Preparation method of biomass cellulose nanofibers with high length-diameter ratio
The invention relates to a preparation method of biomass cellulose nanofibers with a high length-diameter ratio, in particular to a preparation method of nano cellulose fibers, solving the problems that nano cellulose fibers prepared by using a traditional method for hydrolyzing biomass cellulose wi...
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creator | ZHANG MINGXIN CHEN WENSHUAI YU HAIPENG CHEN PENG LIU YIXING HAI YUNFEI |
description | The invention relates to a preparation method of biomass cellulose nanofibers with a high length-diameter ratio, in particular to a preparation method of nano cellulose fibers, solving the problems that nano cellulose fibers prepared by using a traditional method for hydrolyzing biomass cellulose with strong acid have short length and small length-diameter ratio, nano cellulose fibers prepared byusing a mechanical shearing method are easy to mutually aggregate, and a microbial fermentation method has high cost. The method comprises the following steps of: (1) purifying biomass cellulose witha benzyl alcohol solution; (2); treating with acidified sodium chlorite; (3) treating lye; (4) treating with the acidified sodium chlorite again; (5) treating with KOH; (6) treating with hydrochloricacid; and (7) ultrasonically treating and drying to obtain biomass cellulose nanofibers with high length-diameter ratio not less than 1500, fiber diameter from 50 nm to 300 nm, length not less than 150 um and length-diameter ra |
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The method comprises the following steps of: (1) purifying biomass cellulose witha benzyl alcohol solution; (2); treating with acidified sodium chlorite; (3) treating lye; (4) treating with the acidified sodium chlorite again; (5) treating with KOH; (6) treating with hydrochloricacid; and (7) ultrasonically treating and drying to obtain biomass cellulose nanofibers with high length-diameter ratio not less than 1500, fiber diameter from 50 nm to 300 nm, length not less than 150 um and length-diameter ra</description><language>chi ; eng</language><subject>APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBONFILAMENTS ; CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS,THREADS, FIBRES, BRISTLES OR RIBBONS ; NATURAL OR ARTIFICIAL THREADS OR FIBRES ; SPINNING ; TEXTILES</subject><creationdate>2011</creationdate><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&date=20110907&DB=EPODOC&CC=CN&NR=101864606B$$EHTML$$P50$$Gepo$$Hfree_for_read</linktohtml><link.rule.ids>230,308,780,885,25563,76318</link.rule.ids><linktorsrc>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&date=20110907&DB=EPODOC&CC=CN&NR=101864606B$$EView_record_in_European_Patent_Office$$FView_record_in_$$GEuropean_Patent_Office$$Hfree_for_read</linktorsrc></links><search><creatorcontrib>ZHANG MINGXIN</creatorcontrib><creatorcontrib>CHEN WENSHUAI</creatorcontrib><creatorcontrib>YU HAIPENG</creatorcontrib><creatorcontrib>CHEN PENG</creatorcontrib><creatorcontrib>LIU YIXING</creatorcontrib><creatorcontrib>HAI YUNFEI</creatorcontrib><title>Preparation method of biomass cellulose nanofibers with high length-diameter ratio</title><description>The invention relates to a preparation method of biomass cellulose nanofibers with a high length-diameter ratio, in particular to a preparation method of nano cellulose fibers, solving the problems that nano cellulose fibers prepared by using a traditional method for hydrolyzing biomass cellulose with strong acid have short length and small length-diameter ratio, nano cellulose fibers prepared byusing a mechanical shearing method are easy to mutually aggregate, and a microbial fermentation method has high cost. 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The method comprises the following steps of: (1) purifying biomass cellulose witha benzyl alcohol solution; (2); treating with acidified sodium chlorite; (3) treating lye; (4) treating with the acidified sodium chlorite again; (5) treating with KOH; (6) treating with hydrochloricacid; and (7) ultrasonically treating and drying to obtain biomass cellulose nanofibers with high length-diameter ratio not less than 1500, fiber diameter from 50 nm to 300 nm, length not less than 150 um and length-diameter ra</abstract><oa>free_for_read</oa></addata></record> |
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subjects | APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBONFILAMENTS CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS,THREADS, FIBRES, BRISTLES OR RIBBONS NATURAL OR ARTIFICIAL THREADS OR FIBRES SPINNING TEXTILES |
title | Preparation method of biomass cellulose nanofibers with high length-diameter ratio |
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