Preparation method of sulfonated carbon nano tube (CNT) loaded polyaniline nanorod super capacitor electrode material
The invention relates to a preparation method of a sulfonated CNT loaded polyaniline nanorod super capacitor electrode material, comprising the following steps of: (1) ultrasonically processing a CNT and subjecting the CNT to diazotization reaction with diazosalt of sulfanilic acid so as to obtain a...
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| creator | WANG GENGCHAO LI XINGWEI ZHU ZHONGZE SUN MINQIANG |
| description | The invention relates to a preparation method of a sulfonated CNT loaded polyaniline nanorod super capacitor electrode material, comprising the following steps of: (1) ultrasonically processing a CNT and subjecting the CNT to diazotization reaction with diazosalt of sulfanilic acid so as to obtain a water soluble sulfonated CNT; (2) carrying out a chemical oxidation polymerization method to prepare a sulfonated CNT loaded polyaniline nanorod conductive composite material by employing the water soluble sulfonated CNT as a carrier, selecting the protonic acid with large-size acid radical ions as a reaction medium, employing the aniline as a reaction monomer, employing the ammonium persulfate as an oxidant and controlling the mole ratio of the ammonium persulfate to the aniline monomer to be less than 2; and (3) performing oxidation post-processing to the composite material by adopting the oxidant so as to prepare the sulfonated CNT loaded polyaniline nanorod super capacitor electrode material. The invention has |
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The invention has</description><language>chi ; eng</language><subject>BASIC ELECTRIC ELEMENTS ; CAPACITORS ; CAPACITORS, RECTIFIERS, DETECTORS, SWITCHING DEVICES ORLIGHT-SENSITIVE DEVICES, OF THE ELECTROLYTIC TYPE ; CHEMISTRY ; COMPOSITIONS BASED THEREON ; COMPOSITIONS OF MACROMOLECULAR COMPOUNDS ; ELECTRICITY ; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC ; GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS ; MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONSONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS ; METALLURGY ; ORGANIC MACROMOLECULAR COMPOUNDS ; REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGYGENERATION, TRANSMISSION OR DISTRIBUTION ; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS ; TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINSTCLIMATE CHANGE ; THEIR PREPARATION OR CHEMICAL WORKING-UP ; USE OF INORGANIC OR NON-MACROMOLECULAR ORGANIC SUBSTANCES ASCOMPOUNDING INGREDIENTS</subject><creationdate>2011</creationdate><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&date=20110105&DB=EPODOC&CC=CN&NR=101935452A$$EHTML$$P50$$Gepo$$Hfree_for_read</linktohtml><link.rule.ids>230,308,780,885,25564,76547</link.rule.ids><linktorsrc>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&date=20110105&DB=EPODOC&CC=CN&NR=101935452A$$EView_record_in_European_Patent_Office$$FView_record_in_$$GEuropean_Patent_Office$$Hfree_for_read</linktorsrc></links><search><creatorcontrib>WANG GENGCHAO</creatorcontrib><creatorcontrib>LI XINGWEI</creatorcontrib><creatorcontrib>ZHU ZHONGZE</creatorcontrib><creatorcontrib>SUN MINQIANG</creatorcontrib><title>Preparation method of sulfonated carbon nano tube (CNT) loaded polyaniline nanorod super capacitor electrode material</title><description>The invention relates to a preparation method of a sulfonated CNT loaded polyaniline nanorod super capacitor electrode material, comprising the following steps of: (1) ultrasonically processing a CNT and subjecting the CNT to diazotization reaction with diazosalt of sulfanilic acid so as to obtain a water soluble sulfonated CNT; (2) carrying out a chemical oxidation polymerization method to prepare a sulfonated CNT loaded polyaniline nanorod conductive composite material by employing the water soluble sulfonated CNT as a carrier, selecting the protonic acid with large-size acid radical ions as a reaction medium, employing the aniline as a reaction monomer, employing the ammonium persulfate as an oxidant and controlling the mole ratio of the ammonium persulfate to the aniline monomer to be less than 2; and (3) performing oxidation post-processing to the composite material by adopting the oxidant so as to prepare the sulfonated CNT loaded polyaniline nanorod super capacitor electrode material. 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(2) carrying out a chemical oxidation polymerization method to prepare a sulfonated CNT loaded polyaniline nanorod conductive composite material by employing the water soluble sulfonated CNT as a carrier, selecting the protonic acid with large-size acid radical ions as a reaction medium, employing the aniline as a reaction monomer, employing the ammonium persulfate as an oxidant and controlling the mole ratio of the ammonium persulfate to the aniline monomer to be less than 2; and (3) performing oxidation post-processing to the composite material by adopting the oxidant so as to prepare the sulfonated CNT loaded polyaniline nanorod super capacitor electrode material. The invention has</abstract><oa>free_for_read</oa></addata></record> |
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| subjects | BASIC ELECTRIC ELEMENTS CAPACITORS CAPACITORS, RECTIFIERS, DETECTORS, SWITCHING DEVICES ORLIGHT-SENSITIVE DEVICES, OF THE ELECTROLYTIC TYPE CHEMISTRY COMPOSITIONS BASED THEREON COMPOSITIONS OF MACROMOLECULAR COMPOUNDS ELECTRICITY GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONSONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS METALLURGY ORGANIC MACROMOLECULAR COMPOUNDS REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGYGENERATION, TRANSMISSION OR DISTRIBUTION TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINSTCLIMATE CHANGE THEIR PREPARATION OR CHEMICAL WORKING-UP USE OF INORGANIC OR NON-MACROMOLECULAR ORGANIC SUBSTANCES ASCOMPOUNDING INGREDIENTS |
| title | Preparation method of sulfonated carbon nano tube (CNT) loaded polyaniline nanorod super capacitor electrode material |
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