract>The invention belongs to the field of chemical and pharmaceutical engineering, and relates to a darunavir crystal form and a preparation method thereof. A powder X-ray diffraction spectrum of the darunavir crystal form has characteristic peaks when a reflection angle 2theta is 7.50+/-0.2, 8.62+/-0.2, 12.17+/-0.2, 13.64+/-0.2, 15.65+/-0.2 and 18.16+/-0.2, and an infrared spectrum has characteristic peaks at 1693cm<-1>, 3348cm<-1> and 3465<-1> locations. Meanwhile, the invention also provides the preparation method of the crystal form.</abstract><oa>free_for_read</oa></addata></record> |
fulltext | fulltext_linktorsrc |
identifier | |
ispartof | |
issn | |
language | eng |
recordid | cdi_epo_espacenet_CN104744488A |
source | esp@cenet |
subjects | APPARATUS THEREFOR CHEMISTRY GENERAL METHODS OF ORGANIC CHEMISTRY HETEROCYCLIC COMPOUNDS METALLURGY ORGANIC CHEMISTRY |
title | Darunavir crystal form and preparation method thereof |
url | https://sfx.bib-bvb.de/sfx_tum?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2024-12-25T18%3A47%3A02IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-epo_EVB&rft_val_fmt=info:ofi/fmt:kev:mtx:patent&rft.genre=patent&rft.au=ZHU%20JIALONG&rft.date=2015-07-01&rft_id=info:doi/&rft_dat=%3Cepo_EVB%3ECN104744488A%3C/epo_EVB%3E%3Curl%3E%3C/url%3E&disable_directlink=true&sfx.directlink=off&sfx.report_link=0&rft_id=info:oai/&rft_id=info:pmid/&rfr_iscdi=true |