Synthesis of Zeolite from Electrolytic Manganese Residue: Investigation on the Variation of the Propert of Zeolite during the Conversion Process
In this study, the cation exchange capacity (CEC); phosphate immobilization capacity (PIC); and chemical, mineralogical, and morphological characteristics of the synthesized electrolytic manganese residue (EMR) based zeolite (EMRZ) were systematically investigated during the synthesis process. By va...
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| Veröffentlicht in: | Journal of chemistry 2020-08, Vol.2020 (2020), p.1-9, Article 6939101 |
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| creator | Zhong, Hong Zhang, Qingwu Yu, Yuan Li, Changxin Wang, Shuai |
| description | In this study, the cation exchange capacity (CEC); phosphate immobilization capacity (PIC); and chemical, mineralogical, and morphological characteristics of the synthesized electrolytic manganese residue (EMR) based zeolite (EMRZ) were systematically investigated during the synthesis process. By varying synthesis conditions, different zeolites with different purity were generated, and it was proven that a lower Si/Al ratio, relatively higher temperature, and relatively longer time favored the synthesis of zeolite. Besides, the decrease in Si/Al ratio and variation within a narrow range contributed to the forming of Al rich zeolite. Meanwhile, the discrepancy of CEC and PIC of EMRZ contributed to the case in which various elements in EMRZ do have an impact on CEC (Na2O element and type of zeolite) and PIC (calcium and iron components). Moreover, the synthesis conditions were optimized and evaluated in terms of their CEC, specific surface area (SSA), and crystallinity. According to the analyses using XRD, FE-SEM, and XRF and the SSA analysis, the EMRZ (mainly zeolite A, LTA) synthesized under the optimum conditions (initial Si/Al ratio of 1.5, at 100°C, for 1.5 h) was found to be mainly composed of highly ordered cubic zeolites A crystals with a Si/Al ratio of 1.02 and a CEC of 3.45 meq/g. |
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By varying synthesis conditions, different zeolites with different purity were generated, and it was proven that a lower Si/Al ratio, relatively higher temperature, and relatively longer time favored the synthesis of zeolite. Besides, the decrease in Si/Al ratio and variation within a narrow range contributed to the forming of Al rich zeolite. Meanwhile, the discrepancy of CEC and PIC of EMRZ contributed to the case in which various elements in EMRZ do have an impact on CEC (Na2O element and type of zeolite) and PIC (calcium and iron components). Moreover, the synthesis conditions were optimized and evaluated in terms of their CEC, specific surface area (SSA), and crystallinity. According to the analyses using XRD, FE-SEM, and XRF and the SSA analysis, the EMRZ (mainly zeolite A, LTA) synthesized under the optimum conditions (initial Si/Al ratio of 1.5, at 100°C, for 1.5 h) was found to be mainly composed of highly ordered cubic zeolites A crystals with a Si/Al ratio of 1.02 and a CEC of 3.45 meq/g.</description><identifier>ISSN: 2090-9063</identifier><identifier>EISSN: 2090-9071</identifier><identifier>DOI: 10.1155/2020/6939101</identifier><language>eng</language><publisher>Cairo, Egypt: Hindawi Publishing Corporation</publisher><subject>Adsorption ; Aluminum ; Analysis ; Cation exchanging ; Chemistry ; Chemistry, Multidisciplinary ; Investigations ; Manganese ; Mineralogy ; Phosphates ; Physical Sciences ; Pollutants ; Production capacity ; Residues ; Science & Technology ; Silicon ; Zeolites</subject><ispartof>Journal of chemistry, 2020-08, Vol.2020 (2020), p.1-9, Article 6939101</ispartof><rights>Copyright © 2020 Changxin Li et al.</rights><rights>COPYRIGHT 2020 John Wiley & Sons, Inc.</rights><rights>Copyright © 2020 Changxin Li et al. This is an open access article distributed under the Creative Commons Attribution License (the “License”), which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited. 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Zhang, Qingwu ; Yu, Yuan ; Li, Changxin ; Wang, Shuai</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c517t-c7de55bafd81fac53dfb2e7fd425a91be183cb32454987d23485c927561365493</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2020</creationdate><topic>Adsorption</topic><topic>Aluminum</topic><topic>Analysis</topic><topic>Cation exchanging</topic><topic>Chemistry</topic><topic>Chemistry, Multidisciplinary</topic><topic>Investigations</topic><topic>Manganese</topic><topic>Mineralogy</topic><topic>Phosphates</topic><topic>Physical Sciences</topic><topic>Pollutants</topic><topic>Production capacity</topic><topic>Residues</topic><topic>Science & Technology</topic><topic>Silicon</topic><topic>Zeolites</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Zhong, Hong</creatorcontrib><creatorcontrib>Zhang, Qingwu</creatorcontrib><creatorcontrib>Yu, Yuan</creatorcontrib><creatorcontrib>Li, Changxin</creatorcontrib><creatorcontrib>Wang, Shuai</creatorcontrib><collection>الدوريات العلمية والإحصائية - e-Marefa Academic and Statistical Periodicals</collection><collection>معرفة - المحتوى العربي الأكاديمي المتكامل - e-Marefa Academic Complete</collection><collection>Hindawi Publishing Complete</collection><collection>Hindawi Publishing Subscription Journals</collection><collection>Hindawi Publishing Open Access Journals</collection><collection>Web of Science - Science Citation Index Expanded - 2020</collection><collection>Web of Science Core Collection</collection><collection>Science Citation Index Expanded</collection><collection>CrossRef</collection><collection>ProQuest SciTech Collection</collection><collection>ProQuest Technology Collection</collection><collection>Materials Science & Engineering Collection</collection><collection>ProQuest Central (Alumni Edition)</collection><collection>ProQuest Central UK/Ireland</collection><collection>ProQuest Central Essentials</collection><collection>ProQuest Central</collection><collection>Technology Collection</collection><collection>ProQuest One Community College</collection><collection>ProQuest Materials Science Collection</collection><collection>ProQuest Central Korea</collection><collection>SciTech Premium Collection</collection><collection>Materials Science Database</collection><collection>Materials Science Collection</collection><collection>Access via ProQuest (Open Access)</collection><collection>ProQuest One Academic Eastern Edition (DO NOT USE)</collection><collection>ProQuest One Academic</collection><collection>ProQuest One Academic UKI Edition</collection><collection>ProQuest Central China</collection><collection>DOAJ Directory of Open Access Journals</collection><jtitle>Journal of chemistry</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Zhong, Hong</au><au>Zhang, Qingwu</au><au>Yu, Yuan</au><au>Li, Changxin</au><au>Wang, Shuai</au><au>Mancini, Pedro M.</au><au>Pedro M Mancini</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Synthesis of Zeolite from Electrolytic Manganese Residue: Investigation on the Variation of the Propert of Zeolite during the Conversion Process</atitle><jtitle>Journal of chemistry</jtitle><stitle>J CHEM-NY</stitle><date>2020-08-17</date><risdate>2020</risdate><volume>2020</volume><issue>2020</issue><spage>1</spage><epage>9</epage><pages>1-9</pages><artnum>6939101</artnum><issn>2090-9063</issn><eissn>2090-9071</eissn><abstract>In this study, the cation exchange capacity (CEC); phosphate immobilization capacity (PIC); and chemical, mineralogical, and morphological characteristics of the synthesized electrolytic manganese residue (EMR) based zeolite (EMRZ) were systematically investigated during the synthesis process. By varying synthesis conditions, different zeolites with different purity were generated, and it was proven that a lower Si/Al ratio, relatively higher temperature, and relatively longer time favored the synthesis of zeolite. Besides, the decrease in Si/Al ratio and variation within a narrow range contributed to the forming of Al rich zeolite. Meanwhile, the discrepancy of CEC and PIC of EMRZ contributed to the case in which various elements in EMRZ do have an impact on CEC (Na2O element and type of zeolite) and PIC (calcium and iron components). Moreover, the synthesis conditions were optimized and evaluated in terms of their CEC, specific surface area (SSA), and crystallinity. According to the analyses using XRD, FE-SEM, and XRF and the SSA analysis, the EMRZ (mainly zeolite A, LTA) synthesized under the optimum conditions (initial Si/Al ratio of 1.5, at 100°C, for 1.5 h) was found to be mainly composed of highly ordered cubic zeolites A crystals with a Si/Al ratio of 1.02 and a CEC of 3.45 meq/g.</abstract><cop>Cairo, Egypt</cop><pub>Hindawi Publishing Corporation</pub><doi>10.1155/2020/6939101</doi><tpages>9</tpages><orcidid>https://orcid.org/0000-0002-7728-8677</orcidid><orcidid>https://orcid.org/0000-0002-5108-9178</orcidid><oa>free_for_read</oa></addata></record> |
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| subjects | Adsorption Aluminum Analysis Cation exchanging Chemistry Chemistry, Multidisciplinary Investigations Manganese Mineralogy Phosphates Physical Sciences Pollutants Production capacity Residues Science & Technology Silicon Zeolites |
| title | Synthesis of Zeolite from Electrolytic Manganese Residue: Investigation on the Variation of the Propert of Zeolite during the Conversion Process |
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