Characterization and catalytic performance of potassium loaded on rice husk silica and zeolite nay for transesterification of jatropha seed oil
Rice husk silica (RHS) and NaY were used as supports for potassium (K) prepared from acetate buffer (B) and acetate (A) solutions. K loading did not destroy the NaY structure, but it caused a decrease in the surface area; the K species resided in micropores and on the external surface. In contrast,...
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Veröffentlicht in: | Química Nova 2013, Vol.36 (8), p.1116-1120 |
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description | Rice husk silica (RHS) and NaY were used as supports for potassium (K) prepared from acetate buffer (B) and acetate (A) solutions. K loading did not destroy the NaY structure, but it caused a decrease in the surface area; the K species resided in micropores and on the external surface. In contrast, K loading resulted in the collapse and a decrease in the surface area of RHS. It was found that 12K/NaY-B was the most active catalyst for the transesterification of Jatropha seed oil. The minimum K content in K/NaY-B that provided complete conversion of the Jatropha seed oil was 11 wt%, and the biodiesel yield was 77.9%. |
doi_str_mv | 10.1590/S0100-40422013000800007 |
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K loading did not destroy the NaY structure, but it caused a decrease in the surface area; the K species resided in micropores and on the external surface. In contrast, K loading resulted in the collapse and a decrease in the surface area of RHS. It was found that 12K/NaY-B was the most active catalyst for the transesterification of Jatropha seed oil. The minimum K content in K/NaY-B that provided complete conversion of the Jatropha seed oil was 11 wt%, and the biodiesel yield was 77.9%.</description><identifier>ISSN: 0100-4042</identifier><identifier>ISSN: 1678-7064</identifier><identifier>DOI: 10.1590/S0100-40422013000800007</identifier><language>eng</language><publisher>Sociedade Brasileira de Química</publisher><subject>CHEMISTRY, MULTIDISCIPLINARY ; Jatropha seed oil ; potassium ; zeolite NaY</subject><ispartof>Química Nova, 2013, Vol.36 (8), p.1116-1120</ispartof><rights>This work is licensed under a Creative Commons Attribution-NonCommercial 4.0 International License.</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c411t-19dcd0a8acb60d402c496e62acc69d164a01590fd9116ae293875010d6f627c73</citedby></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>230,314,780,784,864,885,4024,27923,27924,27925</link.rule.ids></links><search><creatorcontrib>Montalbo, Kathrina D.</creatorcontrib><creatorcontrib>Leon, Rizalinda L. de</creatorcontrib><creatorcontrib>Sophiphun, Onsulang</creatorcontrib><creatorcontrib>Manadee, Saowanee</creatorcontrib><creatorcontrib>Prayoonpokarach, Sanchai</creatorcontrib><creatorcontrib>Wittayakun, Jatuporn</creatorcontrib><title>Characterization and catalytic performance of potassium loaded on rice husk silica and zeolite nay for transesterification of jatropha seed oil</title><title>Química Nova</title><addtitle>Quím. Nova</addtitle><description>Rice husk silica (RHS) and NaY were used as supports for potassium (K) prepared from acetate buffer (B) and acetate (A) solutions. K loading did not destroy the NaY structure, but it caused a decrease in the surface area; the K species resided in micropores and on the external surface. In contrast, K loading resulted in the collapse and a decrease in the surface area of RHS. It was found that 12K/NaY-B was the most active catalyst for the transesterification of Jatropha seed oil. The minimum K content in K/NaY-B that provided complete conversion of the Jatropha seed oil was 11 wt%, and the biodiesel yield was 77.9%.</description><subject>CHEMISTRY, MULTIDISCIPLINARY</subject><subject>Jatropha seed oil</subject><subject>potassium</subject><subject>zeolite NaY</subject><issn>0100-4042</issn><issn>1678-7064</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2013</creationdate><recordtype>article</recordtype><sourceid>DOA</sourceid><recordid>eNp1kU1OwzAQhbMAiVI4A75AythJnWSJKn4qVWIBrK2Jf6hDGle2u2gvwZVxWtQNYjGyNOP3zdObLLujMKPzBu7fgALkJZSMAS0AoE4F1UU2OQ-ususQOgBWFdV8kn0v1uhRRu3tAaN1A8FBEYkR-320kmy1N85vcJCaOEO2LmIIdrchvUOlFUkCb9NsvQtfJNjeSjwSDtr1Nmoy4J4kAIkeh6DDuMekP8dNiddh9G67RhL0CLP9TXZpsA_69vedZh9Pj--Ll3z1-rxcPKxyWVIac9ooqQBrlC0HVQKTZcM1ZyglbxTlJcIYiFENpRw1a4q6mqcMFDecVbIqptnyxFUOO7H1doN-LxxacWw4_ynQpwB6LTRww1pV1Yis5K1pS4mc1nVCa962MrFmJ1aQVvdOdG7nh2ReHM8h_pwjCaqTQHoXgtfmbICCGH3_q_wBZdSTUw</recordid><startdate>2013</startdate><enddate>2013</enddate><creator>Montalbo, Kathrina D.</creator><creator>Leon, Rizalinda L. de</creator><creator>Sophiphun, Onsulang</creator><creator>Manadee, Saowanee</creator><creator>Prayoonpokarach, Sanchai</creator><creator>Wittayakun, Jatuporn</creator><general>Sociedade Brasileira de Química</general><scope>AAYXX</scope><scope>CITATION</scope><scope>GPN</scope><scope>DOA</scope></search><sort><creationdate>2013</creationdate><title>Characterization and catalytic performance of potassium loaded on rice husk silica and zeolite nay for transesterification of jatropha seed oil</title><author>Montalbo, Kathrina D. ; Leon, Rizalinda L. de ; Sophiphun, Onsulang ; Manadee, Saowanee ; Prayoonpokarach, Sanchai ; Wittayakun, Jatuporn</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c411t-19dcd0a8acb60d402c496e62acc69d164a01590fd9116ae293875010d6f627c73</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2013</creationdate><topic>CHEMISTRY, MULTIDISCIPLINARY</topic><topic>Jatropha seed oil</topic><topic>potassium</topic><topic>zeolite NaY</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Montalbo, Kathrina D.</creatorcontrib><creatorcontrib>Leon, Rizalinda L. de</creatorcontrib><creatorcontrib>Sophiphun, Onsulang</creatorcontrib><creatorcontrib>Manadee, Saowanee</creatorcontrib><creatorcontrib>Prayoonpokarach, Sanchai</creatorcontrib><creatorcontrib>Wittayakun, Jatuporn</creatorcontrib><collection>CrossRef</collection><collection>SciELO</collection><collection>DOAJ Directory of Open Access Journals</collection><jtitle>Química Nova</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Montalbo, Kathrina D.</au><au>Leon, Rizalinda L. de</au><au>Sophiphun, Onsulang</au><au>Manadee, Saowanee</au><au>Prayoonpokarach, Sanchai</au><au>Wittayakun, Jatuporn</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Characterization and catalytic performance of potassium loaded on rice husk silica and zeolite nay for transesterification of jatropha seed oil</atitle><jtitle>Química Nova</jtitle><addtitle>Quím. Nova</addtitle><date>2013</date><risdate>2013</risdate><volume>36</volume><issue>8</issue><spage>1116</spage><epage>1120</epage><pages>1116-1120</pages><issn>0100-4042</issn><issn>1678-7064</issn><abstract>Rice husk silica (RHS) and NaY were used as supports for potassium (K) prepared from acetate buffer (B) and acetate (A) solutions. K loading did not destroy the NaY structure, but it caused a decrease in the surface area; the K species resided in micropores and on the external surface. In contrast, K loading resulted in the collapse and a decrease in the surface area of RHS. It was found that 12K/NaY-B was the most active catalyst for the transesterification of Jatropha seed oil. The minimum K content in K/NaY-B that provided complete conversion of the Jatropha seed oil was 11 wt%, and the biodiesel yield was 77.9%.</abstract><pub>Sociedade Brasileira de Química</pub><doi>10.1590/S0100-40422013000800007</doi><tpages>5</tpages><oa>free_for_read</oa></addata></record> |
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subjects | CHEMISTRY, MULTIDISCIPLINARY Jatropha seed oil potassium zeolite NaY |
title | Characterization and catalytic performance of potassium loaded on rice husk silica and zeolite nay for transesterification of jatropha seed oil |
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