Process for separating hydrogen fluoride from its mixtures with 1,1,1-trifluoro-2-chloroethane

Separation of hydrogen fluoride (HF) from its mixtures with 1,1,1-trifluoro-2-chloroethane (F133a). By settling the mixture of HF and F133a at a temperature below 0 DEG C, there is obtained a lower organic phase which is poor in HF and an upper phase which is rich in HF. The latter can be directly r...

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1. Verfasser:	BERNARD BERTHE
Format:	Patent
Sprache:	eng
Schlagworte:	ACYCLIC OR CARBOCYCLIC COMPOUNDS CHEMISTRY COMPOUNDS THEREOF INORGANIC CHEMISTRY METALLURGY NON-METALLIC ELEMENTS ORGANIC CHEMISTRY
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creator	BERNARD BERTHE
description	Separation of hydrogen fluoride (HF) from its mixtures with 1,1,1-trifluoro-2-chloroethane (F133a). By settling the mixture of HF and F133a at a temperature below 0 DEG C, there is obtained a lower organic phase which is poor in HF and an upper phase which is rich in HF. The latter can be directly recycled to the fluorination reactor or subjected to a distillation to separate the HF/F133a azeotrope at the head, which is sent back to the settler, and to recover practically pure HF at the base. By distillation of the lower phase, the HF/F133a azeotrope is separated at the head, which is sent back to the settler, and F133a is recovered at the base.
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By settling the mixture of HF and F133a at a temperature below 0 DEG C, there is obtained a lower organic phase which is poor in HF and an upper phase which is rich in HF. The latter can be directly recycled to the fluorination reactor or subjected to a distillation to separate the HF/F133a azeotrope at the head, which is sent back to the settler, and to recover practically pure HF at the base. By distillation of the lower phase, the HF/F133a azeotrope is separated at the head, which is sent back to the settler, and F133a is recovered at the base.</description><edition>5</edition><language>eng</language><subject>ACYCLIC OR CARBOCYCLIC COMPOUNDS ; CHEMISTRY ; COMPOUNDS THEREOF ; INORGANIC CHEMISTRY ; METALLURGY ; NON-METALLIC ELEMENTS ; ORGANIC CHEMISTRY</subject><creationdate>1994</creationdate><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&date=19940616&DB=EPODOC&CC=AU&NR=650333B2$$EHTML$$P50$$Gepo$$Hfree_for_read</linktohtml><link.rule.ids>230,308,776,881,25543,76293</link.rule.ids><linktorsrc>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&date=19940616&DB=EPODOC&CC=AU&NR=650333B2$$EView_record_in_European_Patent_Office$$FView_record_in_$$GEuropean_Patent_Office$$Hfree_for_read</linktorsrc></links><search><creatorcontrib>BERNARD BERTHE</creatorcontrib><title>Process for separating hydrogen fluoride from its mixtures with 1,1,1-trifluoro-2-chloroethane</title><description>Separation of hydrogen fluoride (HF) from its mixtures with 1,1,1-trifluoro-2-chloroethane (F133a). 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By settling the mixture of HF and F133a at a temperature below 0 DEG C, there is obtained a lower organic phase which is poor in HF and an upper phase which is rich in HF. The latter can be directly recycled to the fluorination reactor or subjected to a distillation to separate the HF/F133a azeotrope at the head, which is sent back to the settler, and to recover practically pure HF at the base. By distillation of the lower phase, the HF/F133a azeotrope is separated at the head, which is sent back to the settler, and F133a is recovered at the base.</abstract><edition>5</edition><oa>free_for_read</oa></addata></record>
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subjects	ACYCLIC OR CARBOCYCLIC COMPOUNDS CHEMISTRY COMPOUNDS THEREOF INORGANIC CHEMISTRY METALLURGY NON-METALLIC ELEMENTS ORGANIC CHEMISTRY
title	Process for separating hydrogen fluoride from its mixtures with 1,1,1-trifluoro-2-chloroethane
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