PROCESS AND ARRANGEMENT FOR PREPARING SOLUTION OF CELLULOSE

For producing solutions of cellulose in water-containing tertiary amine oxides from a suspension of cellulose in an aqueous solution of the tertiary amine oxide by supplying heat under reduced pressure, the suspension having a viscosity between 50 and 15,000 Pas.sec, measured in a relative system, i...

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Hauptverfasser: STEFAN ZIKELI, BERND WOLSCHNER, DIETER EICHINGER
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creator STEFAN ZIKELI
BERND WOLSCHNER
DIETER EICHINGER
description For producing solutions of cellulose in water-containing tertiary amine oxides from a suspension of cellulose in an aqueous solution of the tertiary amine oxide by supplying heat under reduced pressure, the suspension having a viscosity between 50 and 15,000 Pas.sec, measured in a relative system, is spread as a layer or film over a heating surface and transported until a homogeneous solution of the cellulose is formed, the feeding of the suspension and the take-off of the homogeneous solution being carried out continuously. These solutions can be produced in an indirectly heated vessel which is provided with a stirring device and can be evacuated and which is designed as a cylindrical container (2) with a centrally mounted stirrer shaft (7) and stirrer blades (8) attached thereto, the radial distance (13) of the stirrer blades (8) from the inside wall (1) of the container (2) being at most 20 mm, and an inlet (11) for the cellulose suspension being provided in the upper part of the container and an outlet (12) for the homogeneous cellulose solution being provided at the lower end.
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These solutions can be produced in an indirectly heated vessel which is provided with a stirring device and can be evacuated and which is designed as a cylindrical container (2) with a centrally mounted stirrer shaft (7) and stirrer blades (8) attached thereto, the radial distance (13) of the stirrer blades (8) from the inside wall (1) of the container (2) being at most 20 mm, and an inlet (11) for the cellulose suspension being provided in the upper part of the container and an outlet (12) for the homogeneous cellulose solution being provided at the lower end.</description><edition>5</edition><language>eng</language><subject>AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F,C08G ; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBONFILAMENTS ; CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS,THREADS, FIBRES, BRISTLES OR RIBBONS ; CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOIDCHEMISTRY ; CHEMISTRY ; COMPOSITIONS BASED THEREON ; COMPOSITIONS OF MACROMOLECULAR COMPOUNDS ; DERIVATIVES THEREOF ; GENERAL PROCESSES OF COMPOUNDING ; MECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OFARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES ORRIBBONS ; METALLURGY ; MIXING, e.g. DISSOLVING, EMULSIFYING, DISPERSING ; NATURAL OR ARTIFICIAL THREADS OR FIBRES ; ORGANIC MACROMOLECULAR COMPOUNDS ; PERFORMING OPERATIONS ; PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL ; POLYSACCHARIDES ; SPINNING ; TEXTILES ; THEIR PREPARATION OR CHEMICAL WORKING-UP ; THEIR RELEVANT APPARATUS ; TRANSPORTING ; WORKING-UP</subject><creationdate>1990</creationdate><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&amp;date=19900516&amp;DB=EPODOC&amp;CC=CN&amp;NR=1042165A$$EHTML$$P50$$Gepo$$Hfree_for_read</linktohtml><link.rule.ids>230,308,780,885,25562,76317</link.rule.ids><linktorsrc>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&amp;date=19900516&amp;DB=EPODOC&amp;CC=CN&amp;NR=1042165A$$EView_record_in_European_Patent_Office$$FView_record_in_$$GEuropean_Patent_Office$$Hfree_for_read</linktorsrc></links><search><creatorcontrib>STEFAN ZIKELI</creatorcontrib><creatorcontrib>BERND WOLSCHNER</creatorcontrib><creatorcontrib>DIETER EICHINGER</creatorcontrib><title>PROCESS AND ARRANGEMENT FOR PREPARING SOLUTION OF CELLULOSE</title><description>For producing solutions of cellulose in water-containing tertiary amine oxides from a suspension of cellulose in an aqueous solution of the tertiary amine oxide by supplying heat under reduced pressure, the suspension having a viscosity between 50 and 15,000 Pas.sec, measured in a relative system, is spread as a layer or film over a heating surface and transported until a homogeneous solution of the cellulose is formed, the feeding of the suspension and the take-off of the homogeneous solution being carried out continuously. 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subjects AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F,C08G
APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBONFILAMENTS
CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS,THREADS, FIBRES, BRISTLES OR RIBBONS
CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOIDCHEMISTRY
CHEMISTRY
COMPOSITIONS BASED THEREON
COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
DERIVATIVES THEREOF
GENERAL PROCESSES OF COMPOUNDING
MECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OFARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES ORRIBBONS
METALLURGY
MIXING, e.g. DISSOLVING, EMULSIFYING, DISPERSING
NATURAL OR ARTIFICIAL THREADS OR FIBRES
ORGANIC MACROMOLECULAR COMPOUNDS
PERFORMING OPERATIONS
PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
POLYSACCHARIDES
SPINNING
TEXTILES
THEIR PREPARATION OR CHEMICAL WORKING-UP
THEIR RELEVANT APPARATUS
TRANSPORTING
WORKING-UP
title PROCESS AND ARRANGEMENT FOR PREPARING SOLUTION OF CELLULOSE
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