METHOD OF PREPARING PRIMARY REFRACTORY METAL

A method of preparing primary refractory metals (e.g., primary tantalum metal) by contacting a particulate refractory metal oxide (e.g., tantalum pentoxide) with a heated gas (e.g., a plasma), is described. The heated gas comprises hydrogen gas. The temperature range of the heated gas and the mass r...

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Hauptverfasser: LANIN, LEONID, GREVILLE, HUGH P, SHEKHTER, LEONID NATAN, SIMKINS, LEAH F
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creator LANIN, LEONID
GREVILLE, HUGH P
SHEKHTER, LEONID NATAN
SIMKINS, LEAH F
description A method of preparing primary refractory metals (e.g., primary tantalum metal) by contacting a particulate refractory metal oxide (e.g., tantalum pentoxide) with a heated gas (e.g., a plasma), is described. The heated gas comprises hydrogen gas. The temperature range of the heated gas and the mass ratio of hydrogen gas to refractory metal oxide are each selected such that: (i) the heated gas comprises atomic hydrogen; (ii) the refractory metal oxide feed material is substantially thermodynamically stabilized (i.e., the concurrent formation of suboxides that are not reduced by atomic hydrogen is minimized); and (iii) the refractory metal oxide is reduced by contact with the heated gas, thereby forming primary refractory metal (e.g., primary tantalum metal and/or primary niobium metal).
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subjects CHEMISTRY
FERROUS OR NON-FERROUS ALLOYS
METALLURGY
PRETREATMENT OF RAW MATERIALS
PRODUCTION AND REFINING OF METALS
TREATMENT OF ALLOYS OR NON-FERROUS METALS
title METHOD OF PREPARING PRIMARY REFRACTORY METAL
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