A facile thermal decomposition route to synthesise CoFe2O4 nanostructures

The synthesis of CoFe 2 O 4 nanoparticles has been achieved by a simple thermal decomposition method from an inorganic precursor, cobalt ferrous cinnamate hydrazinate (CoFe 2 (cin) 3 (N 2 H 4 ) 3 ) which was obtained by a novel precipitation method from the corresponding metal salts, cinnamic acid and hydrazine hydrate. The precursor was characterized by hydrazine and metal analyses, infrared spectral analysis and thermo gravimetric analysis. Under appropriate annealing, CoFe 2 (cin) 3 (N 2 H 4 ) 3 yielded CoFe 2 O 4 nanoparticles, which were characterized for their size and structure using X-Ray diffraction (XRD), high resolution transmission electron microscopic (HRTEM), selected area electron diffraction (SAED) and scanning electron microscopic (SEM) techniques.