Method for preparing superfine CaSiO3 conductive powder in micro-composite mode
The invention relates to a method for preparing superfine CaSiO3 conductive powder in a micro-composite mode. The method comprises the steps that alcohol serves as a reaction medium, at the temperature ranging from 10 DEG C to 100 DEG C, soluble calcium salt and orthosilicate ester are added accordi...
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| creator | HAO ZHIJUN GUO FENG QIU LIPING JIANG JINXIAN ZHAO GUIQIAO ZOU ENGUANG DU WEI ZHAO XINGLONG WANG SIHAN WANG DENGFEI YANG GUOXING LI RUI LV HONGLI WANG GANG GAO YUXIN LIU DONGMEI XIAO BO GUO HAIFENG MA JIANYING HUANG QINGDONG LIU LIJUN SUN BINBIN |
| description | The invention relates to a method for preparing superfine CaSiO3 conductive powder in a micro-composite mode. The method comprises the steps that alcohol serves as a reaction medium, at the temperature ranging from 10 DEG C to 100 DEG C, soluble calcium salt and orthosilicate ester are added according to the mole ratio of 1:1 so that CaSiO3 superfine powder can be prepared; the use amount of the alcohol is 1 to 10 times that of the soluble calcium salt according the mole ratio; ammonium hydroxide with the mass percent concentration smaller than or equal to 10% is gradually dripped in a silver nitrate solution with the concentration smaller than or equal to 6mol/L, so that a clear and transparent silver ammonia solution is obtained; at the temperature ranging from 10 DEG C to 100 DEG C, a mixed solution is prepared through the silver ammonia solution and an aldehyde solution according to the volume ratio of 1:1 and the CaSiO3 conductive powder is prepared through the mixed solution and the CaSiO3 superfine pow |
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The method comprises the steps that alcohol serves as a reaction medium, at the temperature ranging from 10 DEG C to 100 DEG C, soluble calcium salt and orthosilicate ester are added according to the mole ratio of 1:1 so that CaSiO3 superfine powder can be prepared; the use amount of the alcohol is 1 to 10 times that of the soluble calcium salt according the mole ratio; ammonium hydroxide with the mass percent concentration smaller than or equal to 10% is gradually dripped in a silver nitrate solution with the concentration smaller than or equal to 6mol/L, so that a clear and transparent silver ammonia solution is obtained; at the temperature ranging from 10 DEG C to 100 DEG C, a mixed solution is prepared through the silver ammonia solution and an aldehyde solution according to the volume ratio of 1:1 and the CaSiO3 conductive powder is prepared through the mixed solution and the CaSiO3 superfine pow</description><language>chi ; eng</language><subject>BASIC ELECTRIC ELEMENTS ; CABLES ; CHEMICAL SURFACE TREATMENT ; CHEMISTRY ; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATIONOR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL ; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY IONIMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL ; COATING MATERIAL WITH METALLIC MATERIAL ; COATING METALLIC MATERIAL ; COMPOUNDS THEREOF ; CONDUCTORS ; DIFFUSION TREATMENT OF METALLIC MATERIAL ; ELECTRICITY ; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION INGENERAL ; INORGANIC CHEMISTRY ; INSULATORS ; METALLURGY ; NON-METALLIC ELEMENTS ; SELECTION OF MATERIALS FOR THEIR CONDUCTIVE, INSULATING ORDIELECTRIC PROPERTIES ; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THESURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION</subject><creationdate>2013</creationdate><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&date=20131204&DB=EPODOC&CC=CN&NR=103426562A$$EHTML$$P50$$Gepo$$Hfree_for_read</linktohtml><link.rule.ids>230,308,780,885,25564,76547</link.rule.ids><linktorsrc>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&date=20131204&DB=EPODOC&CC=CN&NR=103426562A$$EView_record_in_European_Patent_Office$$FView_record_in_$$GEuropean_Patent_Office$$Hfree_for_read</linktorsrc></links><search><creatorcontrib>HAO ZHIJUN</creatorcontrib><creatorcontrib>GUO FENG</creatorcontrib><creatorcontrib>QIU LIPING</creatorcontrib><creatorcontrib>JIANG JINXIAN</creatorcontrib><creatorcontrib>ZHAO GUIQIAO</creatorcontrib><creatorcontrib>ZOU ENGUANG</creatorcontrib><creatorcontrib>DU WEI</creatorcontrib><creatorcontrib>ZHAO XINGLONG</creatorcontrib><creatorcontrib>WANG SIHAN</creatorcontrib><creatorcontrib>WANG DENGFEI</creatorcontrib><creatorcontrib>YANG GUOXING</creatorcontrib><creatorcontrib>LI RUI</creatorcontrib><creatorcontrib>LV HONGLI</creatorcontrib><creatorcontrib>WANG GANG</creatorcontrib><creatorcontrib>GAO YUXIN</creatorcontrib><creatorcontrib>LIU DONGMEI</creatorcontrib><creatorcontrib>XIAO BO</creatorcontrib><creatorcontrib>GUO HAIFENG</creatorcontrib><creatorcontrib>MA JIANYING</creatorcontrib><creatorcontrib>HUANG QINGDONG</creatorcontrib><creatorcontrib>LIU LIJUN</creatorcontrib><creatorcontrib>SUN BINBIN</creatorcontrib><title>Method for preparing superfine CaSiO3 conductive powder in micro-composite mode</title><description>The invention relates to a method for preparing superfine CaSiO3 conductive powder in a micro-composite mode. 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The method comprises the steps that alcohol serves as a reaction medium, at the temperature ranging from 10 DEG C to 100 DEG C, soluble calcium salt and orthosilicate ester are added according to the mole ratio of 1:1 so that CaSiO3 superfine powder can be prepared; the use amount of the alcohol is 1 to 10 times that of the soluble calcium salt according the mole ratio; ammonium hydroxide with the mass percent concentration smaller than or equal to 10% is gradually dripped in a silver nitrate solution with the concentration smaller than or equal to 6mol/L, so that a clear and transparent silver ammonia solution is obtained; at the temperature ranging from 10 DEG C to 100 DEG C, a mixed solution is prepared through the silver ammonia solution and an aldehyde solution according to the volume ratio of 1:1 and the CaSiO3 conductive powder is prepared through the mixed solution and the CaSiO3 superfine pow</abstract><oa>free_for_read</oa></addata></record> |
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| subjects | BASIC ELECTRIC ELEMENTS CABLES CHEMICAL SURFACE TREATMENT CHEMISTRY COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATIONOR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY IONIMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL COATING MATERIAL WITH METALLIC MATERIAL COATING METALLIC MATERIAL COMPOUNDS THEREOF CONDUCTORS DIFFUSION TREATMENT OF METALLIC MATERIAL ELECTRICITY INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION INGENERAL INORGANIC CHEMISTRY INSULATORS METALLURGY NON-METALLIC ELEMENTS SELECTION OF MATERIALS FOR THEIR CONDUCTIVE, INSULATING ORDIELECTRIC PROPERTIES SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THESURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION |
| title | Method for preparing superfine CaSiO3 conductive powder in micro-composite mode |
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