Method for preparing compositey sealed polyisocyanates coating
The invention discloses a method for preparing a compositely sealed polyisocyanates coating. The method comprises the following steps: heating and stirring polyether polyol and 4,4-diphenylmethane diisocyanate, reacting to obtain a 4,4-diphenylmethane diisocyanate-polyether polyol prepolymer, perfor...
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creator | YIN HUAZHONG TANG NITING YAN YISHU LIU YALI |
description | The invention discloses a method for preparing a compositely sealed polyisocyanates coating. The method comprises the following steps: heating and stirring polyether polyol and 4,4-diphenylmethane diisocyanate, reacting to obtain a 4,4-diphenylmethane diisocyanate-polyether polyol prepolymer, performing composite sealing on the 4,4-diphenylmethane diisocyanate-polyether polyol prepolymer by using malonic acid diethyl ester, ethyl acetoacetate and 3,5-lutidine so as to obtain a polyisocyanates curing agent, and finally adding an amino chain expanding agent and a powder filling material into the compositely sealed polyisocyanates curing agent, thereby obtaining the compositely sealed polyisocyanates coating. When heated, the compositely sealed polyisocyanates coating prepared by using the method can be gradually unsealed and cured in different periods, the phenomenon of edge curtain coating of conventional singly sealed polyisocyanates in the baking process because of too high unsealing temperature is avoided, the filming property of the compositely sealed polyisocyanates coating is improved, a prepared film is relatively high in cross-linking degree, and thus good mechanical property is achieved. |
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The method comprises the following steps: heating and stirring polyether polyol and 4,4-diphenylmethane diisocyanate, reacting to obtain a 4,4-diphenylmethane diisocyanate-polyether polyol prepolymer, performing composite sealing on the 4,4-diphenylmethane diisocyanate-polyether polyol prepolymer by using malonic acid diethyl ester, ethyl acetoacetate and 3,5-lutidine so as to obtain a polyisocyanates curing agent, and finally adding an amino chain expanding agent and a powder filling material into the compositely sealed polyisocyanates curing agent, thereby obtaining the compositely sealed polyisocyanates coating. When heated, the compositely sealed polyisocyanates coating prepared by using the method can be gradually unsealed and cured in different periods, the phenomenon of edge curtain coating of conventional singly sealed polyisocyanates in the baking process because of too high unsealing temperature is avoided, the filming property of the compositely sealed polyisocyanates coating is improved, a prepared film is relatively high in cross-linking degree, and thus good mechanical property is achieved.</description><language>eng</language><subject>ADHESIVES ; CHEMICAL PAINT OR INK REMOVERS ; CHEMISTRY ; COATING COMPOSITIONS, e.g. PAINTS, VARNISHES ORLACQUERS ; COMPOSITIONS BASED THEREON ; CORRECTING FLUIDS ; DYES ; FILLING PASTES ; INKS ; MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONSONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS ; METALLURGY ; MISCELLANEOUS APPLICATIONS OF MATERIALS ; MISCELLANEOUS COMPOSITIONS ; NATURAL RESINS ; ORGANIC MACROMOLECULAR COMPOUNDS ; PAINTS ; PASTES OR SOLIDS FOR COLOURING OR PRINTING ; POLISHES ; THEIR PREPARATION OR CHEMICAL WORKING-UP ; USE OF MATERIALS THEREFOR ; WOODSTAINS</subject><creationdate>2015</creationdate><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&date=20150128&DB=EPODOC&CC=CN&NR=104311792A$$EHTML$$P50$$Gepo$$Hfree_for_read</linktohtml><link.rule.ids>230,308,780,885,25564,76547</link.rule.ids><linktorsrc>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&date=20150128&DB=EPODOC&CC=CN&NR=104311792A$$EView_record_in_European_Patent_Office$$FView_record_in_$$GEuropean_Patent_Office$$Hfree_for_read</linktorsrc></links><search><creatorcontrib>YIN HUAZHONG</creatorcontrib><creatorcontrib>TANG NITING</creatorcontrib><creatorcontrib>YAN YISHU</creatorcontrib><creatorcontrib>LIU YALI</creatorcontrib><title>Method for preparing compositey sealed polyisocyanates coating</title><description>The invention discloses a method for preparing a compositely sealed polyisocyanates coating. The method comprises the following steps: heating and stirring polyether polyol and 4,4-diphenylmethane diisocyanate, reacting to obtain a 4,4-diphenylmethane diisocyanate-polyether polyol prepolymer, performing composite sealing on the 4,4-diphenylmethane diisocyanate-polyether polyol prepolymer by using malonic acid diethyl ester, ethyl acetoacetate and 3,5-lutidine so as to obtain a polyisocyanates curing agent, and finally adding an amino chain expanding agent and a powder filling material into the compositely sealed polyisocyanates curing agent, thereby obtaining the compositely sealed polyisocyanates coating. When heated, the compositely sealed polyisocyanates coating prepared by using the method can be gradually unsealed and cured in different periods, the phenomenon of edge curtain coating of conventional singly sealed polyisocyanates in the baking process because of too high unsealing temperature is avoided, the filming property of the compositely sealed polyisocyanates coating is improved, a prepared film is relatively high in cross-linking degree, and thus good mechanical property is achieved.</description><subject>ADHESIVES</subject><subject>CHEMICAL PAINT OR INK REMOVERS</subject><subject>CHEMISTRY</subject><subject>COATING COMPOSITIONS, e.g. PAINTS, VARNISHES ORLACQUERS</subject><subject>COMPOSITIONS BASED THEREON</subject><subject>CORRECTING FLUIDS</subject><subject>DYES</subject><subject>FILLING PASTES</subject><subject>INKS</subject><subject>MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONSONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS</subject><subject>METALLURGY</subject><subject>MISCELLANEOUS APPLICATIONS OF MATERIALS</subject><subject>MISCELLANEOUS COMPOSITIONS</subject><subject>NATURAL RESINS</subject><subject>ORGANIC MACROMOLECULAR COMPOUNDS</subject><subject>PAINTS</subject><subject>PASTES OR SOLIDS FOR COLOURING OR PRINTING</subject><subject>POLISHES</subject><subject>THEIR PREPARATION OR CHEMICAL WORKING-UP</subject><subject>USE OF MATERIALS THEREFOR</subject><subject>WOODSTAINS</subject><fulltext>true</fulltext><rsrctype>patent</rsrctype><creationdate>2015</creationdate><recordtype>patent</recordtype><sourceid>EVB</sourceid><recordid>eNrjZLDzTS3JyE9RSMsvUigoSi1ILMrMS1dIzs8tyC_OLEmtVChOTcxJTVEoyM-pzCzOT65MzEssSS0GqkgsAarkYWBNS8wpTuWF0twMim6uIc4euqkF-fGpxQWJyal5qSXxzn6GBibGhobmlkaOxsSoAQCwdDFT</recordid><startdate>20150128</startdate><enddate>20150128</enddate><creator>YIN HUAZHONG</creator><creator>TANG NITING</creator><creator>YAN YISHU</creator><creator>LIU YALI</creator><scope>EVB</scope></search><sort><creationdate>20150128</creationdate><title>Method for preparing compositey sealed polyisocyanates coating</title><author>YIN HUAZHONG ; TANG NITING ; YAN YISHU ; LIU YALI</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-epo_espacenet_CN104311792A3</frbrgroupid><rsrctype>patents</rsrctype><prefilter>patents</prefilter><language>eng</language><creationdate>2015</creationdate><topic>ADHESIVES</topic><topic>CHEMICAL PAINT OR INK REMOVERS</topic><topic>CHEMISTRY</topic><topic>COATING COMPOSITIONS, e.g. PAINTS, VARNISHES ORLACQUERS</topic><topic>COMPOSITIONS BASED THEREON</topic><topic>CORRECTING FLUIDS</topic><topic>DYES</topic><topic>FILLING PASTES</topic><topic>INKS</topic><topic>MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONSONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS</topic><topic>METALLURGY</topic><topic>MISCELLANEOUS APPLICATIONS OF MATERIALS</topic><topic>MISCELLANEOUS COMPOSITIONS</topic><topic>NATURAL RESINS</topic><topic>ORGANIC MACROMOLECULAR COMPOUNDS</topic><topic>PAINTS</topic><topic>PASTES OR SOLIDS FOR COLOURING OR PRINTING</topic><topic>POLISHES</topic><topic>THEIR PREPARATION OR CHEMICAL WORKING-UP</topic><topic>USE OF MATERIALS THEREFOR</topic><topic>WOODSTAINS</topic><toplevel>online_resources</toplevel><creatorcontrib>YIN HUAZHONG</creatorcontrib><creatorcontrib>TANG NITING</creatorcontrib><creatorcontrib>YAN YISHU</creatorcontrib><creatorcontrib>LIU YALI</creatorcontrib><collection>esp@cenet</collection></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext_linktorsrc</fulltext></delivery><addata><au>YIN HUAZHONG</au><au>TANG NITING</au><au>YAN YISHU</au><au>LIU YALI</au><format>patent</format><genre>patent</genre><ristype>GEN</ristype><title>Method for preparing compositey sealed polyisocyanates coating</title><date>2015-01-28</date><risdate>2015</risdate><abstract>The invention discloses a method for preparing a compositely sealed polyisocyanates coating. The method comprises the following steps: heating and stirring polyether polyol and 4,4-diphenylmethane diisocyanate, reacting to obtain a 4,4-diphenylmethane diisocyanate-polyether polyol prepolymer, performing composite sealing on the 4,4-diphenylmethane diisocyanate-polyether polyol prepolymer by using malonic acid diethyl ester, ethyl acetoacetate and 3,5-lutidine so as to obtain a polyisocyanates curing agent, and finally adding an amino chain expanding agent and a powder filling material into the compositely sealed polyisocyanates curing agent, thereby obtaining the compositely sealed polyisocyanates coating. When heated, the compositely sealed polyisocyanates coating prepared by using the method can be gradually unsealed and cured in different periods, the phenomenon of edge curtain coating of conventional singly sealed polyisocyanates in the baking process because of too high unsealing temperature is avoided, the filming property of the compositely sealed polyisocyanates coating is improved, a prepared film is relatively high in cross-linking degree, and thus good mechanical property is achieved.</abstract><oa>free_for_read</oa></addata></record> |
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subjects | ADHESIVES CHEMICAL PAINT OR INK REMOVERS CHEMISTRY COATING COMPOSITIONS, e.g. PAINTS, VARNISHES ORLACQUERS COMPOSITIONS BASED THEREON CORRECTING FLUIDS DYES FILLING PASTES INKS MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONSONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS METALLURGY MISCELLANEOUS APPLICATIONS OF MATERIALS MISCELLANEOUS COMPOSITIONS NATURAL RESINS ORGANIC MACROMOLECULAR COMPOUNDS PAINTS PASTES OR SOLIDS FOR COLOURING OR PRINTING POLISHES THEIR PREPARATION OR CHEMICAL WORKING-UP USE OF MATERIALS THEREFOR WOODSTAINS |
title | Method for preparing compositey sealed polyisocyanates coating |
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