Low temperature degradation of laser patterned 3Y-TZP: Enhancement of resistance after thermal treatment

The aim of this study is to characterize the resistance to low temperature degradation (LTD) of the surface of dental-grade zirconia (3Y-TZP) patterned with a Nd:YAG laser (532nm harmonic and pulse duration of 10ns) employing an interference setup. Laser patterning decreases the resistance to LTD of...

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Veröffentlicht in:Journal of the European Ceramic Society 2018-04, Vol.38 (4), p.1742-1749
Hauptverfasser: Roitero, E., Ochoa, M., Anglada, M., Mücklich, F., Jiménez-Piqué, E.
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container_end_page 1749
container_issue 4
container_start_page 1742
container_title Journal of the European Ceramic Society
container_volume 38
creator Roitero, E.
Ochoa, M.
Anglada, M.
Mücklich, F.
Jiménez-Piqué, E.
description The aim of this study is to characterize the resistance to low temperature degradation (LTD) of the surface of dental-grade zirconia (3Y-TZP) patterned with a Nd:YAG laser (532nm harmonic and pulse duration of 10ns) employing an interference setup. Laser patterning decreases the resistance to LTD of 3Y-TZP because of the presence of monoclinic phase and residual stresses, induced by the thermal shock during laser-material interaction. A thermal treatment (1h at 1200°C) anneals the affected microstructure and increase the resistance to LTD of laser patterned 3Y-TZP. Transformation delay may be attributed to monoclinic phase reversion, texture in the tetragonal phase and the existence of a net of shallow microcracks on the surface, accommodating autocatalytic transformation.
doi_str_mv 10.1016/j.jeurceramsoc.2017.10.044
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source Recercat; Elsevier ScienceDirect Journals
subjects 3Y-TZP
Aging
Direct laser interference patterning
Enginyeria dels materials
Envelliment
Laser treatment
Low temperature degradation
Low temperature engineering
Àrees temàtiques de la UPC
title Low temperature degradation of laser patterned 3Y-TZP: Enhancement of resistance after thermal treatment
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