GAS CHROMATOGRAPHIC DETERMINATION OF METHYL CENTRALITE AND DIPHENYLAMINE IN 20-MM GUN PROPELLANT
This report presents a rapid procedure for precise determinations of both methyl centralite (MC), also known as dimethyldiphenylurea, and diphenylamine (DPA). The sample is extracted with methylene chloride, removing the MC and DPA. The extract is blown to dryness with dry air, dissolved in ethylene...
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creator | Alston, Percy L Den Hartog, Laura J Oesterling, David H Shafer, James E |
description | This report presents a rapid procedure for precise determinations of both methyl centralite (MC), also known as dimethyldiphenylurea, and diphenylamine (DPA). The sample is extracted with methylene chloride, removing the MC and DPA. The extract is blown to dryness with dry air, dissolved in ethylene dichloride, and analyzed on a Perkin-Elmer 226 Flame Chromatograph. |
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The sample is extracted with methylene chloride, removing the MC and DPA. The extract is blown to dryness with dry air, dissolved in ethylene dichloride, and analyzed on a Perkin-Elmer 226 Flame Chromatograph.</description><language>eng</language><subject>AMINES ; Ammunition and Explosives ; AROMATIC COMPOUNDS ; CHLORIDES ; CORROSION ; DIPHENYLAMINE ; ETHYLENES ; GAS CHROMATOGRAPHY ; GUNS ; METHYL CENTRALITE ; Physical Chemistry ; POLYCYCLIC COMPOUNDS ; PROPELLANTS ; QUANTITATIVE ANALYSIS ; STABILITY ; STORAGE ; TEMPERATURE</subject><creationdate>1966</creationdate><rights>Approved for public release; distribution is unlimited.</rights><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>230,780,885,27567,27568</link.rule.ids><linktorsrc>$$Uhttps://apps.dtic.mil/sti/citations/AD0805926$$EView_record_in_DTIC$$FView_record_in_$$GDTIC$$Hfree_for_read</linktorsrc></links><search><creatorcontrib>Alston, Percy L</creatorcontrib><creatorcontrib>Den Hartog, Laura J</creatorcontrib><creatorcontrib>Oesterling, David H</creatorcontrib><creatorcontrib>Shafer, James E</creatorcontrib><creatorcontrib>NAVAL ORDNANCE STATION INDIAN HEAD MD QUALITY ASSURANCE DEPT</creatorcontrib><title>GAS CHROMATOGRAPHIC DETERMINATION OF METHYL CENTRALITE AND DIPHENYLAMINE IN 20-MM GUN PROPELLANT</title><description>This report presents a rapid procedure for precise determinations of both methyl centralite (MC), also known as dimethyldiphenylurea, and diphenylamine (DPA). The sample is extracted with methylene chloride, removing the MC and DPA. The extract is blown to dryness with dry air, dissolved in ethylene dichloride, and analyzed on a Perkin-Elmer 226 Flame Chromatograph.</description><subject>AMINES</subject><subject>Ammunition and Explosives</subject><subject>AROMATIC COMPOUNDS</subject><subject>CHLORIDES</subject><subject>CORROSION</subject><subject>DIPHENYLAMINE</subject><subject>ETHYLENES</subject><subject>GAS CHROMATOGRAPHY</subject><subject>GUNS</subject><subject>METHYL CENTRALITE</subject><subject>Physical Chemistry</subject><subject>POLYCYCLIC COMPOUNDS</subject><subject>PROPELLANTS</subject><subject>QUANTITATIVE ANALYSIS</subject><subject>STABILITY</subject><subject>STORAGE</subject><subject>TEMPERATURE</subject><fulltext>true</fulltext><rsrctype>report</rsrctype><creationdate>1966</creationdate><recordtype>report</recordtype><sourceid>1RU</sourceid><recordid>eNqFyrEKwjAQgOEsDqK-gcO9QKFUFB2P5NoEkkuI59CpilYoiEvz_ujg7vQP379U1w7PoG2OASV2GZN1GgwJ5eAYxUWG2EIgsb0HTSwZvRMCZAPGJUvce_yuBI6hqasQoLswpBwTeY8sa7V43l7zuPl1pbYtibbVo0z3YS7TeywDmvpY70_NYfeHP3pQMF4</recordid><startdate>19661207</startdate><enddate>19661207</enddate><creator>Alston, Percy L</creator><creator>Den Hartog, Laura J</creator><creator>Oesterling, David H</creator><creator>Shafer, James E</creator><scope>1RU</scope><scope>BHM</scope></search><sort><creationdate>19661207</creationdate><title>GAS CHROMATOGRAPHIC DETERMINATION OF METHYL CENTRALITE AND DIPHENYLAMINE IN 20-MM GUN PROPELLANT</title><author>Alston, Percy L ; Den Hartog, Laura J ; Oesterling, David H ; Shafer, James E</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-dtic_stinet_AD08059263</frbrgroupid><rsrctype>reports</rsrctype><prefilter>reports</prefilter><language>eng</language><creationdate>1966</creationdate><topic>AMINES</topic><topic>Ammunition and Explosives</topic><topic>AROMATIC COMPOUNDS</topic><topic>CHLORIDES</topic><topic>CORROSION</topic><topic>DIPHENYLAMINE</topic><topic>ETHYLENES</topic><topic>GAS CHROMATOGRAPHY</topic><topic>GUNS</topic><topic>METHYL CENTRALITE</topic><topic>Physical Chemistry</topic><topic>POLYCYCLIC COMPOUNDS</topic><topic>PROPELLANTS</topic><topic>QUANTITATIVE ANALYSIS</topic><topic>STABILITY</topic><topic>STORAGE</topic><topic>TEMPERATURE</topic><toplevel>online_resources</toplevel><creatorcontrib>Alston, Percy L</creatorcontrib><creatorcontrib>Den Hartog, Laura J</creatorcontrib><creatorcontrib>Oesterling, David H</creatorcontrib><creatorcontrib>Shafer, James E</creatorcontrib><creatorcontrib>NAVAL ORDNANCE STATION INDIAN HEAD MD QUALITY ASSURANCE DEPT</creatorcontrib><collection>DTIC Technical Reports</collection><collection>DTIC STINET</collection></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext_linktorsrc</fulltext></delivery><addata><au>Alston, Percy L</au><au>Den Hartog, Laura J</au><au>Oesterling, David H</au><au>Shafer, James E</au><aucorp>NAVAL ORDNANCE STATION INDIAN HEAD MD QUALITY ASSURANCE DEPT</aucorp><format>book</format><genre>unknown</genre><ristype>RPRT</ristype><btitle>GAS CHROMATOGRAPHIC DETERMINATION OF METHYL CENTRALITE AND DIPHENYLAMINE IN 20-MM GUN PROPELLANT</btitle><date>1966-12-07</date><risdate>1966</risdate><abstract>This report presents a rapid procedure for precise determinations of both methyl centralite (MC), also known as dimethyldiphenylurea, and diphenylamine (DPA). The sample is extracted with methylene chloride, removing the MC and DPA. The extract is blown to dryness with dry air, dissolved in ethylene dichloride, and analyzed on a Perkin-Elmer 226 Flame Chromatograph.</abstract><oa>free_for_read</oa></addata></record> |
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source | DTIC Technical Reports |
subjects | AMINES Ammunition and Explosives AROMATIC COMPOUNDS CHLORIDES CORROSION DIPHENYLAMINE ETHYLENES GAS CHROMATOGRAPHY GUNS METHYL CENTRALITE Physical Chemistry POLYCYCLIC COMPOUNDS PROPELLANTS QUANTITATIVE ANALYSIS STABILITY STORAGE TEMPERATURE |
title | GAS CHROMATOGRAPHIC DETERMINATION OF METHYL CENTRALITE AND DIPHENYLAMINE IN 20-MM GUN PROPELLANT |
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