VERFAHREN ZUR REINIGUNG VON POLYETHERPOLYOLEN, HERGESTELLT MIT DOPPELMETALLCYANID-KATALYSATOREN

Purificn. of a poly(oxypropylene) polyol is effected by (a) combining a polyol that contains double metal cyanide (DMC) catalyst residues with an amt. of an alkali metal cpd. sufficient to convert the catalyst residues to an insoluble species but not sufficient to generate polyol alkoxide gps., (b)...

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description Purificn. of a poly(oxypropylene) polyol is effected by (a) combining a polyol that contains double metal cyanide (DMC) catalyst residues with an amt. of an alkali metal cpd. sufficient to convert the catalyst residues to an insoluble species but not sufficient to generate polyol alkoxide gps., (b) heating the mixt. in the absence of magnesium silicate with at least ca. 1.5 wt.% water based on polyol, at 80-150 [deg] C; (c) filtering the polyol mixt. to remove insoluble catalyst residues; and (d) stripping the polyol mixt. to remove water.
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subjects CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOIDCHEMISTRY
CHEMISTRY
COMPOSITIONS BASED THEREON
MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONSONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
METALLURGY
ORGANIC MACROMOLECULAR COMPOUNDS
PERFORMING OPERATIONS
PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
THEIR PREPARATION OR CHEMICAL WORKING-UP
THEIR RELEVANT APPARATUS
TRANSPORTING
title VERFAHREN ZUR REINIGUNG VON POLYETHERPOLYOLEN, HERGESTELLT MIT DOPPELMETALLCYANID-KATALYSATOREN
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