Method for producing acrylonitrile compound
The present invention provides a method for producing 3-acyloxyacrylonitrile compound represented by the formula (1), wherein Ar is 4-tert-butyl benzene, Ar is 1, 3, 5-trimethyl5-pyrazole. The method is characterized in that reacting an acetonitrile compound represented by the formula (5) (wherein A...
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creator | TANAKA NORIO ONARI MASATOSHI SUZUKI HIDEAKI KONDO YASUO NISHIO KOICHI FUKUDA KENZO |
description | The present invention provides a method for producing 3-acyloxyacrylonitrile compound represented by the formula (1), wherein Ar is 4-tert-butyl benzene, Ar is 1, 3, 5-trimethyl5-pyrazole. The method is characterized in that reacting an acetonitrile compound represented by the formula (5) (wherein Ar is 4-tert-butyl benzene) with an aromatic ester compound represented by the formula (6) (wherein Ar is 1, 3, 5-trimethyl5-pyrazole, R is alkyl) in a hydrocarbon solvent with the aid of an alkali metal alkoxide while removing the by-product alcohol by azeotropic distillation in a separating tank. |
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The method is characterized in that reacting an acetonitrile compound represented by the formula (5) (wherein Ar is 4-tert-butyl benzene) with an aromatic ester compound represented by the formula (6) (wherein Ar is 1, 3, 5-trimethyl5-pyrazole, R is alkyl) in a hydrocarbon solvent with the aid of an alkali metal alkoxide while removing the by-product alcohol by azeotropic distillation in a separating tank.</description><subject>CHEMISTRY</subject><subject>HETEROCYCLIC COMPOUNDS</subject><subject>METALLURGY</subject><subject>ORGANIC CHEMISTRY</subject><fulltext>true</fulltext><rsrctype>patent</rsrctype><creationdate>2011</creationdate><recordtype>patent</recordtype><sourceid>EVB</sourceid><recordid>eNrjZND2TS3JyE9RSMsvUigoyk8pTc7MS1dITC6qzMnPyywpysxJVUjOzy3IL81L4WFgTUvMKU7lhdLcDEpuriHOHrqpBfnxqcUFicmpeakl8c5-hgaGRhYmFoYmTk7GRCkCAOgoKm0</recordid><startdate>20110817</startdate><enddate>20110817</enddate><creator>TANAKA NORIO</creator><creator>ONARI MASATOSHI</creator><creator>SUZUKI HIDEAKI</creator><creator>KONDO YASUO</creator><creator>NISHIO KOICHI</creator><creator>FUKUDA KENZO</creator><scope>EVB</scope></search><sort><creationdate>20110817</creationdate><title>Method for producing acrylonitrile compound</title><author>TANAKA NORIO ; ONARI MASATOSHI ; SUZUKI HIDEAKI ; KONDO YASUO ; NISHIO KOICHI ; FUKUDA KENZO</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-epo_espacenet_CN101284814BB3</frbrgroupid><rsrctype>patents</rsrctype><prefilter>patents</prefilter><language>chi ; eng</language><creationdate>2011</creationdate><topic>CHEMISTRY</topic><topic>HETEROCYCLIC COMPOUNDS</topic><topic>METALLURGY</topic><topic>ORGANIC CHEMISTRY</topic><toplevel>online_resources</toplevel><creatorcontrib>TANAKA NORIO</creatorcontrib><creatorcontrib>ONARI MASATOSHI</creatorcontrib><creatorcontrib>SUZUKI HIDEAKI</creatorcontrib><creatorcontrib>KONDO YASUO</creatorcontrib><creatorcontrib>NISHIO KOICHI</creatorcontrib><creatorcontrib>FUKUDA KENZO</creatorcontrib><collection>esp@cenet</collection></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext_linktorsrc</fulltext></delivery><addata><au>TANAKA NORIO</au><au>ONARI MASATOSHI</au><au>SUZUKI HIDEAKI</au><au>KONDO YASUO</au><au>NISHIO KOICHI</au><au>FUKUDA KENZO</au><format>patent</format><genre>patent</genre><ristype>GEN</ristype><title>Method for producing acrylonitrile compound</title><date>2011-08-17</date><risdate>2011</risdate><abstract>The present invention provides a method for producing 3-acyloxyacrylonitrile compound represented by the formula (1), wherein Ar is 4-tert-butyl benzene, Ar is 1, 3, 5-trimethyl5-pyrazole. 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title | Method for producing acrylonitrile compound |
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