SPECTROSCOPY-BASED REAL-TIME CONTROL FOR MICROWAVE-ASSISTED CHEMISTRY

The invention is an instrument and method for microwave-assisted chemical synthesis. The instrument includes a source of microwave radiation for applying microwave energy to a sample, a microwave cavity in wave communication with the source for holding the sample during the application of microwave...

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Hauptverfasser: COLLINS, MICHAEL JOHN, JR, MCMANUS, MICHAEL E, COLLINS, MICHAEL JOHN, SR
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Sprache:eng ; fre
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creator COLLINS, MICHAEL JOHN, JR
MCMANUS, MICHAEL E
COLLINS, MICHAEL JOHN, SR
description The invention is an instrument and method for microwave-assisted chemical synthesis. The instrument includes a source of microwave radiation for applying microwave energy to a sample, a microwave cavity in wave communication with the source for holding the sample during the application of microwave energy, an d a substantially monochromatic radiation source in electromagnetic communicatio n with the cavity for applying substantially monochromatic light to the sample. The instrument further includes a detector positioned to detect Raman scattering of light from the monochromatic source by the sample, and a controller in signal communication with the microwave energy source and the Raman scattering detector for moderating the application of microwave energy to the sample based upon the detected Raman scattering.
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subjects CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOIDCHEMISTRY
INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIRCHEMICAL OR PHYSICAL PROPERTIES
MEASURING
PERFORMING OPERATIONS
PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
PHYSICS
TESTING
THEIR RELEVANT APPARATUS
TRANSPORTING
title SPECTROSCOPY-BASED REAL-TIME CONTROL FOR MICROWAVE-ASSISTED CHEMISTRY
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