GAS CHROMATOGRAPHIC DETERMINATION OF METHYL CENTRALITE AND DIPHENYLAMINE IN 20-MM GUN PROPELLANT

This report presents a rapid procedure for precise determinations of both methyl centralite (MC), also known as dimethyldiphenylurea, and diphenylamine (DPA). The sample is extracted with methylene chloride, removing the MC and DPA. The extract is blown to dryness with dry air, dissolved in ethylene...

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Hauptverfasser: Alston, Percy L, Den Hartog, Laura J, Oesterling, David H, Shafer, James E
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creator Alston, Percy L
Den Hartog, Laura J
Oesterling, David H
Shafer, James E
description This report presents a rapid procedure for precise determinations of both methyl centralite (MC), also known as dimethyldiphenylurea, and diphenylamine (DPA). The sample is extracted with methylene chloride, removing the MC and DPA. The extract is blown to dryness with dry air, dissolved in ethylene dichloride, and analyzed on a Perkin-Elmer 226 Flame Chromatograph.
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source DTIC Technical Reports
subjects AMINES
Ammunition and Explosives
AROMATIC COMPOUNDS
CHLORIDES
CORROSION
DIPHENYLAMINE
ETHYLENES
GAS CHROMATOGRAPHY
GUNS
METHYL CENTRALITE
Physical Chemistry
POLYCYCLIC COMPOUNDS
PROPELLANTS
QUANTITATIVE ANALYSIS
STABILITY
STORAGE
TEMPERATURE
title GAS CHROMATOGRAPHIC DETERMINATION OF METHYL CENTRALITE AND DIPHENYLAMINE IN 20-MM GUN PROPELLANT
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