Internal-pressure-type vacuum membrane distillation concentration method of ethylene glycol solution
The invention discloses an internal-pressure-type vacuum membrane distillation concentration method of an ethylene glycol solution. Concentration and purification of the ethylene glycol solution in a process of preparing ethylene glycol from oxirane through a hydration method are carried out through...
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creator | PENG HAIZHU ZHANG XINMIAO YANG YONGQIANG |
description | The invention discloses an internal-pressure-type vacuum membrane distillation concentration method of an ethylene glycol solution. Concentration and purification of the ethylene glycol solution in a process of preparing ethylene glycol from oxirane through a hydration method are carried out through the internal-pressure-type vacuum membrane distillation coupled with a rectification technology. The method comprises following steps: (1) pumping the ethylene glycol water solution at about 85-100 DEG C into a raw water tank; (2) pumping the ethylene glycol water solution in the raw water tank to a tube pass of a hollow fiber membrane assembly at a specific membrane surface flow rate through a material feeding pump; and (3) vacuumizing a permeation side, namely, a shell pass, of a hollow fiber membrane assembly, so that condensable gas is condensed through a condenser at the permeation side to form water while a concentrated ethylene glycol solution in the tube pass is fed back to the raw water tank for circulating concentration. Compared with multiple-effect evaporation, the method is less in equipment investment, is high in treatment efficiency, is low in operation temperature and operation pressure and is low in energy consumption. |
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Concentration and purification of the ethylene glycol solution in a process of preparing ethylene glycol from oxirane through a hydration method are carried out through the internal-pressure-type vacuum membrane distillation coupled with a rectification technology. The method comprises following steps: (1) pumping the ethylene glycol water solution at about 85-100 DEG C into a raw water tank; (2) pumping the ethylene glycol water solution in the raw water tank to a tube pass of a hollow fiber membrane assembly at a specific membrane surface flow rate through a material feeding pump; and (3) vacuumizing a permeation side, namely, a shell pass, of a hollow fiber membrane assembly, so that condensable gas is condensed through a condenser at the permeation side to form water while a concentrated ethylene glycol solution in the tube pass is fed back to the raw water tank for circulating concentration. Compared with multiple-effect evaporation, the method is less in equipment investment, is high in treatment efficiency, is low in operation temperature and operation pressure and is low in energy consumption.</description><language>eng</language><subject>ACYCLIC OR CARBOCYCLIC COMPOUNDS ; CHEMISTRY ; METALLURGY ; ORGANIC CHEMISTRY ; PERFORMING OPERATIONS ; PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL ; SEPARATION ; TRANSPORTING</subject><creationdate>2015</creationdate><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&date=20150318&DB=EPODOC&CC=CN&NR=104415664A$$EHTML$$P50$$Gepo$$Hfree_for_read</linktohtml><link.rule.ids>230,308,780,885,25564,76547</link.rule.ids><linktorsrc>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&date=20150318&DB=EPODOC&CC=CN&NR=104415664A$$EView_record_in_European_Patent_Office$$FView_record_in_$$GEuropean_Patent_Office$$Hfree_for_read</linktorsrc></links><search><creatorcontrib>PENG HAIZHU</creatorcontrib><creatorcontrib>ZHANG XINMIAO</creatorcontrib><creatorcontrib>YANG YONGQIANG</creatorcontrib><title>Internal-pressure-type vacuum membrane distillation concentration method of ethylene glycol solution</title><description>The invention discloses an internal-pressure-type vacuum membrane distillation concentration method of an ethylene glycol solution. Concentration and purification of the ethylene glycol solution in a process of preparing ethylene glycol from oxirane through a hydration method are carried out through the internal-pressure-type vacuum membrane distillation coupled with a rectification technology. The method comprises following steps: (1) pumping the ethylene glycol water solution at about 85-100 DEG C into a raw water tank; (2) pumping the ethylene glycol water solution in the raw water tank to a tube pass of a hollow fiber membrane assembly at a specific membrane surface flow rate through a material feeding pump; and (3) vacuumizing a permeation side, namely, a shell pass, of a hollow fiber membrane assembly, so that condensable gas is condensed through a condenser at the permeation side to form water while a concentrated ethylene glycol solution in the tube pass is fed back to the raw water tank for circulating concentration. Compared with multiple-effect evaporation, the method is less in equipment investment, is high in treatment efficiency, is low in operation temperature and operation pressure and is low in energy consumption.</description><subject>ACYCLIC OR CARBOCYCLIC COMPOUNDS</subject><subject>CHEMISTRY</subject><subject>METALLURGY</subject><subject>ORGANIC CHEMISTRY</subject><subject>PERFORMING OPERATIONS</subject><subject>PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL</subject><subject>SEPARATION</subject><subject>TRANSPORTING</subject><fulltext>true</fulltext><rsrctype>patent</rsrctype><creationdate>2015</creationdate><recordtype>patent</recordtype><sourceid>EVB</sourceid><recordid>eNqNzEEKwjAUBNBuXIh6h-8BChareymKbly5LzGdauEnPyQ_Qm9vRQ_gambgMfOiu3hF9IbLEJFSjih1DKCXsTk7cnD3aDyoG5IOzEYH8WTFW3iN3-WgT-lIeprKyJj0g0crTEk4f8iymPWGE1a_XBTr0_HWnEsEaZGCmd6gbXOtNnVd7fb7-rD9x7wBtS9AVQ</recordid><startdate>20150318</startdate><enddate>20150318</enddate><creator>PENG HAIZHU</creator><creator>ZHANG XINMIAO</creator><creator>YANG YONGQIANG</creator><scope>EVB</scope></search><sort><creationdate>20150318</creationdate><title>Internal-pressure-type vacuum membrane distillation concentration method of ethylene glycol solution</title><author>PENG HAIZHU ; ZHANG XINMIAO ; YANG YONGQIANG</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-epo_espacenet_CN104415664A3</frbrgroupid><rsrctype>patents</rsrctype><prefilter>patents</prefilter><language>eng</language><creationdate>2015</creationdate><topic>ACYCLIC OR CARBOCYCLIC COMPOUNDS</topic><topic>CHEMISTRY</topic><topic>METALLURGY</topic><topic>ORGANIC CHEMISTRY</topic><topic>PERFORMING OPERATIONS</topic><topic>PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL</topic><topic>SEPARATION</topic><topic>TRANSPORTING</topic><toplevel>online_resources</toplevel><creatorcontrib>PENG HAIZHU</creatorcontrib><creatorcontrib>ZHANG XINMIAO</creatorcontrib><creatorcontrib>YANG YONGQIANG</creatorcontrib><collection>esp@cenet</collection></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext_linktorsrc</fulltext></delivery><addata><au>PENG HAIZHU</au><au>ZHANG XINMIAO</au><au>YANG YONGQIANG</au><format>patent</format><genre>patent</genre><ristype>GEN</ristype><title>Internal-pressure-type vacuum membrane distillation concentration method of ethylene glycol solution</title><date>2015-03-18</date><risdate>2015</risdate><abstract>The invention discloses an internal-pressure-type vacuum membrane distillation concentration method of an ethylene glycol solution. Concentration and purification of the ethylene glycol solution in a process of preparing ethylene glycol from oxirane through a hydration method are carried out through the internal-pressure-type vacuum membrane distillation coupled with a rectification technology. The method comprises following steps: (1) pumping the ethylene glycol water solution at about 85-100 DEG C into a raw water tank; (2) pumping the ethylene glycol water solution in the raw water tank to a tube pass of a hollow fiber membrane assembly at a specific membrane surface flow rate through a material feeding pump; and (3) vacuumizing a permeation side, namely, a shell pass, of a hollow fiber membrane assembly, so that condensable gas is condensed through a condenser at the permeation side to form water while a concentrated ethylene glycol solution in the tube pass is fed back to the raw water tank for circulating concentration. Compared with multiple-effect evaporation, the method is less in equipment investment, is high in treatment efficiency, is low in operation temperature and operation pressure and is low in energy consumption.</abstract><oa>free_for_read</oa></addata></record> |
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title | Internal-pressure-type vacuum membrane distillation concentration method of ethylene glycol solution |
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